Particle Beam Sample Opening for High-Resolution Analysis

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Solution Overview

Problem

Current methods for analyzing samples in particle beam devices are prone to contamination, time-consuming, and risk sample damage due to the need to transfer samples between devices, and offer limited spatial resolution due to oblique angles of examination.

Innovation Solution

A method where a particle beam is used to create an opening in the sample material adjacent to the area of interest, allowing for the separation and detailed examination of the sample without transfer, using backscattered particles for analysis, enabling perpendicular beam incidence and reducing contamination risks.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If the part of the sample to be analyzed is taken out of the first particle beam device and taken into a second particle beam device, then detailed examination can be performed, but the sample part may be contaminated, damaged, and the process becomes very time-consuming

Engineering Contradiction:
Improveexamination detailVSAvoidtime-consuming transfer process
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent combines the sample preparation function (ion beam column) and the examination function (electron beam column) into a single particle beam device. This merging eliminates the need to transfer the sample part between different devices, thereby preventing contamination and damage during transfer while significantly reducing the time required for the analysis process.

Inventive Principle:
Principle #5Merging (Combining)

2Reliability

If the part of the sample to be analyzed is examined in the first particle beam device from an oblique angle, then the sample does not have to be taken out, but the spatial resolution is impaired and images may be distorted

Engineering Contradiction:
Improvesample integrityVSAvoidspatial resolution
Core Design Contradiction:
ReliabilityVSMeasurement precision

Solution Approach 1:

The patent employs a movable sample holder that can dynamically adjust the orientation and position of the sample part. This allows the sample to be positioned at optimal angles for examination, enabling high spatial resolution imaging while keeping the sample part securely mounted and preventing the need for physical transfer that could compromise sample integrity.

Inventive Principle:
Principle #15Dynamics

3Measurement precision

If a thin sample slice of only a few nm thickness is generated for transmission analysis, then transmission examination is possible, but the sample generation becomes very complicated

Engineering Contradiction:
Improvetransmission analysis capabilityVSAvoidsample generation complexity
Core Design Contradiction:
Measurement precisionVSEase of manufacture

Solution Approach 1:

The patent uses an ion beam column to segment and locally remove material from the sample, creating precisely defined openings or thinning specific regions. This segmented approach allows for controlled sample preparation where only the necessary areas are thinned or removed, making the sample generation process more manageable and less complicated while still achieving the required thickness for transmission analysis.

Inventive Principle:
Principle #1Segmentation

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach simplifies sample generation and analysis, enhances spatial resolution, and reduces the risk of sample damage by allowing examination within the same vacuum chamber without the need for sample transfer, thus improving efficiency and accuracy.

Implementation Method 1

analyzed by detecting the particles backscattered from the part of the sample to be analyzed or emitted from the part of the sample to be analyzed

Methodology Applied
Scientific EffectBackscattering: Scattering

Implementation Method 2

an opening is introduced in the sample material with the aid of a particle beam

Methodology Applied
Scientific EffectAblation: Ablation

Data Source

PatentUS8502142B2Charged particle beam analysis while part of a sample to be analyzed remains in a generated opening of the sample
Publication Date: 2013.08.06 CARL ZEISS MICROSCOPY GMBH
  • US8502142B2 patent drawing
  • US8502142B2 patent drawing
  • US8502142B2 patent drawing

AI summary

A device and method for analyzing a sample provide for extracting a part to be analyzed from the sample with the aid of a previously generated opening in the sample. The part to be analyzed is examined in greater detail with the aid of a particle beam. For this purpose, the sample is placed in the opening or on a sample holder.