Perfume Particle Preparation Process for High Activity and Flowability

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Solution Overview

Problem

Current perfume production processes struggle to meet increasing demand for high scent laundry detergents without significant capital investment, resulting in perfume particles with poor powder characteristics and flowability, especially in hot climates.

Innovation Solution

A process involving contacting a perfume ingredient with a molten material to form a pre-mix, then with solid materials to create a hardened-solid intermediate, followed by further processing to produce a perfume composition with a high perfume ingredient ratio, enhancing storage stability and flowability without requiring extensive equipment modifications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If perfume activity in perfume particles is increased to meet consumer demand for high scent laundry detergents, then perfume performance is improved, but powder characteristics and flowability deteriorate, especially in hot climates

Engineering Contradiction:
Improveperfume activityVSAvoidflowability
Core Design Contradiction:
Quantity of substanceVSEase of operation

Solution Approach 1:

The patent applies parameter changes by controlling the water content of the perfume particles within a specific range (0.5-5% w/w) and adjusting processing temperatures. By optimizing these parameters, the invention achieves high perfume activity while maintaining good powder characteristics and flowability, even in hot climates where temperatures exceed 30°C.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite materials by combining perfume ingredients with carrier materials to create perfume particles with optimized properties. The composite structure allows high perfume loading while maintaining desirable powder characteristics including flowability and stability in various environmental conditions.

Inventive Principle:
Principle #40Composite materials

2Productivity

If production capacity is increased to meet rising consumer demand, then productivity is improved, but capital cost and equipment complexity increase significantly

Engineering Contradiction:
Improveproduction capacityVSAvoidequipment complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The patent applies universality by designing a multi-functional processing system that can handle multiple perfume formulations and production volumes using the same equipment. The process can be applied to existing perfume manufacturing equipment, allowing increased production capacity without requiring entirely new specialized equipment for each function.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The invention increases production capacity through parameter changes in the processing conditions, such as temperature, residence time, and material ratios, rather than through equipment expansion. This allows existing equipment to operate at higher capacities while maintaining product quality.

Inventive Principle:
Principle #35Parameter changes

3Quantity of substance

If perfume particles are produced with high perfume ingredient content, then perfume performance is improved, but storage stability deteriorates and refrigerated transport becomes necessary

Engineering Contradiction:
Improveperfume ingredient contentVSAvoidstorage stability
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent achieves storage stability with high perfume ingredient content (greater than 10% w/w, preferably greater than 20% w/w) by controlling the water content parameter within 0.5-5% w/w and optimizing the perfume-to-carrier ratio. These parameter changes prevent degradation while maintaining high perfume activity without requiring refrigerated storage or transport.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses stable carrier materials that provide a protective matrix for the perfume ingredients, allowing high perfume content to be maintained in a stable form that does not require expensive refrigerated storage infrastructure.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Increases production capacity, ensures storage stability, and maintains good powder characteristics and flowability, making the perfume suitable for various applications, including laundry detergents, without the need for refrigerated transport or storage.

Implementation Method 1

contacting a perfume ingredient with a molten material to form a pre-mix; contacting the pre-mix with a first solid material to form a soft-solid intermediate high active perfume material; solidifying the molten material to form a hardened-solid intermediate high active perfume material

Methodology Applied
Scientific EffectPhase change: Phase Change

Data Source

PatentEP2451928B1A process for preparing a perfume particle
Publication Date: 2015.09.09 PROCTER & GAMBLE CO

AI summary

The present invention relates to a process for preparing a perfume composition, the process comprising the steps of; (a) contacting a perfume ingredient with a molten material to form a pre-mix; (b) contacting the pre-mix with a first solid material to form a soft-solid intermediate high active perfume material; (c) solidifying the molten material to form a hardened-solid intermediate high active perfume material; (d) contacting the hardened-solid intermediate high active perfume intermediate material with a second solid material to form a perfume composition, wherein the ratio of the wt% amount of perfume ingredient present in the hardened-solid intermediate high active perfume material to the wt% amount of perfume ingredient present in the perfume composition is greater than 1.5:1.