PET Bottle Headspace Pressure Control via Liquid Nitrogen Phase Change

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Solution Overview

Problem

Existing methods for maintaining internal pressure in beverage containers, particularly PET bottles, are prone to variability due to factors like temperature changes and volume fluctuations, leading to inconsistent pressures that can result in container bursting or contamination, and are limited to cylindrical geometries.

Innovation Solution

A method and device for filling and sealing thin-walled plastic containers that involves introducing an exchange medium, such as liquid nitrogen, into the headspace to displace air and set a predetermined internal pressure by adjusting the gaseous medium supply or discharge through openings in the container walls, allowing for precise control of internal pressure and adaptation to handling and storage conditions.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If liquid nitrogen is introduced into the headspace to displace air, then the container internal pressure increases, but the pressure becomes difficult to control and may cause container bursting

Engineering Contradiction:
Improvecontainer pressure controlVSAvoidpressure setting precision
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent introduces a multi-stage pressurization process where the container is pressurized in steps rather than all at once. The system monitors pressure continuously and adjusts the nitrogen flow rate dynamically, changing parameters like flow rate and pressure thresholds to achieve precise control. This resolves the contradiction by transforming a single uncontrolled pressure increase into a controlled multi-stage process.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent employs a feedback control system with pressure sensors that continuously monitor the container internal pressure and adjust the nitrogen supply accordingly. The control unit receives pressure signals and modulates the flow valve to maintain pressure within desired limits, preventing both under-pressurization and over-pressurization that could lead to bursting.

Inventive Principle:
Principle #23Feedback

2Object-affected harmful factors

If the container internal pressure is increased to prevent contamination, then the sealing requirement increases, but thin-walled containers may deform or burst

Engineering Contradiction:
Improvecontamination protectionVSAvoidcontainer structural integrity
Core Design Contradiction:
Object-affected harmful factorsVSStrength

Solution Approach 1:

The patent applies partial pressurization rather than extreme over-pressurization. By introducing nitrogen gradually and maintaining pressure within a specific range (slightly above atmospheric pressure), the system achieves contamination protection without subjecting thin-walled containers to excessive stresses that would cause deformation or bursting.

Inventive Principle:
Principle #16Partial or excessive action

Solution Approach 2:

The patent pre-cools the container and filling material before introduction of liquid nitrogen, and establishes a controlled pressurization protocol that prevents sudden pressure spikes. This cushioning approach prepares the system to handle the phase change of nitrogen without causing thermal or mechanical shock to the thin-walled container structure.

Inventive Principle:
Principle #11Beforehand cushioning (Prior cushioning)

3Reliability

If liquid nitrogen is used for headspace pressurization, then air displacement is effective, but volume fluctuations and temperature changes cause pressure instability

Engineering Contradiction:
Improveheadspace protectionVSAvoidinternal pressure stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The patent implements continuous pressure monitoring with feedback control that automatically adjusts nitrogen flow to compensate for volume fluctuations and temperature changes. The control system detects pressure deviations caused by these variables and modulates the supply rate accordingly, maintaining stable internal pressure throughout the storage period.

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The patent maintains continuous nitrogen flow adjustment rather than single-stage pressurization. The system continuously monitors pressure and adjusts the nitrogen supply rate to account for ongoing temperature changes and volume fluctuations, ensuring stable headspace protection throughout the storage period.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach ensures consistent internal pressure, preventing container bursting and contamination, while accommodating various container geometries, ensuring safe transport and stackability, and maintaining pressure above ambient levels even after cooling.

Implementation Method 1

the enormous volume expansion of liquid nitrogen during its transition into the gas phase when it comes into contact with the filling material

Methodology Applied
Scientific EffectPhase change: Phase Change

Implementation Method 2

the enormous volume expansion of liquid nitrogen during its transition into the gas phase

Methodology Applied
Scientific EffectThermal expansion: Thermal Expansion

Implementation Method 3

a predetermined container internal pressure is adjusted by supplying and/or discharging a gaseous medium

Methodology Applied
Scientific EffectPressure adjustment: Pressure Increase

Data Source

PatentEP3702319B1Device and method for guaranteeing a container interior pressure through multiple pressurization of the headspace
Publication Date: 2021.12.08 KRONES AG
  • EP3702319B1 patent drawingFigure 1
  • EP3702319B1 patent drawingFigure 2

AI summary

The invention relates to a device and a method for filling and closing a thin-walled plastic container (11), in particular a PET bottle, wherein a plastic container is produced from a preform by a blow molding process, and the plastic container is filled with a flowable medium and in particular a liquid, and an exchange medium is introduced into the plastic container, whereby, with the formation of an increased internal pressure of the container, at least partial displacement of the previously contained medium takes place and the plastic container is at least partially closed, wherein in at least one section of a wall of the plastic container surrounding a headspace of the plastic container,at least one opening is provided in a wall of the container closure or between a wall of the plastic container and a wall of the container closure, and a predetermined internal pressure is set through this opening in the interior of the plastic container by supplying and/or removing a gaseous medium.