Pharmaceutical Wastewater Treatment with Calcium Silicate Buffering

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Solution Overview

Problem

Current pharmaceutical wastewater treatment processes face challenges such as low pH values affecting methane production, inefficient conversion of particulate pollutants, low biogas production, slow granular sludge formation, and high energy consumption, leading to unstable operations and low carbon resource recovery.

Innovation Solution

A device comprising a floatation tank, pH adjusting tank, enhanced hydrolysis acidification tank, methanogenic tank, anoxic pool, aerobic pool, and sedimentation tanks, along with specific fillers and additives like micron calcium silicate, which adjusts pH, enhances acid production, and supports granular sludge formation, improving methane production and carbon resource recovery.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If hydrolytic acidification is used to remove refractory pollutants, then organic matter removal is improved, but pH value decreases affecting subsequent methane production

Engineering Contradiction:
Improveorganic matter removal efficiencyVSAvoidmethane production stability
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The patent introduces a buffering substance (such as calcium carbonate or sodium hydroxide) as an intermediary to neutralize the acid produced during hydrolytic acidification. This mediator maintains the pH within an optimal range for subsequent methane production while preserving the organic matter removal efficiency of the acidification process.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The patent adjusts the pH parameter by controlling the dosage of buffering substances and optimizing the hydraulic retention time in the hydrolytic acidification reactor. This parameter adjustment ensures that the effluent pH remains suitable for methane production while maintaining high organic matter removal efficiency.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If hydraulic retention time is shortened to increase productivity, then treatment capacity is improved, but conversion of particulate pollutants to dissolved organic matter is insufficient

Engineering Contradiction:
Improvetreatment capacityVSAvoidpollutant conversion efficiency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent divides the treatment process into distinct stages: a hydrolytic acidification stage for converting particulate pollutants, followed by a methane production stage. This segmentation allows each stage to be optimized independently - the hydrolysis stage ensures adequate conversion time while the overall system maintains high treatment capacity through controlled loading rates.

Inventive Principle:
Principle #1Segmentation

3Reliability

If physical and chemical methods are used for deep treatment, then treatment effect is improved, but operating costs and energy consumption increase

Engineering Contradiction:
Improvetreatment effectVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by stationary object

Solution Approach 1:

The patent replaces energy-intensive physical and chemical treatment methods with a biological treatment system. The anaerobic digestion process uses microorganisms to degrade organic pollutants, eliminating the need for high-energy operations such as evaporation, advanced oxidation, or membrane filtration, while achieving comparable or superior treatment effects.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

4Ease of operation

If conventional anaerobic treatment is used, then operation management is simplified, but biogas production per unit volume is low and granular sludge formation is slow

Engineering Contradiction:
Improveoperation management convenienceVSAvoidbiogas production efficiency
Core Design Contradiction:
Ease of operationVSProductivity

Solution Approach 1:

The patent creates conditions for self-organizing granular sludge formation by optimizing the anaerobic reactor environment - including controlled mixing, appropriate loading rates, and nutrient balance. The granular sludge forms spontaneously through microbial self-organization, eliminating the need for external intervention while significantly enhancing biogas production efficiency and simplifying operation management.

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution stabilizes the treatment process, increases carbon resource recovery efficiency, reduces energy consumption, and simplifies operation, achieving efficient and stable pharmaceutical wastewater treatment.

Implementation Method 1

a floatation tank; a decontamination device is disposed in the floatation tank

Methodology Applied
Scientific EffectFlotation: Froth Floatation

Implementation Method 2

a pH adjusting tank; the acid tank and the base tank are independently connected to the pH adjusting tank

Methodology Applied
Scientific EffectpH adjustment:

Implementation Method 3

an enhanced hydrolysis acidification tank... so that the organic matter in the influent is mostly removed

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 4

hydrolytic acidification/methane production, so that the organic matter in the influent is mostly removed

Methodology Applied
Scientific EffectAcidification:

Implementation Method 5

a methanogenic tank... there is often a lower pH value of effluent, affecting the subsequent methane production

Methodology Applied
Scientific EffectAnaerobic digestion: Anaerobic Digestion

Implementation Method 6

hydrolytic acidification/methane production, so that the organic matter in the influent is mostly removed

Methodology Applied
Scientific EffectMethanogenesis: Electromethanogenesis

Implementation Method 7

the organic matter and total nitrogen in the anoxic + aerobic section are removed

Methodology Applied
Scientific EffectDenitrification:

Implementation Method 8

the organic matter and total nitrogen in the anoxic + aerobic section are removed

Methodology Applied
Scientific EffectAerobic degradation: Aerobic Digestion

Implementation Method 9

a secondary sedimentation tank

Methodology Applied
Scientific EffectSedimentation: Sedimentation

Implementation Method 10

a coagulation sedimentation tank

Methodology Applied
Scientific EffectCoagulation: Coagulation

Data Source

PatentEP3611135B1Device and method for pharmaceutical wastewater treatment with high efficiency resource recovery and low energy consumption
Publication Date: 2021.06.16 NANJING UNIV
  • EP3611135B1 patent drawingFigure 1
  • EP3611135B1 patent drawingFigure 2
  • EP3611135B1 patent drawingFigure 3

AI summary

A device for pharmaceutical wastewater treatment with high efficiency resource recovery and low energy consumption, the device including: a floatation tank; a pH adjusting tank; an acid tank; a base tank; an enhanced hydrolysis acidification tank; a micron calcium silicate tank; a methanogenic tank; an anoxic pool; an aerobic pool; a biogas collection and treatment device; a secondary sedimentation tank; a coagulation sedimentation tank; a polyaluminium chloride (PAC) tank; a control device; and a power supply. The floatation tank, the pH adjusting tank, the enhanced hydrolysis acidification tank, the methanogenic tank, the anoxic pool, the aerobic pool, the secondary sedimentation tank and the coagulation sedimentation tank are connected sequentially. A decontamination device is disposed in the floatation tank. The acid tank and the base tank are independently connected to the pH adjusting tank, and joints thereof are provided with magnetic valves, respectively.