Phosphorus-Sodium Catalyst for Selective Hydrodesulfurization

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Solution Overview

Problem

Current hydrotreating processes for gasoline cuts from fluidized-bed catalytic cracking units face challenges in reducing sulfur content without significantly lowering the octane number, as they often hydrogenate olefins, which is undesirable.

Innovation Solution

A catalyst comprising a group VIB element, a group VIII element, phosphorus, and an alumina support with specific sodium and phosphorus ratios, which enhances selectivity and activity in hydrodesulfurization, allowing for effective sulfur removal without substantial hydrogenation of olefins.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional hydrotreating catalysts are used to reduce sulfur content, then sulfur removal efficiency is improved, but octane number decreases due to olefin hydrogenation

Engineering Contradiction:
Improvesulfur content reductionVSAvoidoctane number
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The invention changes the chemical composition parameters of the catalyst by incorporating specific amounts of phosphorus (0.1-5% P2O5) and sodium (50-2000 ppm Na2O), and by optimizing the P/Na molar ratio (1.5-300). This modifies the catalyst's surface properties and electronic structure, enabling selective hydrodesulfurization while suppressing olefin hydrogenation, thus resolving the contradiction between sulfur removal efficiency and octane number preservation

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite catalyst system combining group VIB metal (molybdenum or tungsten), group VIII metal (cobalt or nickel), phosphorus, and sodium on an alumina support. This multi-component composite structure synergistically enhances hydrodesulfurization activity while improving selectivity against olefin hydrogenation, thereby achieving both high sulfur removal and octane preservation

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalyst improves hydrodesulfurization performance by maintaining high selectivity and activity, thereby reducing sulfur content in gasoline cuts while minimizing the loss of octane number, thus meeting stringent sulfur specifications.

Implementation Method 1

a process for the hydrodesulfurization of a sulfur-containing olefinic gasoline cut

Methodology Applied
Scientific EffectHydrodesulfurization: Chemical Bonding

Implementation Method 2

catalyst comprising at least one element from group VIB, at least one element from group VIII, phosphorus, sodium and a support comprising alumina

Methodology Applied
Scientific EffectCatalysis: Catalysis

Data Source

PatentUS20240216896A1Catalyst containing phosphorus and sodium and use thereof in a hydrodesulfurization process
Publication Date: 2024.07.04 IFP ENERGIES NOUVELLES

AI summary

Catalyst comprising an active phase based on at least one group VIB metal, at least one group VIII metal, phosphorus, sodium and an alumina-based support, the sodium content being between 50 and 2000 ppm by weight in the form of Na—O relative to the total weight of said catalyst, and the molar ratio of phosphorus to sodium being between 1.5 and 300.