Chemical Probe with PID Feedback for Optimal Sample Collection

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Solution Overview

Problem

Current chemical analysis systems face challenges in collecting optimal sample quantities and locations due to decoupling from analysis, leading to suboptimal results, including incorrect identifications, missed detections, and poor signal-to-noise ratios, and require decontamination procedures that may degrade samples.

Innovation Solution

A system comprising a probe with a photo ionization detector (PID) module and a microcontroller that determines the optimal sample collection location and quantity, storing data for optimal analysis settings, allowing for precise sample collection and analysis adjustments based on stored data.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If a remote sample collector is used to transport samples from contaminated zones to high performance analyzers, then analysis can be performed under controlled conditions, but the sample collection occurs in non-optimal time and location due to decoupling from analysis

Engineering Contradiction:
Improveanalysis qualityVSAvoidsample collection accuracy
Core Design Contradiction:
ReliabilityVSMeasurement precision

Solution Approach 1:

The system employs a PID detector in the probe that provides real-time feedback on vapor concentration during sample collection. This feedback mechanism allows the system to monitor and adjust collection parameters dynamically, ensuring optimal sample acquisition even when decoupled from the main analyzer, thus resolving the contradiction between reliable controlled analysis and precise sample collection

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The probe performs preliminary detection and sample collection with embedded intelligence before transporting to the analyzer. The PID detector and microcontroller prepare the sample optimally at the source location, conducting preliminary actions that ensure collection accuracy is maintained despite the subsequent decoupling from the high performance analyzer

Inventive Principle:
Principle #10Preliminary action

2Productivity

If sample collection is decoupled from analysis to allow remote collection, then logistical savings are achieved by allowing simultaneous collection in multiple locations, but suboptimal sample quantities are collected leading to poor signal-to-noise ratios

Engineering Contradiction:
Improvesampling efficiencyVSAvoidsignal-to-noise ratio
Core Design Contradiction:
ProductivityVSMeasurement precision

Solution Approach 1:

The microcontroller continuously monitors PID detector signals during sample collection and provides feedback to adjust collection duration and flow rate. This real-time feedback enables the system to collect optimal sample quantities even when operating independently from the analyzer, maintaining high signal-to-noise ratios while preserving the productivity benefits of remote simultaneous sampling

Inventive Principle:
Principle #23Feedback

Solution Approach 2:

The probe is equipped with self-service capabilities including an integrated PID detector, microcontroller, and memory that enable it to autonomously determine optimal collection parameters and execute sample acquisition without continuous analyzer control. This self-service architecture maintains measurement precision while achieving the productivity gains of decentralized simultaneous sampling across multiple locations

Inventive Principle:
Principle #25Self-service

3Weight of moving object

If miniaturized analyzers are used to reduce system size and weight, then portability is improved, but analytical performance is sacrificed making them too expensive for the performance provided

Engineering Contradiction:
Improveanalyzer weightVSAvoidanalytical performance
Core Design Contradiction:
Weight of moving objectVSReliability

Solution Approach 1:

The system is segmented into two functional parts: a lightweight probe for sample collection and a high performance analyzer for definitive analysis. This segmentation allows the probe to be portable and field-deployable while the analyzer, which requires high performance, can be positioned in controlled environments, thus resolving the contradiction between weight reduction and analytical performance

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The probe acts as an intermediary between the field environment and the high performance analyzer. It collects and prepares samples optimally using its integrated PID detector and microcontroller, then transports them to the analyzer. This intermediary role allows the system to achieve both portability in the field component and high analytical performance in the lab component, avoiding the need to compromise analyzer performance for weight reduction

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables accurate and efficient chemical sample collection with optimal quantity and location, improving analysis quality by adjusting instrumental settings dynamically, reducing the need for excessive decontamination and enhancing safety by minimizing exposure to hazardous environments.

Implementation Method 1

The probe includes a photo ionization detector (PID) module configured to measure vapor concentration of a chemical sample

Methodology Applied
Scientific EffectPhoto ionization: Photoionisation

Data Source

PatentUS10175198B2System and method for optimal chemical analysis
Publication Date: 2019.01.08 INFICON INC
  • US10175198B2 patent drawing
  • US10175198B2 patent drawing
  • US10175198B2 patent drawing

AI summary

A system and method for chemical analysis are described herein. The system includes a probe, a sample collection cartridge, and a chemical analyzer. The probe is configured to collect the optimal amount of sample for a future analysis and to store this chemical sample in the sample collection cartridge. The probe also collects sample data. The chemical analyzer is configured to determine the optimal analysis settings based on the sample data and analyze the chemical sample stored in the sample collection cartridge based on the optimal analysis settings.