Layered Pentasil Zeolite Catalyst for Propylene Selectivity

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Solution Overview

Problem

Current zeolite catalysts used in the methanol to olefins (MTO) process are highly selective to ethylene and propylene but deactivate quickly due to coke formation, requiring frequent recycling and inefficiently producing a mix of hydrocarbon products.

Innovation Solution

A new family of layered pentasil zeolites with specific x-ray diffraction patterns and empirical compositions is developed, featuring a 2-dimensional crystal structure and high surface area, which acts as a catalyst for converting oxygenates to olefins, optimizing the production of propylene and reducing ethylene formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional zeolite catalysts are used for methanol to olefins conversion, then ethylene and propylene selectivity is achieved, but catalyst deactivation due to coke formation occurs quickly

Engineering Contradiction:
Improvecatalyst lifeVSAvoidolefin production efficiency
Core Design Contradiction:
ReliabilityVSProductivity

Solution Approach 1:

The patent modifies the zeolite catalyst by changing compositional parameters (incorporating gallium, iron, boron, indium or other trivalent elements in specific amounts) and structural parameters (controlling Si/Al ratio, pore size distribution, and crystal morphology) to reduce coke formation and extend catalyst life while maintaining olefin production efficiency

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite zeolite catalyst by combining multiple elements (aluminum, silicon, gallium/iron/boron/indium, and alkali metals) in specific ratios within the zeolite framework to achieve both high selectivity and reduced deactivation

Inventive Principle:
Principle #40Composite materials

2Productivity

If conventional zeolite catalysts are used, then a mix of hydrocarbon products is produced, but downstream separation complexities increase

Engineering Contradiction:
Improveproduct distributionVSAvoiddownstream separation process
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent optimizes the local catalytic properties of the zeolite catalyst by controlling the distribution and concentration of specific elements (gallium, iron, boron, indium) within the zeolite structure to enhance propylene selectivity and reduce ethylene formation, thereby simplifying downstream separation

Inventive Principle:
Principle #3Local quality

3Reliability

If conventional zeolite catalysts are used, then frequent recycling is required, but process efficiency decreases

Engineering Contradiction:
Improvecatalyst stabilityVSAvoidprocess energy efficiency
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The patent changes the chemical composition parameters of the catalyst by incorporating trivalent elements (gallium, iron, boron, indium) and controlling alkali metal content to improve catalyst stability and reduce frequent recycling, thereby lowering energy losses associated with recycling operations

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The new zeolite catalyst exhibits high propylene selectivity (47-52%) and low ethylene selectivity (3-6%), extending catalyst life and improving the yield of heavier olefins, thus enhancing the economic viability of the methanol to olefins process by reducing downstream separation complexities.

Implementation Method 1

a catalyst having an layered pentasil zeolite... to generate a process stream comprising olefins

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentUS9688587B2Process for oxygenate to olefin conversion using 2-D pentasil zeolite
Publication Date: 2017.06.27 UOP LLC

AI summary

A process for the conversion of oxygenates to olefins is presented. The process utilizes a catalyst having a 2-dimensional morphology, and the catalyst is a pentasil zeolite. The process is an oxygenate to olefins conversion under typical temperatures and pressures, but provides for an increased propylene yield and a reduced ethylene yield.