Parallelized Millireactor System Flow Damping

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Solution Overview

Problem

Current micro/millireactor systems face limitations in volumetric throughput due to flow rate pulsations and uneven fluid distribution in parallelized multiphase reactor networks, leading to instability and reduced productivity in multiphase reactions.

Innovation Solution

A quantitative fluidic circuit-based design framework combining resistance-based fluid distribution and capacitance-based autonomous flow regulation, utilizing a simple passive capacitance-based method for damping periodic and aperiodic flow pulsations, and incorporating inline hydraulic dampers for stable operation of parallelized triphasic segmented-flow reactor systems.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If multiple identical micro/millireactors are operated in parallel to increase volumetric throughput, then productivity is improved, but flow rate pulsations and uneven fluid distribution occur leading to system instability

Engineering Contradiction:
Improvevolumetric throughputVSAvoidflow stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

A flow distributor network with damping elements is introduced as an intermediary component between the pump and the parallel reactor array. This mediator absorbs flow pulsations and ensures uniform distribution of reactants to each reactor, resolving the contradiction between high throughput and flow stability.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The system segments the flow distribution into multiple independent pathways, each with its own damping characteristics. By dividing the total flow into N separate reactor feeds with individual flow resistance elements, the system maintains stability in each channel while achieving high overall throughput through parallel operation.

Inventive Principle:
Principle #1Segmentation

2Ease of operation

If peristaltic pumps are used to continuously withdraw feedstock from large reservoirs, then ease of operation is improved, but flow rate pulsations are introduced into the system

Engineering Contradiction:
Improvecontinuous feedstock withdrawalVSAvoidflow rate stability
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The flow distributor network acts as an intermediary that decouples the pump's pulsatile output from the reactor's steady-state requirements. The damping elements in the distributor absorb the pulsations generated by the peristaltic pump, allowing continuous feedstock withdrawal while maintaining stable flow rates to the reactors.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

Damping elements are placed in advance within the flow distribution network to cushion the flow pulsations before they reach the reactors. This preemptive cushioning prevents pulsations from affecting reaction stability while preserving the operational simplicity of continuous pump feeding.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

3Manufacturing precision

If feed distribution is optimized for evenness, then reaction consistency is improved, but device complexity increases due to additional flow control components

Engineering Contradiction:
Improvefeed distribution uniformityVSAvoidflow distribution network complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The system achieves even feed distribution by carefully selecting and adjusting flow resistance parameters of the damping elements and channel dimensions. By optimizing these physical parameters rather than adding complex active control mechanisms, uniformity is achieved with minimal additional complexity.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The flow distributor network is designed to self-regulate and automatically equalize flow distribution across parallel channels through passive damping elements. This self-service mechanism eliminates the need for complex external control systems while maintaining consistent feed distribution to all reactors.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution achieves tremendous mass transport acceleration and facilitates continuous catalyst recovery and recycle, ensuring consistent substrate conversion across multiple reactors with reduced flow rate deviations, enhancing the efficiency and stability of multiphase reactions.

Implementation Method 1

a first hydraulic damper disposed between the two ends of the first feed line; a second hydraulic damper disposed between the two ends of the second feed line

Methodology Applied
Scientific EffectHydraulic damping: Damping

Data Source

PatentUS9902686B2Multiphase reactor system
Publication Date: 2018.02.27 NATIONAL UNIVERSITY OF SINGAPORE
  • US9902686B2 patent drawing
  • US9902686B2 patent drawing
  • US9902686B2 patent drawing

AI summary

A one-to-many parallelized millireactor system capable of high throughput production in millireactors. Also disclosed is a method for carrying out multi-phase reactions.