Planar Sample Holder Lid for FIB-SEM Interference Reduction

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Solution Overview

Problem

Existing sample holders for air-sensitive materials in FIB-SEM systems interfere with the microscope's components due to protruding fasteners, limiting the resolution and complexity of nanofabrication and tilt capabilities, requiring extensive and costly modifications to the FIB-SEM system.

Innovation Solution

A sample holder design with a lid featuring recessed closure arm receiving portions and an in-built elevator mechanism, allowing for a planar top surface without protrusions and enabling secure sealing through complementary surfaces, reducing interference with microscope components and enhancing tilt capabilities.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If traditional fasteners (screws and knobs) are used to secure the lid, then the sealing and securing function is achieved, but the fasteners protrude outward and interfere with microscope components, restricting resolution and tilt capabilities

Engineering Contradiction:
Improvesealing functionVSAvoidinterference with microscope components
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent extracts the fastening function from protruding external fasteners and relocates it to recessed closure arm receiving portions on the lid. The closure arms engage with these recessed portions from below, removing the need for outward-protruding screws or knobs while maintaining secure sealing capability.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent transitions from a top-down fastening approach (protruding fasteners on the lid surface) to a bottom-up approach (closure arms engaging from below). This dimensional change allows the fastening mechanism to operate in a different spatial dimension, eliminating interference with overhead microscope components.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

2Reliability

If protruding fasteners are used on the lid, then secure closure is achieved, but the tilt mechanism range is restricted

Engineering Contradiction:
Improveclosure securityVSAvoidtilt capability
Core Design Contradiction:
ReliabilityVSEase of operation

Solution Approach 1:

The patent removes protruding fasteners that physically block the tilt mechanism's range of motion. By relocating the fastening function to recessed receiving portions, the lid surface remains clear, allowing the tilt mechanism to operate through its full intended range without mechanical interference.

Inventive Principle:
Principle #2Taking out (Extraction)

3Adaptability or versatility

If extensive modifications are made to the FIB-SEM system to accommodate protruding fasteners, then the sample holder can be used, but time and cost increase significantly

Engineering Contradiction:
Improvecompatibility with FIB-SEMVSAvoidmodification time
Core Design Contradiction:
Adaptability or versatilityVSLoss of time

Solution Approach 1:

Instead of modifying the expensive FIB-SEM microscope to accommodate protruding fasteners, the patent inverts the approach by designing the sample holder lid to accommodate closure arms from below. This eliminates the need for costly and time-consuming microscope modifications while achieving full compatibility.

Inventive Principle:
Principle #13The other way round (Inversion)

4Device complexity

If a planar flat surface lid is used, then interference with high-resolution microscopy is reduced, but traditional sealing mechanisms become more difficult to implement

Engineering Contradiction:
Improveinterference with microscopeVSAvoidsealing mechanism implementation
Core Design Contradiction:
Device complexityVSEase of manufacture

Solution Approach 1:

The patent implements sealing from the bottom dimension rather than the top surface. Closure arms engage with recessed receiving portions and apply sealing force from below, maintaining a clean planar top surface while achieving effective sealing through a different spatial approach.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

Solution Approach 2:

The recessed closure arm receiving portions serve as intermediary structures that enable sealing functionality without requiring protruding elements. These recessed portions act as mediators between the closure arms and the lid, allowing sealing force application while preserving the planar surface geometry.

Inventive Principle:
Principle #24Intermediary (Mediator)

Data Source

PatentUS11521824B2Sample holder for electron microscopy
Publication Date: 2022.12.06 ZONEXUS LLC
  • US11521824B2 patent drawing
  • US11521824B2 patent drawing
  • US11521824B2 patent drawing

AI summary

A sample holder for electron microscopy of air-sensitive samples for use in electron microscopy incorporates a housing and a closure assembly. The closure assembly comprises a lid comprising at least one closure arm receiving portions recessed within a flat, planar upper surface thereof. The housing comprises one or more closure arm(s) corresponding to one or more closure arm receiving portion(s). In a fully closed position, the closure arm(s) share contact with the closure arm receiving portion(s). The lid is flexibly coupled to a motor cover plate which can be actuated by a motor assembly configured to open and close the lid. The sample holder also includes an elevator assembly with a vertically adjustable sample stage which sits below the lid. The sample stage is vertically adjusted by actuation of a bellows assembly which sits beneath the sample stage.