Metal Plating Composition for Uniform Hole Filling

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Solution Overview

Problem

Metal plating processes face challenges in achieving uniform metal distribution, particularly in small-diameter holes of printed wiring boards, leading to potential mechanical and thermal failures due to insufficient metal layer thickness, which affects the reliability of electronic components.

Innovation Solution

The use of specific water-soluble compounds with a general formula H-A′p-Q-[C(O)—CH2O—((R1CH)t—O)z—CH2—C(O)—NH-A]u—H, where A′, A, R1, Q, p, r′, w′, x′, y′, r, w, x, y, t, u, and z are defined integers, is incorporated into metal plating compositions to enhance leveling and throwing power, ensuring uniform metal deposition.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Manufacturing precision

If conventional plating formulations are used, then the plating process is simple, but the metal layer thickness is non-uniform particularly in small-diameter holes

Engineering Contradiction:
Improvemetal layer thickness uniformityVSAvoidplating formulation complexity
Core Design Contradiction:
Manufacturing precisionVSDevice complexity

Solution Approach 1:

The patent modifies the chemical parameters of the plating formulation by incorporating specific compounds (polyamidoamines, ethoxylated dicarboxylic acids, ethoxylated diamines) with controlled molecular weights and functional groups. These parameter changes in the formulation chemistry enable improved metal ion transport into small-diameter holes while maintaining uniform deposition across the substrate surface.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention uses composite plating formulations that combine multiple functional components: levelers (polyamidoamines), brighteners (ethoxylated dicarboxylic acids), and carriers (ethoxylated diamines). This composite approach allows each component to perform its specific function synergistically, achieving uniform metal distribution in complex geometries including small-diameter holes while maintaining processability.

Inventive Principle:
Principle #40Composite materials

2Strength

If metal layer thickness is increased to prevent tearing, then mechanical strength is improved, but the plating uniformity deteriorates with smaller hole diameters

Engineering Contradiction:
Improvemetal layer mechanical strengthVSAvoidmetal plating distribution uniformity
Core Design Contradiction:
StrengthVSManufacturing precision

Solution Approach 1:

The patent applies local quality by using plating formulation components that selectively interact with different regions of the substrate. The levelers and brighteners in the formulation create locally optimized deposition conditions: they suppress excessive deposition on flat surfaces while promoting adequate filling of small-diameter holes and vias. This local differentiation enables achieving sufficient thickness in critical areas without compromising overall uniformity.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention introduces intermediary compounds (polyamidoamines, ethoxylated dicarboxylic acids) that act as mediators between the metal ions and the substrate surface. These intermediaries adsorb preferentially on certain surface features, modifying local electrochemical conditions to promote uniform current distribution. This mediation effect ensures adequate metal deposition in small holes while preventing excessive buildup on surfaces, thereby achieving both strength and uniformity.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Manufacturing precision

If conventional levelers are used (e.g., transformation products from epihalohydrins), then some leveling performance is achieved, but throwing power and overall plating performance remain insufficient

Engineering Contradiction:
Improveleveling performanceVSAvoidthermal reliability of metal layer
Core Design Contradiction:
Manufacturing precisionVSReliability

Solution Approach 1:

The patent changes the chemical parameters of conventional levelers by using polyamidoamines with specific molecular weight ranges (500-10,000) and controlled degrees of ethoxylation. These parameter modifications enhance not only leveling performance but also throwing power and thermal stability of the metal deposit. The specific structural parameters (amino group content, molecular weight) are optimized to achieve multiple performance targets simultaneously.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces single-function conventional levelers with composite formulations containing multiple synergistic components: polyamidoamines for leveling and adhesion, ethoxylated dicarboxylic acids for brightness and throw, and ethoxylated diamines for carrier functions. This composite approach enhances overall plating performance including thermal reliability, which cannot be achieved with conventional single-component levelers alone.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

These compounds improve the uniformity and thickness of metal layers in small-diameter holes, enhancing the thermal reliability and performance of metal-plated electronic components by optimizing the metal plating process.

Implementation Method 1

metal plating compositions and methods which provide improved leveling and throwing power

Methodology Applied
Scientific EffectElectroplating: Electroplating

Data Source

PatentUS8956523B2Metal plating compositions and methods
Publication Date: 2015.02.17 DUPONT ELECTRONIC MATERIALS INT LLC

AI summary

Disclosed are metal plating compositions and methods. The metal plating compositions provide good leveling performance and throwing power.