Plant Protein Separation via Acidification and Heating

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Solution Overview

Problem

Current processes for producing plant products, such as protein isolates, often result in denatured proteins with reduced functional properties and fail to effectively separate nutritionally valuable components from those of negative nutritional value, particularly considering multiple contaminant components simultaneously.

Innovation Solution

A process involving lowering the pH to below 3.5 and increasing the temperature to 50-80°C, which enhances protein solubility and allows for easier separation of proteins from non-protein components like phytate, phenolics, and alkaloids, thereby producing plant products with reduced content of negative nutritional components without the need for additional enzymes or inhibitors.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If heat coagulation is used to recover protein from plant raw materials, then protein recovery is achieved on industrial scale, but the protein becomes denatured and loses functional properties

Engineering Contradiction:
Improveprotein recoveryVSAvoidfunctional properties
Core Design Contradiction:
ProductivityVSReliability

Solution Approach 1:

The invention changes the pH parameter to a range of 3.0-6.0 (below the conventional isoelectric point) and controls temperature to prevent denaturation. This parameter change allows protein separation while maintaining functional properties, resolving the contradiction between recovery and functionality.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the mechanical/thermal coagulation system with a pH-based separation system. Instead of using heat to coagulate proteins, the process uses acidification to alter solubility and enable separation, thereby preserving protein structure and function while achieving industrial-scale recovery.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Manufacturing precision

If current processes focus on individual contaminant removal, then specific components can be reduced, but multiple contaminant components are not effectively addressed simultaneously

Engineering Contradiction:
Improvecontaminant removalVSAvoidmulti-contaminant handling
Core Design Contradiction:
Manufacturing precisionVSAdaptability or versatility

Solution Approach 1:

The invention creates a universal process that simultaneously addresses multiple contaminant types (phytate, phenolics, saponins, alkaloids, oligosaccharides) through a single pH adjustment mechanism. This multi-functional approach resolves the contradiction between precision removal and versatile applicability.

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The invention merges the removal of multiple different contaminant classes into a single integrated process step by adjusting pH to 3.0-6.0. This consolidation achieves simultaneous removal of diverse contaminants, resolving the contradiction between targeted precision and broad applicability.

Inventive Principle:
Principle #5Merging (Combining)

3Manufacturing precision

If pH is lowered to below 3.5 and temperature increased to 50-80°C, then protein solubility increases and separation from non-protein components is enhanced, but energy consumption increases

Engineering Contradiction:
Improveseparation efficiencyVSAvoidenergy consumption
Core Design Contradiction:
Manufacturing precisionVSUse of energy by moving object

Solution Approach 1:

The invention optimizes the balance between pH and temperature parameters to achieve effective separation while controlling energy input. By selecting specific ranges (pH 3.0-6.0, temperature 50-80°C), the process achieves high separation efficiency with moderate energy consumption, resolving the contradiction between precision and energy use.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method increases protein solubility and separation efficiency, resulting in plant products with improved nutritional value and reduced content of non-protein components, maintaining functional properties of proteins and preventing enzymatic browning or discolouration.

Implementation Method 1

lowering the pH to below 3.5

Methodology Applied
Scientific EffectpH adjustment:

Implementation Method 2

increasing the temperature to 50-80°C

Methodology Applied
Scientific EffectTemperature increase: Heating

Implementation Method 3

enhances protein solubility

Methodology Applied
Scientific EffectProtein solubility enhancement:

Implementation Method 4

allows for easier separation of proteins from non-protein components like phytate, phenolics, and alkaloids

Methodology Applied
Scientific EffectSeparation of components:

Implementation Method 5

preventing enzymatic browning or discolouration

Methodology Applied
Scientific EffectEnzymatic browning prevention:

Data Source

PatentEP2680709B1A process for the manufacture of a product from a plant material
Publication Date: 2023.06.14 UNIVERSITY OF COPENHAGEN
  • EP2680709B1 patent drawingFigure 1
  • EP2680709B1 patent drawingFigure 2
  • EP2680709B1 patent drawingFigure 3

AI summary

The present invention relates to a process for the manufacture of a product from a plant material comprising the steps of providing a disrupted plant material comprising <10 %(w/w) starch and <10 %(w/w) oil/lipids; adjusting the pH of the disrupted plant material to a value of pH 3.5 or below to provide an acidic suspension; heating the acidic suspension to a temperature in the range of about 50°C to about 80°C; isolating the product from the heated, acidic suspension. The product may be a protein product or a non-protein product. In particular, the process of the invention provides a protein product with reduced contents of non-protein components of negative nutritional value.