Methanol-Free Phenolic Resole Ink for Non-Porous Substrates

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Solution Overview

Problem

Continuous inkjet ink compositions pose safety concerns due to the presence of harmful chemicals like methanol, halogens, and bisphenol A, which are toxic and carcinogenic, and existing formulations do not adequately address the need for safe and reliable printing on non-porous substrates.

Innovation Solution

The development of ink compositions that are free or substantially free of methanol, halogens, halogenated compounds, and bisphenol A, using phenolic resole resins with less than 0.1% free formaldehyde, combined with organic solvents and colorants, to ensure safe and effective printing on various substrates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If phenolic resins with 0.3% or greater free formaldehyde are used to achieve good adhesion to non-porous substrates, then adhesion performance is improved, but health safety deteriorates due to carcinogenic classification

Engineering Contradiction:
Improveadhesion to non-porous substratesVSAvoidfree formaldehyde content
Core Design Contradiction:
StrengthVSObject-affected harmful factors

Solution Approach 1:

The patent changes the critical parameter of free formaldehyde content from 0.3% or greater to less than 0.3%, thereby reclassifying the phenolic resin from Category 1B carcinogen to a safer classification while maintaining adhesion performance through optimized resin formulation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent uses composite binder resin systems combining phenolic resins with other resin types (such as polyurethane, acrylic, or epoxy resins) to achieve the required adhesion to non-porous substrates without relying solely on high formaldehyde-content phenolic resins

Inventive Principle:
Principle #40Composite materials

2Loss of time

If methanol is used as the main solvent to achieve fast-dry time and good adhesion, then drying speed is improved, but health safety deteriorates due to toxic inhalation risks

Engineering Contradiction:
Improvedrying timeVSAvoidmethanol toxicity
Core Design Contradiction:
Loss of timeVSObject-affected harmful factors

Solution Approach 1:

The patent extracts and removes methanol from the ink composition entirely, replacing it with alternative solvents such as water, alcohols (ethanol, isopropanol), or glycol ethers that provide comparable drying characteristics without the severe toxic inhalation risks of methanol

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the solvent composition parameters by reducing methanol content to less than 5% by weight (preferably less than 1% or completely eliminated) and adjusting the proportions of alternative solvents to maintain fast-dry performance

Inventive Principle:
Principle #35Parameter changes

3Reliability

If halogenated compounds are included in binder resins and conductive agents to achieve desired performance, then functional performance is improved, but health safety deteriorates due to extreme toxicity of gaseous halogens

Engineering Contradiction:
Improvefunctional performanceVSAvoidhalogen toxicity
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The patent extracts and removes halogenated compounds from the ink composition, specifically eliminating substances containing fluorine, chlorine, bromine, or iodine from binder resins, conductive agents, and other additives, replacing them with non-halogenated alternatives that provide equivalent functional performance

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent changes the chemical composition parameters by specifying that the ink contains less than 50 ppm (preferably less than 1 ppm or completely eliminated) of halogenated compounds, thereby eliminating the source of toxic gaseous halogens

Inventive Principle:
Principle #35Parameter changes

4Stability of the object's composition

If bisphenol A is present in phenolic resins to achieve resin stability and performance, then resin performance is improved, but health safety deteriorates due to reproductive toxin classification

Engineering Contradiction:
Improveresin stabilityVSAvoidbisphenol A content
Core Design Contradiction:
Stability of the object's compositionVSObject-affected harmful factors

Solution Approach 1:

The patent changes the parameter of bisphenol A content by specifying that the ink contains less than 50 ppm (preferably less than 1 ppm or completely eliminated) of this reproductive toxin, achieving resin stability through alternative phenolic resin formulations without BPA

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The ink compositions provide superior health and safety profiles, ensuring reliable adhesion and drying times while avoiding the use of hazardous substances, making them suitable for industrial applications in continuous inkjet printing.

Implementation Method 1

Resole type phenolic resins undergo cross-link reactions at elevated temperatures and display good adhesion to non-porous substrates such as glass, polymer films, aluminum and steel

Methodology Applied
Scientific EffectCross-link reactions: Chemical Bonding

Implementation Method 2

Some commercial thermo-curable continuous inkjet inks use methanol as the solvent or the main solvent because such inks produce a fast-dry time due to their volatility

Methodology Applied
Scientific EffectEvaporation: Evaporation

Data Source

PatentUS11208569B2Continuous inkjet ink composition
Publication Date: 2021.12.28 VIDEOJET TECH INC

AI summary

Embodiments of the invention relate to ink compositions suitable for applications in the printing industry, for example continuous inkjet printing, including ultra-high speed continuous inkjet printing. The ink compositions use volatile organic solvents, a colorant, and one or more binder resins including a resin that is a phenolic resole resin, wherein the ink composition is free of methanol, halogens, halogenated compounds and bisphenol-A. A phenolic resole resin of the ink composition preferably contains less than 0.1% by weight of free formaldehyde. The one or more binder resins including the phenolic resole resin may be present in an amount that is from about 5% to about 30% by weight of the ink composition.