3D Graphene-Resin Composites via Plasma Functionalization

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Solution Overview

Problem

Current methods for producing carbon-resin composites face challenges in achieving optimal mechanical and electrical properties due to limitations in the uniform dispersion of carbon materials within polymer resins, leading to issues with agglomeration and undesirable material performance.

Innovation Solution

The production of carbon particles with a 3D structure, such as 3D graphene, in a plasma reactor, where these particles are functionalized in-situ to enhance adhesion with a binder, allowing for improved interfacial strength and bonding within the composite material, thereby customizing properties like tensile strength and modulus.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Strength

If carbon particles are added to polymer resin to improve mechanical and electrical properties, then the composite material achieves enhanced strength and conductivity, but the carbon particles tend to agglomerate leading to non-uniform dispersion and undesirable material performance

Engineering Contradiction:
Improvemechanical strengthVSAvoiduniform dispersion
Core Design Contradiction:
StrengthVSStability of the object's composition

Solution Approach 1:

The patent applies parameter changes by modifying the surface chemistry of carbon particles through plasma treatment, which alters surface energy and chemical composition to improve dispersion stability in polymer resin matrices, preventing agglomeration while maintaining enhanced mechanical strength

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite system combining carbon particles with polymer resin, where the carbon phase provides mechanical reinforcement and electrical conductivity while the polymer matrix provides structural continuity and dispersion medium, achieving synergistic properties

Inventive Principle:
Principle #40Composite materials

2Strength

If carbon particles are functionalized to improve adhesion with binder, then interfacial strength increases, but the complexity of the production process increases

Engineering Contradiction:
Improveinterfacial strengthVSAvoidproduction process complexity
Core Design Contradiction:
StrengthVSDevice complexity

Solution Approach 1:

The patent merges the carbon particle production and surface functionalization steps into a single plasma reactor process, where both the carbon particles are synthesized and simultaneously surface-modified with polymer chains, eliminating separate functionalization steps and reducing overall process complexity

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The plasma reactor enables self-service by allowing carbon particles to be produced and functionalized in-situ within the same reaction environment, where the plasma environment automatically provides both synthesis and surface modification functions without requiring external intervention

Inventive Principle:
Principle #25Self-service

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach results in composites with enhanced mechanical properties, including higher strength and toughness, while maintaining a low viscosity of the uncured polymer-carbon mixture, and allows for tailored properties such as flexibility and directional conductivity.

Implementation Method 1

producing a plurality of carbon particles in a plasma reactor

Methodology Applied
Scientific EffectPlasma: Plasma

Implementation Method 2

functionalizing the plurality of carbon particles in-situ in the plasma reactor to promote adhesion to a binder

Methodology Applied
Scientific EffectPlasma enhanced chemical reactions: Plasma Enhanced Chemical Vapour Deposition

Data Source

PatentUS10907031B2Composite materials systems containing carbon and resin
Publication Date: 2021.02.02 LYTEN INC
  • US10907031B2 patent drawing
  • US10907031B2 patent drawing
  • US10907031B2 patent drawing

AI summary

Methods include producing a plurality of carbon particles in a plasma reactor, functionalizing the plurality of carbon particles in-situ in the plasma reactor to promote adhesion to a binder, and combining the plurality of carbon particles with the binder to form a composite material. The plurality of carbon particles comprises 3D graphene, where the 3D graphene comprises a pore matrix and graphene nanoplatelet sub-particles in the form of at least one of: single layer graphene, few layer graphene, or many layer graphene. Methods also include producing a plurality of carbon particles in a plasma reactor; functionalizing, in the plasma reactor, the plurality of carbon particles to promote chemical bonding with a resin; and combining, within the plasma reactor, the functionalized plurality of carbon particles with the resin to form a composite material.