Phase-Inverted Porous Electrodes Without Support Structures

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Solution Overview

Problem

Existing porous electrodes for water electrolysis are brittle, have high internal electrical resistance due to large pores, and require additional supportive structures, making them costly and less efficient.

Innovation Solution

A method for producing self-standing porous electrodes comprising a polymeric binder material and electrochemically active particles, achieved by preparing a slurry, shaping it into a green body, and subjecting it to phase inversion, which eliminates the need for additional supportive structures and reduces complexity and cost.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of moving object

If porous electrodes are produced using conventional methods with large pores, then porosity is improved for mass transport, but internal electrical resistance increases and mechanical strength decreases

Engineering Contradiction:
Improvepore sizeVSAvoidelectrical resistance
Core Design Contradiction:
Length of moving objectVSReliability

Solution Approach 1:

The patent employs porous silicon particles as the electrochemically active material, creating an intrinsically porous structure that provides both high porosity for mass transport and sufficient mechanical strength. The porous structure eliminates the need for additional supportive compounds while maintaining electrical conductivity and structural integrity during electrolysis operations.

Inventive Principle:
Principle #31Porous materials

2Length of moving object

If porous electrodes are produced using conventional methods, then porosity is improved, but additional supportive structures are required increasing device complexity

Engineering Contradiction:
Improvepore sizeVSAvoidsupportive structures
Core Design Contradiction:
Length of moving objectVSDevice complexity

Solution Approach 1:

The porous silicon particles serve as both the electrochemically active material and the structural support simultaneously. The particles' inherent porosity and mechanical strength eliminate the need for separate supportive compounds or structures, simplifying the electrode design and reducing device complexity while maintaining functionality.

Inventive Principle:
Principle #25Self-service

3Length of moving object

If porous electrodes are produced using conventional methods with large pores, then porosity is improved, but mechanical strength decreases making electrodes brittle

Engineering Contradiction:
Improvepore sizeVSAvoidmechanical strength
Core Design Contradiction:
Length of moving objectVSStrength

Solution Approach 1:

The use of porous silicon particles with controlled pore structures provides both the necessary porosity for mass transport and sufficient mechanical strength to prevent brittleness. The porous structure is optimized to maintain structural integrity while enabling efficient electrolyte penetration and gas transport during operation.

Inventive Principle:
Principle #31Porous materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting porous electrodes are flexible, have improved electrochemical performance and efficiency, and exhibit enhanced mass transport and ionic diffusion, leading to increased durability and reduced production costs.

Implementation Method 1

shaping it into a green body, and subjecting it to phase inversion

Methodology Applied
Scientific EffectPhase inversion: Phase Change

Data Source

PatentEP4570951A1Method for producing a porous electrode
Publication Date: 2025.06.18 VLAAMSE INSTELLING VOOR TECHNOLOGISCH ONDERZOEK NV (VITO)
  • EP4570951A1 patent drawingFigure 1~2
  • EP4570951A1 patent drawingFigure 3~4
  • EP4570951A1 patent drawingFigure 5~7

AI summary

The present invention relates to a method (1) for producing a porous electrode comprising: preparing (2) a slurry comprising a solvent, between 1 % and 25 % by weight of a polymeric binder material and between 10 % and 80 % by weight of particles comprising an electrochemically active material, based on the total weight of the slurry, wherein the polymeric binder material is at least partially dissolved in the solvent; shaping (3) the slurry, thereby obtaining a green body; subjecting the green body to phase inversion (4), thereby forming the porous electrode, which comprises a porous matrix and the particles comprising the electrochemically active material, wherein the porous matrix comprises the polymeric binder material; wherein the weight ratio of the polymeric binder material to the particles in the slurry is between 2:98 and 50:50, and a total amount of the polymeric binder material and the particles in the slurry is between 32 % and 80 % by weight, based on the total weight of the slurry. The invention further relates to a porous electrode comprising a porous matrix comprising a polymeric binder material, and particles comprising an electrochemically active material.