Pd-P Alloy Interlayer for Ceramic Substrate Wire Bonding

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Solution Overview

Problem

The existing methods for forming ceramic substrate parts with wire-bonding electrodes face issues such as nickel plating layer corrosion and palladium diffusion to the gold layer, leading to poor wire bondability and reliability, especially when using high-density mounting and lead-free, high-melting-point solders.

Innovation Solution

A ceramic substrate part is developed with a structure comprising a primer layer, a Ni-based lower layer, an intermediate Pd-P alloy layer, and a gold upper layer, where the Pd-P alloy layer prevents nickel corrosion and palladium diffusion, ensuring excellent wire bondability by controlling the phosphorus content and layer thickness.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a Ni plating layer is used as a barrier layer to protect the primer layer from solder, then the primer layer is protected from corrosion, but the Ni plating layer corrodes during substitution gold plating, forming pinholes that deteriorate wire bondability

Engineering Contradiction:
Improveprotection of primer layerVSAvoidnickel corrosion and pinhole formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

An intermediate layer based on a Pd-P alloy is introduced between the Ni-based lower layer and the Au-based upper layer. This intermediate layer acts as a mediator that prevents direct contact between the Ni layer and the substitution gold plating solution, thereby preventing Ni corrosion and pinhole formation while allowing the Au layer to maintain excellent wire bondability.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Reliability

If a thick reduced gold plating layer (0.2-0.7 μm) is formed to close pinholes, then wire bondability is improved, but manufacturing cost increases significantly

Engineering Contradiction:
Improvewire bondabilityVSAvoidmanufacturing cost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The Pd-P alloy intermediate layer eliminates the need for thick reduced gold plating by preventing pinhole formation at the source. This allows the use of a thin Au layer (0.05-0.2 μm) that provides excellent wire bondability without the high cost associated with thick gold plating.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Ease of manufacture

If only a thin substituted gold plating layer (0.1 μm or less) is formed to reduce cost, then manufacturing cost decreases, but the layer has many pinholes and poor bonding reliability

Engineering Contradiction:
Improvemanufacturing costVSAvoidbonding reliability
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The Pd-P alloy intermediate layer provides a dense, pinhole-free barrier that enables the use of a thin Au layer (0.05-0.2 μm) while maintaining high bonding reliability. The intermediate layer compensates for the thinness of the Au layer by providing the necessary protective and bonding functions.

Inventive Principle:
Principle #24Intermediary (Mediator)

4Stability of the object's composition

If a Pd layer is formed between Ni and Au to prevent Ni diffusion, then Ni diffusion is suppressed, but Pd diffuses to the Au layer during soldering, deteriorating wire bondability

Engineering Contradiction:
Improveprevention of Ni diffusionVSAvoidwire bondability
Core Design Contradiction:
Stability of the object's compositionVSReliability

Solution Approach 1:

Phosphorus is added to the Pd layer to form a Pd-P alloy with specific composition (3-12 mass% P). This compositional change fundamentally alters the diffusion behavior during soldering, preventing Pd from diffusing to the Au layer while maintaining Ni diffusion barrier functionality. The P content is carefully controlled to achieve this balance.

Inventive Principle:
Principle #35Parameter changes

5Productivity

If high-density wire bonding is performed with gold wires of 100 μm or less thickness, then mounting density is improved, but wire bondability deteriorates due to Ni corrosion and Pd diffusion

Engineering Contradiction:
Improvemounting densityVSAvoidwire bondability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The Pd-P alloy intermediate layer provides a stable, pinhole-free barrier that ensures excellent wire bondability for high-density mounting applications. It prevents both Ni corrosion and Pd diffusion, creating an ideal surface for ultrasonic wire bonding of fine gold wires (100 μm or less thickness).

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This configuration enhances the bonding strength and reliability of the ceramic substrate parts by suppressing nickel corrosion and palladium diffusion, resulting in improved wire bondability and solder wettability, even under high-temperature conditions.

Implementation Method 1

an intermediate layer based on a Pd-P alloy between a Ni-based lower layer and an Au-based upper layer

Methodology Applied
Scientific EffectDiffusion barrier: Diffusion Barrier

Implementation Method 2

the diffusion of Pd to an uppermost Au layer is suppressed

Methodology Applied
Scientific EffectDiffusion suppression: Diffusion Barrier

Implementation Method 3

the nickel plating layer acts as a barrier layer for protecting the primer layer from a solder

Methodology Applied
Scientific EffectBarrier layer protection: Diffusion Barrier

Implementation Method 4

the strength of bonding between gold wires and a gold plating layer, which is achieved by mutual diffusion with ultrasonic vibration

Methodology Applied
Scientific EffectMutual diffusion: Diffusion

Implementation Method 5

gold wires as thick as 100 μm or less are connected to the wire-bonding electrodes of a heated ceramic substrate part with ultrasonic vibration

Methodology Applied
Scientific EffectUltrasonic vibration: Ultrasonic Vibration

Implementation Method 6

Pd is thermally diffused to the Au layer while soldering devices such as inductors, etc. to mounting electrodes before the wire bonding of semiconductor devices

Methodology Applied
Scientific EffectThermal diffusion: Diffusion

Data Source

PatentEP2073261B1Ceramic substrate component and electronic component using the same
Publication Date: 2012.06.27 PROTERIAL LTD
  • EP2073261B1 patent drawingFigure 1~3
  • EP2073261B1 patent drawingFigure 4~5
  • EP2073261B1 patent drawingFigure 6~7

AI summary

A ceramic substrate part comprising on its upper surface pluralities of external electrodes comprising wire-bonding electrodes, each of which comprises a primer layer based on Ag or Cu, a Ni-based lower layer, an intermediate layer based on a Pd-P alloy containing 0.4-5% by mass of P, and a Au-based upper layer formed in this order on a ceramic substrate, the upper layer containing Pd after heated by soldering, and having a Au concentration of 80 atomic % or more based on the total concentration (100 atomic %) ofAu and Pd.