Planar Grating X-ray Imaging for Low-Absorbing Specimens

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Solution Overview

Problem

Existing x-ray grating-based imaging systems face challenges in fabricating high aspect ratio gratings for high x-ray energies and matching grating geometries to divergent beam geometries, which leads to difficulties in maintaining image quality and requiring high radiation doses, especially for low-absorbing specimens.

Innovation Solution

The use of a novel planar geometry for gratings where X-rays pass through parallel to the substrate, allowing for the fabrication of gratings with extreme aspect ratios and arbitrary geometries, enabling phase-stepping without moving mechanical components, and integrating multiple gratings on a single substrate for enhanced visibility and sensitivity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional absorption-based radiography is used, then the imaging system is simple, but the visibility of low-absorbing specimens is poor and high radiation dose is required

Engineering Contradiction:
Improvevisibility of low-absorbing specimensVSAvoidradiation dose
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention exploits the phase shift effect where X-rays undergo phase changes when passing through specimens, converting invisible phase information into visible intensity variations through interferometric detection, thereby making low-absorbing specimens visible without increasing radiation dose

Inventive Principle:
Principle #32Color changes

Solution Approach 2:

The invention introduces reference beams and gratings as intermediary elements to mediate between the X-ray phase shifts and the detector, enabling the detection of phase contrast information that would otherwise be invisible in conventional absorption-based imaging

Inventive Principle:
Principle #24Intermediary (Mediator)

2Adaptability or versatility

If high aspect ratio gratings are fabricated for high x-ray energies, then the imaging capability for high energy x-rays is improved, but the fabrication difficulty increases significantly

Engineering Contradiction:
Improveimaging capability for high energy x-raysVSAvoidfabrication difficulty of high aspect ratio gratings
Core Design Contradiction:
Adaptability or versatilityVSEase of manufacture

Solution Approach 1:

The invention transitions from fabricating high aspect ratio three-dimensional gratings to using planar two-dimensional gratings with extended path length, changing the dimensional approach to achieve the same functional effect with much easier fabrication

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Solution Approach 2:

The invention uses the natural divergence of the X-ray beam to create an effective extended path length through planar gratings, utilizing the geometric curvature of the divergent beam rather than relying on physical grating height

Inventive Principle:
Principle #14Spheroidality (Curvature)

3Measurement precision

If traditional grating geometries are used, then the grating structure is simple, but the matching to divergent beam geometries is poor leading to reduced image quality

Engineering Contradiction:
Improveimage qualityVSAvoidgrating geometry complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The invention applies different grating line orientations and spacings at different locations across the grating surface to match the local geometry of the divergent beam, with each region optimized for its specific angular range

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention designs grating geometries that dynamically adapt to the divergent beam angles, with grating lines oriented to be perpendicular to the local beam direction at each position, allowing the static grating structure to effectively handle dynamic beam geometry

Inventive Principle:
Principle #15Dynamics

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for the reduction of radiation dose while maintaining image quality by enabling the fabrication of high aspect ratio gratings and matching geometries to divergent beams, improving visibility and sensitivity, and eliminating the need for mechanical phase stepping, thereby enhancing the imaging capabilities for low-absorbing specimens.

Implementation Method 1

Grating based x-ray imaging setups essentially detect the deflections of x-rays in the object. Such deflections can be either caused by refraction on phase shift gradients in the object resulting in differential phase contrast (DPC) or by scattering on inhomogeneities in the sample resulting in the so-called dark-field image (DFI) contrast.

Methodology Applied
Scientific EffectDiffraction: Diffraction

Implementation Method 2

Such deflections can be either caused by refraction on phase shift gradients in the object resulting in differential phase contrast (DPC)

Methodology Applied
Scientific EffectRefraction: Refraction

Implementation Method 3

the imaginary part β describes the absorption property of the sample

Methodology Applied
Scientific EffectAbsorption (EM radiation): Absorption (EM radiation)

Data Source

PatentEP2585817B1A method for x-ray phase contrast and dark-field imaging using an arrangement of gratings in planar geometry
Publication Date: 2020.01.22 PAUL SCHERRER INSTITUT
  • EP2585817B1 patent drawingFigure 1
  • EP2585817B1 patent drawingFigure 2A
  • EP2585817B1 patent drawingFigure 2B

AI summary

An X-ray arrangement is suitable to record absorption, phase contrast, and dark field images of an object. The visibility of low absorbing specimens is improved and required radiation dose is reduced. The assembly includes an X-ray source; two or more gratings; a position-sensitive detector with spatially modulated detection sensitivity; a recorder for recording the images; an evaluator for evaluating the intensities for each pixel to identify the characteristic of the object for each individual pixel as an absorption and/or a differential phase contrast and/or an x-ray scattering dominated pixel. Images are collected by rotating from 0 to n or 2n either the sample or the assembly. The gratings are produced with planar geometry. The X-rays pass through the gratings parallel to the substrate. The grating structures extend along the X-ray path which determines the phase shift. The attenuation of the X-rays caused by the grating structures is no longer given by the thickness, but by the length of the grating structures.