Plasma-Activated Textile Hydrophobization to Reduce Fluorocarbon Use

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Solution Overview

Problem

Current methods for producing hydrophobic textile surfaces often rely on long-lasting chemicals like fluorocarbons, which are environmentally harmful and non-biodegradable, and lack effective, durable, and environmentally friendly processes for creating water-repellent or waterproof textiles suitable for demanding uses.

Innovation Solution

A method involving low-pressure plasma treatment with oxygen-containing compounds in a gas mixture of O2 and inert gases, followed by wet chemical treatment with hydrophobing agents, to create a hydrophobic textile surface that is durable, water-repellent, and potentially waterproof, while minimizing the use of harmful chemicals and ensuring biodegradability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If fluorine-containing chemicals are used to finish textiles for water repellency, then hydrophobic surface properties are achieved, but environmental harm and non-biodegradability occur

Engineering Contradiction:
Improvewater repellencyVSAvoidenvironmental harm
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention changes the chemical composition parameters by using fluorine-free hydrophobing agents (such as silicones, polyurethanes, or wax-based compounds) instead of fluorine-containing chemicals. This substitution maintains the hydrophobic surface properties while eliminating the environmental harm associated with persistent fluorinated compounds.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs biodegradable hydrophobing agents that can break down naturally after performing their function, replacing long-lasting fluorinated chemicals. These shorter-lived, biodegradable substances provide the necessary water repellency during use but do not persist in the environment, thereby reducing ecological harm.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

2Ease of manufacture

If conventional wet chemical treatment is applied without plasma treatment, then processing simplicity is maintained, but hydrophobization durability is insufficient

Engineering Contradiction:
Improveprocessing simplicityVSAvoidhydrophobization durability
Core Design Contradiction:
Ease of manufactureVSDuration of action of stationary object

Solution Approach 1:

The invention introduces a preliminary plasma treatment step before wet chemical hydrophobization. This plasma activation prepares the textile surface by removing contaminants and creating a more reactive surface, which enhances the bonding of subsequent hydrophobing agents and significantly improves the durability of the hydrophobic finish.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The invention combines two different treatment methods (plasma treatment and wet chemical treatment) into a composite process. The plasma treatment modifies the surface properties, while the wet chemical treatment applies the hydrophobing agent, creating a synergistic effect that results in superior and more durable hydrophobization compared to either method alone.

Inventive Principle:
Principle #40Composite materials

3Manufacturing precision

If high oxygen concentration is used in plasma treatment, then surface activation is improved, but material degradation increases

Engineering Contradiction:
Improvesurface activationVSAvoidmaterial integrity
Core Design Contradiction:
Manufacturing precisionVSStrength

Solution Approach 1:

The invention optimizes the oxygen concentration parameter in the plasma treatment process, using a controlled and moderate oxygen level rather than high concentration. This parameter adjustment achieves sufficient surface activation for improved hydrophobization while preventing excessive oxidation and degradation of the textile fibers, thereby maintaining material integrity.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The method produces textiles with robust, long-lasting water-repellent or waterproof properties suitable for professional or industrial use, maintaining performance under demanding conditions and allowing for subsequent refreshment of hydrophobic properties, while reducing environmental impact and promoting biodegradability.

Implementation Method 1

A plasma is a partially ionized gas, which is often referred to as the 'fourth state of matter'. Phenomena such as lightning or the northern lights (aurora borealis) are plasmas that occur in nature. Technically, they can be generated by applying electric fields. Plasmas are interesting because of their physical and chemical properties. Highly excited particles and radicals are generated in them. These can trigger chemical reactions that are not possible under normal conditions.

Methodology Applied
Scientific EffectPlasma: Plasma

Data Source

PatentEP3697958B1Method for producing a textile article with hydrophobised textile surface using plasma treatment and wet chemical processing
Publication Date: 2021.03.10 WERNER & MERTZ GMBH

AI summary

A process for producing a textile article having a water-repellent textile surface is described, comprising the following steps: plasma-treatment of a textile surface such that a plasma-treated textile surface results, and subsequently wet-chemical treatment of the plasma-treaded textile surface, or of a textile surface produced therefrom in further steps, with a water repellent, such that a plasma-treated water-repellent textile surface results. Moreover, a textile article that is producible with the process according to the invention is described. Furthermore, the use of a low-pressure plasma process for the preparatory treatment of a textile surface of an article before the textile surface is made water-repellent by wet-chemical means is described.