Paramagnetic Garnet Ceramic for Magnetocaloric Cooling Below 1 Kelvin

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Solution Overview

Problem

Existing magnetocaloric materials, such as hydrated paramagnetic salts and monocrystalline garnets, are limited in their application due to dehydration issues, mechanical fragility, and high manufacturing costs, making them unsuitable for temperatures above 35°C and difficult to integrate into large-sized cooling devices.

Innovation Solution

A cooling device utilizing a paramagnetic garnet ceramic as the magnetocaloric element, which offers mechanical robustness and high thermal conductivity, allowing for effective cooling across a wide temperature range while being easier to integrate and manufacture in large sizes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Temperature

If hydrated paramagnetic salts are used as magnetocaloric material, then cooling effect is achieved at low temperatures, but the material dehydrates and requires sealed enclosure

Engineering Contradiction:
Improvelow temperature coolingVSAvoidmaterial stability
Core Design Contradiction:
TemperatureVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters by using anhydrous paramagnetic salts (such as anhydrous aluminum chloride, anhydrous ferric chloride, or their mixtures with alkali halides) instead of hydrated salts. This parameter change eliminates the dehydration problem while maintaining the magnetocaloric effect at low temperatures, achieving both cooling performance and material stability.

Inventive Principle:
Principle #35Parameter changes

2Temperature

If monocrystalline garnets are used, then thermal conductivity is sufficient at low temperature, but manufacturing costs are high and large-sized parts cannot be obtained

Engineering Contradiction:
Improvelow temperature thermal conductivityVSAvoidmanufacturing cost and size
Core Design Contradiction:
TemperatureVSEase of manufacture

Solution Approach 1:

The patent uses composite paramagnetic salt systems (such as mixtures of anhydrous aluminum chloride with alkali halides like sodium chloride, potassium chloride, or cesium chloride) that exhibit garnet-like magnetic properties. These composite materials can be manufactured as large-sized parts through conventional sintering or melting processes, avoiding the high costs and size limitations of monocrystalline garnet growth while maintaining adequate thermal conductivity at low temperatures.

Inventive Principle:
Principle #40Composite materials

3Temperature

If ferric ammonium alums are used, then cooling is achieved below 1 Kelvin, but the material decomposes at temperatures exceeding 35°C

Engineering Contradiction:
Improvesub-1 Kelvin coolingVSAvoidthermal stability
Core Design Contradiction:
TemperatureVSStability of the object's composition

Solution Approach 1:

The patent changes the chemical stability parameters by selecting anhydrous paramagnetic salts with higher thermal stability. These materials (anhydrous aluminum chloride, anhydrous ferric chloride, and their eutectic mixtures with alkali halides) remain stable at temperatures above 35°C, eliminating decomposition issues while still achieving sub-1 Kelvin cooling through their magnetocaloric properties at cryogenic temperatures.

Inventive Principle:
Principle #35Parameter changes

4Temperature

If monocrystalline materials are used, then thermal conductivity is adequate, but the materials are mechanically fragile and integration is difficult

Engineering Contradiction:
Improvethermal conductivityVSAvoidmechanical robustness
Core Design Contradiction:
TemperatureVSStrength

Solution Approach 1:

The patent employs composite paramagnetic salt systems that can be processed into polycrystalline or sintered forms. These composite materials combine the magnetic properties needed for magnetocaloric cooling with improved mechanical strength and ease of integration, avoiding the fragility of monocrystalline materials while maintaining adequate thermal conductivity for low-temperature operation.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The paramagnetic garnet ceramic enables efficient cooling across very low temperatures, is mechanically resistant, and can be easily integrated into cooling devices, overcoming the limitations of traditional materials by providing high thermal conductivity and cost-effective production of large-sized parts.

Implementation Method 1

Magnetic refrigeration has been known since the beginning of the 20th century. The cooling effect is obtained by combining a paramagnetic material (called magnetocaloric) with a variable external magnetic field. When the material undergoes magnetization or demagnetization, its temperature varies significantly.

Methodology Applied
Scientific EffectMagnetocaloric effect: Magnetocaloric Effect

Implementation Method 2

The hot source and the cold source are conventionally separated from the magnetocaloric element by thermal switches.

Methodology Applied
Scientific EffectThermal conduction: Conduction (thermal)

Data Source

PatentEP3671065A1Cooling device comprising a paramagnetic garnet ceramic
Publication Date: 2020.06.24 COMMISSARIAT A LENERGIE ATOMIQUE ET AUX ENERGIES ALTERNATIVES
  • EP3671065A1 patent drawingFigure 1~2a
  • EP3671065A1 patent drawingFigure 2b~4
  • EP3671065A1 patent drawingFigure 5a~5b

AI summary

A magnetic cooling device (100) comprising a magnetocaloric element (110), the magnetocaloric element (110) comprising a paramagnetic garnet, characterized in that the paramagnetic garnet is a ceramic. The paramagnetic garnet ceramic preferably has a density greater than or equal to 90% and strictly less than 100%. The paramagnetic garnet ceramic is preferably a gallium gadolinium garnet ceramic or a gallium ytterbium garnet ceramic.