PCD Compact Substrate Cobalt Control

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Solution Overview

Problem

Polycrystalline diamond compact (PCD) cutter elements face a challenge in achieving improved overall erosion resistance without compromising fracture resistance, as existing substrates tend to deteriorate at high temperatures due to residual solvent/catalyst materials.

Innovation Solution

A PCD composite compact element is developed with a cemented carbide substrate having a specific mean free path and elastic limit, bonded to a PCD structure, where the substrate's peripheral region comprises metal carbide particles and a metallic binder material with controlled cobalt content, and optionally reinforced with nano-particles, to enhance erosion and fracture resistance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If conventional cemented carbide substrates with high cobalt content are used to improve fracture toughness, then fracture resistance is improved, but erosion resistance deteriorates due to residual solvent/catalyst material at high temperatures

Engineering Contradiction:
Improvefracture toughnessVSAvoiderosion resistance
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent applies parameter changes by controlling the cobalt content in the cemented carbide substrate to specific ranges (5-15 weight percent) and adjusting the mean free path of the carbide grains (0.1-0.7 microns). These parameter optimizations balance the competing requirements for fracture toughness and erosion resistance, eliminating the need for excessive cobalt while maintaining both properties through controlled material composition and microstructure.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite materials by combining cemented carbide substrate with polycrystalline diamond compact (PCD) layer. The cemented carbide provides fracture toughness while the PCD layer provides erosion resistance. The interface between these two materials is engineered to ensure strong bonding, creating a composite structure where each material contributes its advantageous properties without the drawbacks of individual materials.

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If cemented carbide substrate with optimized mean free path and elastic limit is used, then overall erosion resistance is improved, but manufacturing complexity increases due to specific material requirements

Engineering Contradiction:
Improveerosion resistanceVSAvoidmanufacturing complexity
Core Design Contradiction:
Object-affected harmful factorsVSDevice complexity

Solution Approach 1:

The patent specifies precise parameter ranges for the cemented carbide substrate including mean free path of 0.1-0.7 microns and elastic limit of 1.9-2.4 GPa. By defining these parameters clearly, the manufacturing process becomes more controllable and reproducible. The parameter specifications guide material selection and processing to achieve the desired performance without requiring overly complex manufacturing procedures.

Inventive Principle:
Principle #35Parameter changes

3Productivity

If PCD material is used in high temperature applications, then cutting performance is maintained, but mechanical properties deteriorate due to residual solvent/catalyst material

Engineering Contradiction:
Improvecutting performanceVSAvoidmechanical properties
Core Design Contradiction:
ProductivityVSStrength

Solution Approach 1:

The patent addresses the residual solvent/catalyst material problem by using a cemented carbide substrate with controlled cobalt content (5-15 weight percent) that is optimized to minimize residual solvent material in the PCD layer after sintering. The substrate composition is specifically designed to provide just enough cobalt for the sintering process without excessive amounts that would remain as harmful residual material, thereby maintaining mechanical properties at high temperatures.

Inventive Principle:
Principle #2Taking out (Extraction)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution provides enhanced erosion resistance and fracture toughness, leading to improved durability and extended working life of PCD composite compact elements in applications like earth boring and rock drilling, without significant degradation at elevated temperatures.

Implementation Method 1

PCD may be formed by subjecting an aggregated mass of diamond grains to an ultra-high pressure and temperature

Methodology Applied
Scientific EffectSintering: Sintering

Implementation Method 2

The sintering aid may be referred to as a solvent/catalyst material for diamond, owing to its function of dissolving diamond to some extent and catalyst its re-precipitation

Methodology Applied
Scientific EffectDissolution:

Implementation Method 3

A material capable of promoting the growth of diamond or the direct diamond-to-diamond inter-growth between diamond grains at a pressure and temperature condition at which diamond is thermodynamically stable

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentUS9970240B2Polycrystalline diamond composite compact
Publication Date: 2018.05.15 ELEMENT SIX GMBH
  • US9970240B2 patent drawing
  • US9970240B2 patent drawing
  • US9970240B2 patent drawing

AI summary

A polycrystalline diamond (PCD) composite compact element comprising a PCD structure bonded to a cemented carbide substrate, in which at least a peripheral region of the substrate comprises cemented carbide material having a mean free path (MFP) characteristic of at least about 0.1 microns and at most about 0.7 microns; and an elastic limit of at least about 1.9 GPa.