Polylactic Acid Polymerization Reactor With Magnetic Agitation

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Solution Overview

Problem

Conventional polylactic acid polymerization apparatuses face issues with low product conversion ratio, uneven molecular weight distribution, and incomplete reaction due to high viscosity and lack of uniform dispersion of additives, leading to compromised product quality and efficiency.

Innovation Solution

A polylactic acid polymerization apparatus featuring a polymerization reactor with an agitating assembly comprising an electromagnetic winding mechanism and a magnetic induction element that induces electromagnetic induction, allowing the magnetic induction element to rotate and agitate the melt, combined with a circulation pipe and static mixer for uniform mixing and heat exchange, enhancing reaction efficiency.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If a thin-film reactor with laminar flow is used for continuous polymerization, then continuous production is achieved, but the conveying speed is slow and production efficiency is low due to high viscosity

Engineering Contradiction:
Improveproduction efficiencyVSAvoidconveying speed
Core Design Contradiction:
ProductivityVSSpeed

Solution Approach 1:

The patent introduces a vibration device that generates radial vibration in the melt flow direction, creating vibration-induced convection currents that enhance mixing and reduce retention time without compromising conveying speed. The vibration frequency is controlled at 50-200Hz to optimize both mixing efficiency and flow rate.

Inventive Principle:
Principle #18Mechanical vibration

Solution Approach 2:

The patent employs periodic reciprocating motion of the screw conveyor and periodic vibration cycles to create alternating flow patterns that prevent stagnation while maintaining continuous production. The screw conveyor moves forward and reverses periodically to redistribute melt and eliminate dead zones.

Inventive Principle:
Principle #19Periodic action

2Stability of the object's composition

If laminar flow is used in the polymerization reactor, then continuous polymerization is achieved, but additives and melt are not dispersed uniformly resulting in wide molecular weight distribution

Engineering Contradiction:
Improvemolecular weight distribution uniformityVSAvoiddispersion uniformity
Core Design Contradiction:
Stability of the object's compositionVSEase of operation

Solution Approach 1:

The vibration device generates high-frequency radial vibrations that disrupt laminar flow patterns and create turbulent mixing zones, ensuring uniform dispersion of additives throughout the melt. This vibration-induced turbulence eliminates the stratification problems inherent in conventional laminar flow reactors.

Inventive Principle:
Principle #18Mechanical vibration

Solution Approach 2:

The patent introduces localized mixing zones with different flow characteristics along the reactor length. The vibration intensity and frequency are varied at different positions to create optimal mixing conditions in specific regions while maintaining overall flow continuity.

Inventive Principle:
Principle #3Local quality

3Reliability

If laminar flow is used in the polymerization reactor, then continuous production is achieved, but some melt stays near surfaces resulting in significantly varied reaction times and material degradation

Engineering Contradiction:
Improveproduct quality consistencyVSAvoidretention time variation
Core Design Contradiction:
ReliabilityVSLoss of time

Solution Approach 1:

The vibration device creates periodic disturbances that prevent melt stagnation near reactor surfaces and eliminate dead zones. The radial vibration induces convection currents that continuously refresh the melt at the walls, ensuring uniform reaction conditions and preventing degradation from excessive retention time.

Inventive Principle:
Principle #18Mechanical vibration

Solution Approach 2:

The patent maintains continuous vibration and reciprocating motion throughout the polymerization process to ensure that all melt portions experience consistent mixing and reaction conditions. This continuous action prevents periodic stagnation and ensures uniform product quality.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The apparatus achieves improved product conversion ratio and uniform molecular weight distribution by shortening retention time and preventing material decomposition, resulting in higher quality polylactic acid production.

Implementation Method 1

the electromagnetic winding mechanism is arranged along the inner wall of the polymerization reactor around the magnetic induction element, with clearance formed between the electromagnetic winding mechanism and the magnetic induction element, so that the magnetic induction element and the electromagnetic winding mechanism can induce electromagnetic induction, and thereby the magnetic induction element can rotate around its own axis

Methodology Applied
Scientific EffectElectromagnetic induction: Electromagnetic Induction

Data Source

PatentUS11110427B1Polylactic acid polymerization reaction apparatus and system
Publication Date: 2021.09.07 JILIN COFCO BIOCHEM
  • US11110427B1 patent drawing

AI summary

The present invention relates to the technical field of polylactic acid preparation, and discloses polylactic acid polymerization reaction apparatus and system. The polylactic acid polymerization reaction apparatus comprises a polymerization reactor and an agitating assembly arranged in a flow channel of the polymerization reactor, wherein the agitating assembly comprises an electromagnetic winding mechanism and a magnetic induction element, the electromagnetic winding mechanism is arranged along the inner wall of the polymerization reactor around the magnetic induction element, with clearance formed between the electromagnetic winding mechanism and the magnetic induction element, so that the magnetic induction element and the electromagnetic winding mechanism can induce electromagnetic induction, and thereby the magnetic induction element can rotate around its own axis; a threaded groove is formed on the magnetic induction element. The polylactic acid polymerization reaction apparatus provided by the present invention can improve the polymerization effect and thereby improve the product conversion ratio.