Plasma-Assisted Ceramic Sintering Device

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Solution Overview

Problem

Ceramic materials prepared by high-temperature sintering often have large grain sizes and high energy consumption, which can limit their mechanical and electrical properties.

Innovation Solution

A plasma-assisted ceramic sintering device and method that uses a plasma jet device to generate plasma, which is applied to a ceramic green body within an enclosed container, optimizing the sintering process to achieve smaller grain sizes and improved properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If high-temperature sintering is used to prepare ceramic materials, then the sintering process can achieve complete densification, but the grain size becomes large and energy consumption increases

Engineering Contradiction:
Improvedensification qualityVSAvoidsintering temperature
Core Design Contradiction:
ReliabilityVSTemperature

Solution Approach 1:

The patent changes the sintering parameters by introducing plasma-assisted sintering at lower temperatures (room temperature to moderate temperatures) instead of conventional high-temperature sintering. The plasma provides localized energy and reactive species that enable densification without requiring high bulk temperatures, thus resolving the contradiction between achieving complete densification and maintaining low temperature to prevent large grain growth

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent replaces the conventional thermal field-based sintering mechanism with a plasma field-based mechanism. The plasma provides ion bombardment, radical reactions, and localized heating that substitute for the uniform thermal diffusion process, enabling effective sintering at lower temperatures and preventing excessive grain growth

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Reliability

If high-temperature sintering is used to prepare ceramic materials, then the sintering process can achieve complete densification, but the energy consumption increases

Engineering Contradiction:
Improvedensification qualityVSAvoidenergy consumption
Core Design Contradiction:
ReliabilityVSUse of energy by moving object

Solution Approach 1:

The patent changes the energy input parameters by using plasma power density instead of bulk thermal energy. The plasma delivers energy directly to the ceramic green body surface and near-surface regions, achieving densification with lower total energy input compared to conventional high-temperature sintering that requires heating the entire system to high temperatures

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent substitutes the energy-intensive thermal field with a more efficient plasma field that delivers energy directly to where it is needed for sintering. The plasma's ion and electron bombardment, along with reactive species, provide localized energy transfer that is more efficient than conventional thermal conduction and radiation, reducing overall energy consumption

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Device complexity

If conventional sintering is used, then the process is simple, but the grain size becomes large which limits mechanical and electrical properties

Engineering Contradiction:
Improvesintering process complexityVSAvoidgrain size control
Core Design Contradiction:
Device complexityVSManufacturing precision

Solution Approach 1:

The patent changes the sintering parameters to include plasma power density, gas flow rate, and exposure time, which provide finer control over the sintering process. These parameters enable precise control of grain growth kinetics, achieving small grain sizes while maintaining densification, unlike conventional sintering where temperature alone provides coarse control

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent substitutes the simple but imprecise thermal field with a plasma field that offers multiple controllable parameters (power, gas composition, flow rate). This substitution increases process complexity but provides the manufacturing precision needed to control grain size and achieve superior mechanical and electrical properties

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The plasma-assisted sintering method enables rapid densification of ceramic materials at room temperature, reducing grain size and enhancing mechanical and electrical properties, while also lowering energy consumption.

Implementation Method 1

the working electrode to discharge and generate plasma in the working gas

Methodology Applied
Scientific EffectPlasma: Plasma

Implementation Method 2

Discharge along dielectric surface of the ceramic green body occurs after the target voltage is achieved. Then, conductivity of the ceramic green body changes. After discharge along dielectric surface of the ceramic green body occurs, conductive channels can be formed inside the ceramic green body

Methodology Applied
Scientific EffectElectrical discharge: Electric Arc

Implementation Method 3

rapid sintering of ceramics can be achieved under Joule heating effect

Methodology Applied
Scientific EffectJoule heating: Joule Heating

Implementation Method 4

The generated plasma can process the ceramic green body in the enclosed container to optimize the properties of the ceramics

Methodology Applied
Scientific EffectPlasma surface treatment: Plasma

Data Source

PatentUS20250051241A1Plasma-assisted ceramic sintering device and ceramic sintering method
Publication Date: 2025.02.13 TSINGHUA SHENZHEN INTERNATIONAL GRADUATE SCHOOL
  • US20250051241A1 patent drawing
  • US20250051241A1 patent drawing
  • US20250051241A1 patent drawing

AI summary

The application provides a plasma-assisted ceramic sintering device and method. The plasma-assisted ceramic sintering device includes an enclosed container receiving ceramic green body and defining a gas outlet. A plasma jet device includes a working power supply and a plasma generation chamber. The plasma generation chamber defines a gas input port, and a gas output port located in the enclosed container. The plasma generation chamber includes a working electrode having a first end and a second end. The first end electrically connects the working power supply, and the second end is adjacent to the gas output port. A gas output device connects the gas input port for inputting working gas into the plasma generation chamber. A power supply device can electrically connect and apply voltage to the ceramic green body, obtaining the ceramic by sintering. The sintering device of the application provides plasma-assisted sintering and optimizes properties of ceramic materials.