Plasma Spray Fabrication of Textured Ceramic Templates

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Solution Overview

Problem

Existing methods for fabricating textured ceramic templates are slow, produce low yields, and require complex processes involving chemical solutions and post-fabrication processing to achieve the desired disk-like structure with specific crystallographic orientation.

Innovation Solution

The use of a plasma torch to transform spherical barium titanate ceramic particles into disk-like, anisometric particles with controlled crystallographic orientation, facilitated by thermal and kinetic energy and a precise cooling process, to produce high-quality ceramic seed templates.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If traditional chemical solution methods are used to fabricate ceramic templates, then crystal growth can be achieved, but the production speed is slow and yield is low

Engineering Contradiction:
Improveproduction speed and yieldVSAvoidfabrication time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

The patent replaces traditional chemical solution-based fabrication methods with a plasma spray physical field method. The plasma spray system uses thermal and kinetic energy from a plasma jet to directly transform spherical ceramic particles into disk-like structures with controlled crystallographic orientation, eliminating the need for slow chemical precipitation and post-fabrication processing steps, thereby dramatically increasing production speed and yield

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

Solution Approach 2:

The patent changes the fundamental processing parameters by using plasma spray technology to control particle temperature, velocity, and cooling rate. By adjusting plasma power, substrate temperature, and spray distance, the process directly forms disk-like particles with desired crystallographic orientation in a single step, achieving high productivity without time-consuming chemical processes

Inventive Principle:
Principle #35Parameter changes

2Manufacturing precision

If complex post-fabrication processing is used to achieve disk-like structure with specific crystallographic orientation, then desired template quality is obtained, but the process complexity increases

Engineering Contradiction:
Improvecrystallographic orientation controlVSAvoidprocess complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent performs preliminary action by pre-heating the substrate to a specific temperature range (600-900°C) before plasma spray deposition. This pre-conditioning of the substrate creates optimal conditions for controlling crystallographic orientation during particle deposition, eliminating the need for complex post-fabrication orientation control processes

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent replaces complex mechanical and chemical post-fabrication processing with a unified plasma spray physical field process. The plasma spray method directly imparts both the disk-like shape and crystallographic orientation in one step through controlled thermal and kinetic energy input, simplifying the overall process while maintaining manufacturing precision

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

3Shape

If spherical ceramic particles are used directly, then material simplicity is maintained, but the desired disk-like anisometric structure cannot be achieved

Engineering Contradiction:
Improvedisk-like anisometric structureVSAvoidparticle transformation complexity
Core Design Contradiction:
ShapeVSEase of manufacture

Solution Approach 1:

The patent utilizes phase transitions of ceramic particles under plasma conditions. The spherical particles are heated to melting or near-melting temperatures in the plasma jet, then rapidly cooled upon substrate deposition. This controlled phase transition from solid to molten and back to solid, combined with substrate temperature control, directly forms the desired disk-like anisometric structure with specific crystallographic orientation

Inventive Principle:
Principle #36Phase transitions

Solution Approach 2:

The patent changes physical parameters (temperature, velocity, cooling rate) of the ceramic particles during plasma spray processing. By controlling plasma power, spray distance, and substrate temperature, the process transforms spherical particles into disk-like structures with desired shape and orientation, achieving ease of manufacture through parameter optimization rather than complex mechanical processing

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This method enables the production of high-quality ceramic seed templates with a higher yield and unique configurations, overcoming the limitations of traditional methods by directly forming disk-like structures with desired crystallographic orientation.

Implementation Method 1

thermal and kinetic energy created from the use of a plasma torch

Methodology Applied
Scientific EffectThermal energy: Heating

Implementation Method 2

thermal and kinetic energy created from the use of a plasma torch

Methodology Applied
Scientific EffectKinetic energy: Impact Force

Implementation Method 3

a precise cooling process may promote crystal growth of a desired orientation

Methodology Applied
Scientific EffectCooling: Cooling

Implementation Method 4

systems and methods for plasma spray fabrication of textured ceramics

Methodology Applied
Scientific EffectPlasma spray: Plasma Spray

Data Source

PatentUS12338185B1Systems and methods for plasma spray fabrication of textured ceramics
Publication Date: 2025.06.24 THE UNITED STATES OF AMERICA AS REPRESENTED BY THE SECRETARY OF THE NAVY
  • US12338185B1 patent drawing
  • US12338185B1 patent drawing
  • US12338185B1 patent drawing

AI summary

Devices, systems and methods are provided to fabricate ceramic templates adapted for the production of textured ceramics. Embodiments may include a lidded canister loaded with ceramic particles, pressurized inert gas adapted to force the ceramic particles through the canister, a rotatable plate at an end of the canister, a particle tube connecting the end of the canister to a plasma torch, and a plasma arc at an end of the plasma torch heated to a temperature for melting the ceramic particles. A ceramic plasma spray may be generated that is adapted to coat a substrate with a non-equilibrium film, resulting in a ceramic template adapted for the production of textured ceramics.