Plasma Emission Spectroscopy for Rapid Heavy Metal Detection

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Solution Overview

Problem

Current methods for analyzing components in fine dust, such as inductively coupled plasma mass spectrometry, are inefficient and time-consuming, making it difficult to accurately and quickly measure heavy metals in air samples.

Innovation Solution

A device and method utilizing a plasma generation unit with electrodes to ionize samples, followed by signal detection units that sense light emitted by heavy metals as they return to a ground state, allowing for accurate measurement of heavy metal concentrations through controlled timing and wavelength filtering.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Measurement precision

If inductively coupled plasma mass spectrometry or mass spectrometer is used to analyze components in fine dust, then measurement precision of heavy metals is improved, but analysis time increases significantly (taking more than one hour)

Engineering Contradiction:
Improveheavy metal concentration measurementVSAvoidanalysis time
Core Design Contradiction:
Measurement precisionVSLoss of time

Solution Approach 1:

The patent extracts only the essential function of plasma generation and light detection needed for heavy metal analysis, removing unnecessary components like complex mass spectrometry systems. By using a simple plasma generation unit with electrodes and photodetectors to directly measure emission spectra, the system achieves rapid heavy metal detection without the time-consuming sample preparation and analysis steps of conventional methods.

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The patent replaces complex mechanical and chemical analysis systems (centrifugal separators, chemical preconditioning) with an optical detection system. The plasma emission spectra are directly detected by photodetectors, substituting mechanical separation and chemical processing with non-contact optical measurement, enabling real-time analysis.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Measurement precision

If conventional methods with chemical preconditioning are used, then measurement accuracy is improved, but device complexity and operation time increase

Engineering Contradiction:
Improveconcentration detection accuracyVSAvoidsystem complexity
Core Design Contradiction:
Measurement precisionVSDevice complexity

Solution Approach 1:

The patent employs self-service principles by allowing the plasma generation unit to automatically ionize the sample and the photodetectors to automatically detect the emission spectra without external chemical preconditioning. The system performs sample introduction, plasma generation, and spectral detection in an integrated manner, eliminating the need for separate chemical preparation steps and reducing operational complexity.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The patent changes the detection parameter from requiring chemical state information (in conventional methods) to detecting optical emission spectra directly. By measuring the intensity of characteristic emission lines at specific wavelengths, the system determines heavy metal concentrations based on optical parameters rather than chemical properties, simplifying the overall process.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

Enables rapid and precise measurement of heavy metal concentrations in air samples by detecting plasma emission spectra without chemical preconditioning, allowing for real-time calculation.

Implementation Method 1

a plasma generation unit (20) connected to the power supply unit (10) and including a pair of electrodes facing each other

Methodology Applied
Scientific EffectPlasma: Plasma

Implementation Method 2

supply power to generate plasma

Methodology Applied
Scientific EffectElectrical discharge: Electric Arc

Implementation Method 3

sense light emitted from the sample because of the plasma

Methodology Applied
Scientific EffectLight emission: Luminescence

Implementation Method 4

signal detection units arranged on the electrodes and configured to sense light emitted

Methodology Applied
Scientific EffectPhotoelectric effect: Photoelectric Effect

Data Source

PatentUS11860107B2Device and method for detecting concentration of specimen
Publication Date: 2024.01.02 SEOUL NATIONAL UNIVERSITY R&DB FOUNDATION
  • US11860107B2 patent drawing
  • US11860107B2 patent drawing
  • US11860107B2 patent drawing

AI summary

A device and a method of detecting a concentration of a sample are provided. The device includes a power supply unit configured to supply power to generate plasma, a plasma generation unit connected to the power supply unit and including a pair of electrodes facing each other, a plurality of signal detection units arranged on the pair of electrodes and configured to sense light emitted from the sample because of the plasma, and a controller configured to control a driving start point of the signal detection unit so that the signal detection unit is driven after a preset period of time after oscillation is terminated between the pair of electrodes.