Phosphonic Acid Degreasing Solution for Galvanizing Bath Stability

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Solution Overview

Problem

Hot-dip galvanizing baths experience reduced service life due to increasing salt concentration from metal degreasing processes, leading to instability and environmental impact, as existing acidic solutions fail to maintain effective degreasing over time.

Innovation Solution

A degreasing solution containing phosphonic acid or its derivatives is used to adjust salt concentration by forming precipitates, maintaining the degreasing effect and extending bath service life, with optimal concentrations of 0.0001 to 50% phosphonic acid and pH less than 4.0, combined with surfactants and additional acids.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of stationary object

If acidic solutions (hydrochloric acid or phosphoric acid) are used to degrease metal surfaces, then the service life of baths is extended, but the salt concentration increases leading to reduced bath stability

Engineering Contradiction:
Improveservice life of bathVSAvoidbath stability
Core Design Contradiction:
Duration of action of stationary objectVSStability of the object's composition

Solution Approach 1:

The invention converts the harmful effect of increasing salt concentration into a beneficial process by adding phosphonic acid to precipitate excess metal salts. The salt concentration that would normally degrade bath stability is instead used to form precipitates that can be removed, thereby extending bath service life while maintaining stability.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The invention changes the chemical parameters of the degreasing bath by introducing phosphonic acid, which alters the precipitation behavior of metal salts. This parameter change allows for controlled salt removal through precipitate formation, enabling extended bath life without compromising stability.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If degreasing is performed repeatedly, then productivity increases, but salt concentration accumulates reducing further degreasing effectiveness

Engineering Contradiction:
Improvedegreasing throughputVSAvoiddegreasing effectiveness
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention enables continuous degreasing operations by maintaining bath effectiveness through phosphonic acid addition. The phosphonic acid continuously precipitates accumulating salts, ensuring that the degreasing action remains effective throughout extended operation periods, thus supporting continuous productivity without effectiveness loss.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The invention facilitates the removal (discarding) of accumulated salt precipitates from the degreasing bath, allowing the useful degreasing action to continue. By periodically removing precipitates, the bath maintains its effectiveness for prolonged periods, enabling sustained high productivity.

Inventive Principle:
Principle #34Discarding and recovering

3Reliability

If surfactant concentration is increased to maintain degreasing effect, then degreasing performance improves, but environmental impact and waste disposal costs increase

Engineering Contradiction:
Improvedegreasing performanceVSAvoidenvironmental impact
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention changes the chemical composition by adding phosphonic acid, which alters the salt precipitation characteristics without requiring increases in surfactant concentration. This parameter change maintains degreasing performance while avoiding the environmental problems associated with high surfactant levels.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution significantly extends the service life of degreasing baths by binding excess iron and removing organic impurities, maintaining effective degreasing over a longer period while minimizing environmental impact and reducing waste disposal costs.

Implementation Method 1

the phosphonic acid and/or the phosphonic acid derivative allows the salt concentration of the solution to be adjusted such that the degreasing effect of the surfactant is maintained for a long time

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Implementation Method 2

The solution itself can be used as the bath or added to a solution in the bath during or after a degreasing process to adjust the salt concentration of the bath

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Data Source

PatentEP2671972B1Use of a solution containing phosphonic acid and/or phosphonic acid derivatives during the degreasing of metal surfaces, degreasing solution and method for degreasing a metal surface
Publication Date: 2021.05.05 STOCKMEIER CHEM GMBH & CO

AI summary

Use of phosphonic acid solution (S1) containing phosphonic acid and/or its derivative for degreasing metal surface e.g. iron or steel surface during hot-dip galvanizing process is claimed. Independent claims are included for the following: (1) degreasing solution used for degreasing metal surface, which contains phosphonic acid and/or its derivative, and a surfactant; (2) use of degreasing solution for degreasing metal surface; and (3) degreasing of metal surface.