Continuous Particle Manufacturing Reactors Using Taylor Vortex Crystallization

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Solution Overview

Problem

Conventional methods for manufacturing particles, such as polymer and inorganic particles, face challenges in producing uniformly sized, high-purity particles due to batch processes that result in non-uniform size distribution, low purity, and unsuitable apparatus designs for continuous production.

Innovation Solution

An apparatus comprising at least two reactors connected in sequence, where the first reactor mixes raw materials and the second reactor utilizes Taylor vortex flows to separate and crystallize particles, allowing for continuous production of uniformly dispersed particles with high purity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Adaptability or versatility

If batch process is used for particle manufacturing, then flexibility in processing different materials is maintained, but particle size uniformity and purity deteriorate

Engineering Contradiction:
Improveflexibility in processingVSAvoidparticle size uniformity
Core Design Contradiction:
Adaptability or versatilityVSManufacturing precision

Solution Approach 1:

The manufacturing process is segmented into multiple sequential reactors (first reactor for nucleation, second reactor for crystallization). This segmentation allows each reactor to perform a specific function, ensuring uniform particle size while maintaining the ability to process different materials by adjusting parameters in each stage.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The invention transitions from batch process to continuous process by connecting multiple reactors in sequence with continuous material feed. This continuous action ensures consistent particle formation and improves both uniformity and purity without sacrificing processing flexibility.

Inventive Principle:
Principle #20Continuity of useful action

2Device complexity

If batch reactor is used, then process simplicity is maintained, but productivity and particle purity deteriorate

Engineering Contradiction:
Improveprocess simplicityVSAvoidcontinuous production capability
Core Design Contradiction:
Device complexityVSProductivity

Solution Approach 1:

The process is divided into sequential reaction stages in different reactors, allowing continuous operation while maintaining manageable complexity through modular design. Each reactor performs a specific function, simplifying the overall process control.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first reactor performs preliminary nucleation before the second reactor completes crystallization. This preliminary action in a dedicated stage improves overall productivity and particle purity while maintaining process simplicity through clear functional separation.

Inventive Principle:
Principle #10Preliminary action

3Device complexity

If single reactor is used, then device complexity is reduced, but particle dispersion uniformity and purity deteriorate

Engineering Contradiction:
Improvenumber of reactorsVSAvoidparticle dispersion uniformity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The reaction process is segmented into nucleation (first reactor) and crystallization (second reactor) stages. This segmentation achieves uniform particle dispersion and high purity by controlling each stage separately, while the modular design keeps device complexity manageable.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The first reactor acts as an intermediary stage that prepares uniformly nucleated particles before they enter the second reactor for final crystallization. This intermediary step is crucial for achieving uniform dispersion and high purity without excessive device complexity.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Device complexity

If conventional particle formation method is used, then process simplicity is maintained, but particle surface uniformity and purity deteriorate

Engineering Contradiction:
Improveprocess structureVSAvoidsurface uniformity
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The particle formation process is segmented into nucleation and crystallization stages in separate reactors. This segmentation enables uniform particle surfaces by controlling crystal growth in the second reactor after uniform nucleation in the first reactor, maintaining reasonable process structure.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Uniform nucleation is achieved as a preliminary action in the first reactor before particles enter the second reactor for controlled crystallization. This preliminary uniformity is essential for achieving smooth particle surfaces and high purity without overly complex processing.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus enables the production of uniformly sized and high-purity particles by separating nucleation and crystallization processes, improving particle uniformity and purity compared to traditional batch methods.

Implementation Method 1

a mixing means formed in the hollow inside of the main body to mix materials fed from the first and second raw material inlets

Methodology Applied
Scientific EffectMixing: Stirring

Implementation Method 2

a heat exchanger material passage formed between the outer circumference and inner circumference of the cylinder to provide a passage for a heat exchanger material

Methodology Applied
Scientific EffectHeat exchange: Heat Exchanger

Implementation Method 3

the second reactor utilizes Taylor vortex flows to separate and crystallize particles

Methodology Applied
Scientific EffectVortex flow: Vortex Ring

Implementation Method 4

the second reactor utilizes Taylor vortex flows to separate and crystallize particles

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Data Source

PatentUS10005062B2Apparatus for manufacturing particles and method for manufacturing particles using the same
Publication Date: 2018.06.26 LAMINAR
  • US10005062B2 patent drawing
  • US10005062B2 patent drawing
  • US10005062B2 patent drawing

AI summary

Apparatus for manufacturing particles has at least one reactor and a method for manufacturing particles using the same. A first reactor has a hollow main body extending in the lengthwise direction, first and second raw material inlets formed at the one side end of the main body, a reactant outlet formed at the other side end of the main body, and a mixer formed inside the main body to mix materials fed from the first and second raw material inlets. A second reactor of the apparatus connected to one side of the first reactor has a non-revolving hollow cylinder extending in the lengthwise direction, a revolving body extending in the lengthwise direction, a driver portion, a reactant inlet formed on the outer circumference at one side end of the cylinder and connected to the reactant outlet of the first reactor.