Plasma Reactor with External Resistive Heating for Metallic Piece Treatment

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Solution Overview

Problem

Current plasma reactors face challenges in achieving homogeneous and controlled high temperatures independent of electrical discharge parameters, leading to potential electrical arcs and contamination issues during the cleaning and thermochemical treatment of metallic pieces, especially those produced by powder metallurgy.

Innovation Solution

A plasma process and reactor design featuring a reaction chamber with external resistive heating and a confined anode-cathode system, where the support and metallic pieces are heated externally to maintain temperatures above contaminant condensation points, allowing for independent control of plasma generation parameters and preventing arc formation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If plasma is used for cleaning and thermochemical treatment in the same reactor, then processing time is reduced and productivity is improved, but temperature control becomes difficult and electrical arcs may occur

Engineering Contradiction:
Improveprocessing timeVSAvoidtemperature control
Core Design Contradiction:
ProductivityVSTemperature

Solution Approach 1:

The reactor is divided into distinct functional zones: a plasma generation zone with confined anode-cathode system for cleaning operations, and a separate heating zone with external resistive heating for thermochemical treatment. This segmentation allows independent control of plasma parameters and temperature, enabling both operations to proceed effectively in sequence within the same reactor without thermal interference or arc formation.

Inventive Principle:
Principle #1Segmentation

2Object-affected harmful factors

If high temperature is achieved through plasma discharge, then contaminant removal is effective, but electrical arcs form and contamination occurs

Engineering Contradiction:
Improvecontaminant removalVSAvoidarc formation and contamination
Core Design Contradiction:
Object-affected harmful factorsVSObject-generated harmful factors

Solution Approach 1:

The harmful effect of high-temperature plasma discharge is extracted and replaced by a separate external resistive heating system. The plasma generation system uses confined anode-cathode geometry to produce low-temperature plasma suitable for cleaning, while the external heating apparatus provides the necessary high temperature for thermochemical treatment without generating electrical arcs or contamination within the reaction chamber.

Inventive Principle:
Principle #2Taking out (Extraction)

3Object-affected harmful factors

If conventional chemical cleaning with organic solvents is used, then complete contaminant removal is achieved, but environmental pollution increases and processing complexity increases

Engineering Contradiction:
Improvecontaminant removal completenessVSAvoidenvironmental pollution
Core Design Contradiction:
Object-affected harmful factorsVSObject-generated harmful factors

Solution Approach 1:

The mechanical-chemical cleaning process using organic solvents and ultrasound is replaced by a plasma-based cleaning system. The plasma generates reactive species that chemically decompose and volatilize contaminants, which are then removed by the vacuum system. This substitution eliminates the need for hazardous chemical solvents and their associated environmental pollution while maintaining effective contaminant removal.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

4Manufacturing precision

If cleaning and thermochemical treatment are performed in separate equipment, then each process can be optimized, but processing time increases and productivity decreases

Engineering Contradiction:
Improveprocess optimizationVSAvoidprocessing time
Core Design Contradiction:
Manufacturing precisionVSProductivity

Solution Approach 1:

The cleaning and thermochemical treatment operations are merged into a single reactor system with integrated plasma generation and external heating capabilities. The reactor features a confined anode-cathode system for plasma cleaning and external resistive heating elements for thermochemical treatment, allowing both processes to be performed sequentially on the same workpiece without transfer between equipment, thereby reducing processing time while maintaining process optimization.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables efficient and homogeneous cleaning and thermochemical treatment of metallic pieces within the same thermal cycle, reducing processing time and energy consumption while avoiding contamination and arc formation, thus enhancing productivity and surface treatment quality.

Implementation Method 1

external resistive heating and a confined anode-cathode system, where the support and metallic pieces are heated externally

Methodology Applied
Scientific EffectResistive heating: Joule Heating

Implementation Method 2

an abnormal electrical discharge. The electrons provoke an electronic bombardment on the assembly defined by the support and pieces

Methodology Applied
Scientific EffectPlasma generation: Plasma

Implementation Method 3

The electrons provoke an electronic bombardment on the assembly defined by the support and pieces connected to the reactor anode

Methodology Applied
Scientific EffectElectron bombardment: Electron Beam

Implementation Method 4

For example, during plasma nitration, the oil retained in the pores and on the surface of the pieces produces instabilities in the electrical discharge

Methodology Applied
Scientific EffectPlasma nitration: Nitriding

Data Source

PatentUS8926757B2Plasma process and reactor for treating metallic pieces
Publication Date: 2015.01.06 EMBRACO IND DE COMPRESSORES E SOLUCOES EM REFRIGERACAO LTDA
  • US8926757B2 patent drawing
  • US8926757B2 patent drawing
  • US8926757B2 patent drawing

AI summary

The plasma reactor defines a reaction chamber provided with a support for the metallic pieces and an anode-cathode system, and a heating means is mounted externally to said plasma reactor. The plasma process, for a cleaning operation, includes the steps of connecting the support to the grounded anode and the cathode to a negative potential of a power source; feeding an ionizable gaseous charge into the reaction chamber and heating the latter at vaporization temperatures of piece contaminants; applying an electrical discharge to the cathode; and providing the exhaustion of the gaseous charge and contaminants. A subsequent heat treatment includes the steps of: inverting the energization polarity of the anode-cathode system; feeding a new gaseous charge to the reaction chamber and maintaining it heated; applying an electrical discharge to the cathode; and exhausting the gaseous charge from the reaction chamber.