Perovskite Lanthanide Catalysts for Oxidative Coupling of Methane

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current catalysts and catalytic processes for oxidative coupling of methane (OCM) and oxidative dehydrogenation (ODH) lack effectiveness, leading to inefficiencies in methane conversion and ethylene selectivity, hindering the commercialization of these reactions.

Innovation Solution

Development of catalytic materials comprising perovskites and lanthanide-based catalysts with specific formulas, combined with diluents or supports, which enhance methane conversion and C2 selectivity, and are designed for use in oxidative coupling reactions at specific temperatures and linear velocities.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If conventional catalysts are used for oxidative coupling of methane, then the reaction can proceed, but methane conversion rate is low and C2 selectivity is poor

Engineering Contradiction:
Improvemethane conversion rateVSAvoidC2 selectivity
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent employs composite catalyst materials comprising multiple components: transition metal oxides (Fe, Co, Ni, Cu, Mn, Zn), alkaline earth metal oxides (Ca, Sr, Ba), and lanthanide oxides (La, Ce, Pr, Nd, Gd, Dy, Ho, Er, Tm, Lu). These composite materials create synergistic effects where different components contribute to specific catalytic functions, achieving both high methane conversion and superior C2 selectivity simultaneously

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The catalyst formulation uses specific ratios of different metal oxides and supports (alumina, silica, titania, zirconia, hafnia) to create localized active sites with optimized properties. The support materials provide structural framework while the metal oxides create active catalytic centers with specific electronic and geometric properties tailored for OCM reaction

Inventive Principle:
Principle #3Local quality

2Productivity

If high temperatures are used for oxidative coupling of methane, then reaction rate increases, but energy consumption increases and unwanted side reactions occur

Engineering Contradiction:
Improvereaction rateVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The patent modifies the catalytic parameters by introducing multiple metal oxides with different activation energies and reaction pathways. This creates a distribution of active sites that can operate at different temperature ranges, allowing the reaction to proceed at lower temperatures while maintaining high rates through the combined effect of multiple catalytic mechanisms

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The composite catalyst system provides continuous catalytic activity through multiple active sites that operate simultaneously at different temperature zones. The heat generated by exothermic reactions at certain sites can be utilized by other sites, creating a self-sustaining thermal field that maintains high reaction rates without requiring continuously high external temperature

Inventive Principle:
Principle #20Continuity of useful action

3Productivity

If catalyst load is increased to improve conversion, then productivity increases, but cost and complexity increase

Engineering Contradiction:
Improvemethane conversionVSAvoidcatalyst formulation complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The support materials (alumina, silica, titania, zirconia, hafnia) serve multiple functions simultaneously: they provide structural support, thermal stability, mass transfer pathways, and additional catalytic activity. The metal oxides also perform multiple functions including methane activation, C-C bond formation, and product selective desorption, reducing the need for separate functional components

Inventive Principle:
Principle #6Universality (Multi-functionality)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed catalytic materials achieve methane conversion rates greater than 20% and C2 selectivity greater than 50% in the oxidative coupling of methane, improving reaction efficiency and stability at temperatures ranging from 550°C to 750°C.

Implementation Method 1

Catalysis is the process in which the rate of a chemical reaction is either increased or decreased by means of a catalyst. Positive catalysts lower the rate-limiting free energy change to the transition state, and thus increase the speed of a chemical reaction at a given temperature.

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

the catalytic reaction generally occurs on the surface of the heterogeneous catalyst. Thus, for the catalytic reaction to occur, the reactants must diffuse to and/or adsorb onto the catalyst surface.

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

This reaction is exothermic (ΔH = -67kcals/mole)

Methodology Applied
Scientific EffectExothermic reaction: Exothermic Reaction

Data Source

PatentEP3825001A1Catalysts for natural gas processes
Publication Date: 2021.05.26 LUMMUS TECHNOLOGY INC
  • EP3825001A1 patent drawingFigure 1~2A
  • EP3825001A1 patent drawingFigure 2B~2D
  • EP3825001A1 patent drawingFigure 2E~2F

AI summary

Catalysts, catalytic forms and formulations, and catalytic methods are provided. The catalysts and catalytic forms and formulations are useful in a variety of catalytic reactions, for example, the oxidative coupling of methane. Related methods for use and manufacture of the same are also disclosed.