Particle Beam Gas Feed Unit With Micro-Valves for Stable Deposition

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Solution Overview

Problem

Existing gas feed devices for particle beam apparatuses face challenges in achieving immediate and constant control over the flow of precursor gases, leading to delayed and inconsistent deposition rates, potential plasma discharges, and contamination risks due to multiple feed units and thermal decomposition issues.

Innovation Solution

A gas feed device with a single feed unit and micro-valves for each precursor reservoir, allowing precise control over the flow of precursor gases, enabling immediate and constant adjustments, and incorporating cleaning mechanisms to prevent contamination and thermal issues.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If multiple feed units are used for different precursors, then the ability to feed multiple precursors is improved, but the risk of contamination between precursors increases

Engineering Contradiction:
Improveability to feed multiple precursorsVSAvoidcontamination risk
Core Design Contradiction:
Adaptability or versatilityVSObject-affected harmful factors

Solution Approach 1:

The patent combines multiple precursor feeding functions into a single feed unit by sequentially introducing different precursors. The feed unit is designed to handle multiple precursors through time-separated introduction, eliminating cross-contamination while maintaining the capability to process multiple precursor types.

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The system employs periodic action by sequentially introducing different precursors at different time intervals through the same feed unit. Each precursor is introduced in a separate time window, preventing contamination while maintaining versatility in handling multiple precursor types.

Inventive Principle:
Principle #19Periodic action

2Object-affected harmful factors

If the precursor reservoir is kept warm to prevent condensation, then condensation is reduced, but thermal decomposition of the precursor increases

Engineering Contradiction:
ImprovecondensationVSAvoidthermal decomposition
Core Design Contradiction:
Object-affected harmful factorsVSObject-generated harmful factors

Solution Approach 1:

The system applies local quality by maintaining different temperature zones: the precursor reservoir is kept at a lower temperature to prevent thermal decomposition, while the feed unit and delivery pathways are heated to prevent condensation. This localized temperature differentiation resolves the contradiction between preventing condensation and avoiding thermal decomposition.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The system segments the temperature control into distinct zones: a cold reservoir for storing precursors and a warm feed unit for delivery. This segmentation allows each component to operate at its optimal temperature, preventing both condensation in the delivery system and thermal decomposition in the storage system.

Inventive Principle:
Principle #1Segmentation

3Stability of the object's composition

If the flow of precursor gas is increased to maintain constant deposition rate, then deposition rate stability is improved, but the likelihood of plasma discharge increases

Engineering Contradiction:
Improvedeposition rate stabilityVSAvoidplasma discharge
Core Design Contradiction:
Stability of the object's compositionVSObject-affected harmful factors

Solution Approach 1:

The system uses periodic action by introducing precursors in pulsed or sequential manner rather than continuous flow. This periodic introduction maintains average deposition rate stability while reducing instantaneous gas flow levels, thereby minimizing plasma discharge risks.

Inventive Principle:
Principle #19Periodic action

Solution Approach 2:

The system dynamically adjusts precursor flow rates based on real-time process conditions. By using feedback control, the system maintains optimal deposition rates while adapting flow levels to prevent plasma discharge conditions, resolving the contradiction between stability and harmful effects.

Inventive Principle:
Principle #15Dynamics

4Measurement precision

If micro-valves are used for precise flow control, then flow control precision is improved, but device complexity increases

Engineering Contradiction:
Improveflow control precisionVSAvoiddevice complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The system merges multiple valve functions into a single micro-valve unit that can sequentially control multiple precursor flows. This consolidation reduces the total number of valves needed while maintaining precise flow control through the shared micro-valve, balancing precision with reduced complexity.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables immediate and constant control over precursor gas flow, reduces deposition rate variability, minimizes contamination risks, and maintains apparatus functionality by using micro-valves and cleaning mechanisms.

Implementation Method 1

each precursor reservoir (1002, 1003) has its own micro-valve (1021, 1022) for controlling the flow of the respective precursor

Methodology Applied
Scientific EffectValve control: Valve

Implementation Method 2

a gaseous precursor substance is admitted into the object chamber... a layer of a substance is deposited on the surface of the object

Methodology Applied
Scientific EffectPhysical vapor deposition: Physical Vapour Deposition

Implementation Method 3

a gaseous precursor substance is admitted into the object chamber... a layer of a substance is deposited on the surface of the object

Methodology Applied
Scientific EffectChemical vapor deposition: Chemical Vapour Deposition

Implementation Method 4

provision is made for the line devices (L1, L2) and/or the feed unit (1001) to be heated

Methodology Applied
Scientific EffectThermal heating: Heating

Implementation Method 5

By means of a gas feed device, a gaseous state of a precursor substance-a so—called precursor—can be admitted into the object chamber... a layer of a substance is deposited on the surface of the object

Methodology Applied
Scientific EffectIon beam interaction: Ion Beam

Implementation Method 6

an electron beam (also referred to as primary electron beam below) is generated by means of a beam generator and focused onto an object

Methodology Applied
Scientific EffectElectron beam interaction: Electron Beam

Data Source

PatentUS12562337B2Gas supply device, particle beam apparatus having a gas supply device, and method of operating the gas supply device and the particle beam apparatus
Publication Date: 2026.02.24 CARL ZEISS MICROSCOPY GMBH
  • US12562337B2 patent drawing
  • US12562337B2 patent drawing
  • US12562337B2 patent drawing

AI summary

The system described herein relates to a gas feed device having a first precursor reservoir that receives a first precursor and having a second precursor reservoir that receives a second precursor, a feed unit that feeds a gaseous state of the first precursor and/or a gaseous state of the second precursor onto a surface of an object. A first line device is arranged between the first precursor reservoir and the feed unit. A second line device is arranged between the second precursor reservoir and the feed unit. A first valve is arranged between the first line device and the feed unit. A second valve is arranged between the second line device and the feed unit. A control valve for the feed of the gaseous state of the first precursor and/or the gaseous state of the second precursor is connected to the first valve, the second valve and the feed unit.