Photoelectric Conversion Element Electron Blocking Layer

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Solution Overview

Problem

Photoelectric conversion elements face challenges in achieving high photoelectric conversion efficiency and fast responsivity while minimizing dark current, especially when subjected to heat treatment, due to limitations in charge transportability and heat resistance of existing materials.

Innovation Solution

A compound with a specific structure, where fused diarylamines are connected through a divalent linking group, enhancing heat resistance and charge transportability without impairing high-speed responsivity and low dark current characteristics, is used as an electron blocking layer to prevent charge injection and reduce dark current.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If a voltage is externally applied to improve photoelectric conversion efficiency or enhance response speed, then photoelectric conversion efficiency and response speed are improved, but dark current increases due to charge injection from electrode

Engineering Contradiction:
Improveresponse speedVSAvoiddark current
Core Design Contradiction:
SpeedVSObject-generated harmful factors

Solution Approach 1:

An electron blocking layer comprising a specific compound (formula 1) is introduced as an intermediary between the electrode and the photoelectric conversion layer. This layer has high ionization potential (5.0-6.0 eV) that prevents electron injection from the electrode into the photoelectric conversion layer, thereby blocking the harmful injected carriers that cause dark current while allowing the application of external voltage for improving photoelectric conversion efficiency and response speed

Inventive Principle:
Principle #24Intermediary (Mediator)

2Object-generated harmful factors

If conventional electron blocking materials are used to suppress charge injection, then dark current is reduced, but heat resistance deteriorates

Engineering Contradiction:
Improvedark currentVSAvoidheat resistance
Core Design Contradiction:
Object-generated harmful factorsVSTemperature

Solution Approach 1:

The invention changes the key parameter of ionization potential to a specific range (5.0-6.0 eV) and introduces a specific molecular structure (formula 1 with fused diarylamine and divalent linking group) that provides both the required electrical properties for electron blocking and sufficient thermal stability. This compound maintains low dark current while exhibiting adequate heat resistance for practical device operation

Inventive Principle:
Principle #35Parameter changes

3Power

If materials with high charge transportability are used to improve photoelectric conversion efficiency, then photoelectric conversion efficiency is improved, but dark current increases due to enhanced charge injection

Engineering Contradiction:
Improvephotoelectric conversion efficiencyVSAvoiddark current
Core Design Contradiction:
PowerVSObject-generated harmful factors

Solution Approach 1:

The electron blocking layer acts as a selective intermediary that exploits the energy level difference (high ionization potential of 5.0-6.0 eV) to allow efficient charge transport in the photoelectric conversion layer while preventing charge injection at the electrode interface. This enables high photoelectric conversion efficiency through good charge transport in the conversion layer without the penalty of increased dark current from electrode injection

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution effectively reduces dark current and maintains performance even under heat treatment, enabling high photoelectric conversion efficiency and fast responsivity in imaging devices.

Implementation Method 1

an energy gap between WF of the electrode and LUMO of the fullerene (C 60 ) becomes small, as a result, particularly an electron is liable to be injected from the electrode into the photoelectric conversion film and a significant increase of dark current is caused

Methodology Applied
Scientific EffectEnergy level mismatch blocking:

Implementation Method 2

photoelectric conversion sites are two-dimensionally arrayed in a semiconductor to form pixels and a signal generated by photoelectric conversion in each pixel

Methodology Applied
Scientific EffectPhotoelectric conversion: Photoelectric Effect

Data Source

PatentEP2439803B1Photoelectric conversion element and method for producing same, photosensor, imaging element and method of driving same
Publication Date: 2017.11.08 FUJIFILM CORP
  • EP2439803B1 patent drawingFigure 1(a)~2
  • EP2439803B1 patent drawingFigure 3~4
  • EP2439803B1 patent drawing

AI summary

To provide a photoelectric conversion element capable of functioning as a photoelectric conversion element when a compound having a specific structure is applied to the photoelectric conversion element, causing the element to exhibit a low dark current, and reducing the range of increase in the dark current even when the element is heat-treated, and an imaging device equipped with such a photoelectric conversion element. A photoelectric conversion element having a photoelectric conversion film which is sandwiched between a transparent electrically conductive film and an electrically conductive film and contains a photoelectric conversion layer and an electron blocking layer, wherein the electron blocking layer contains a compound having, as a substituent, a substituted amino group containing three or more ring structures.