Platinum Molecular Sieve Catalyst Hydroisomerization

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Solution Overview

Problem

Existing methods for improving cold flow properties of hydrocarbon mixtures, such as diesel fuel, often result in yield loss and high hydrogen consumption due to side reactions during hydroisomerization, and traditional dewaxing methods are costly and inefficient.

Innovation Solution

A catalytically active material comprising platinum dispersed on a molecular sieve with a metal oxide support, where at least 80% of the platinum is in clusters smaller than 1 nm, and optionally including carbon and organic additives, is used for hydroisomerization, allowing for improved impregnation and selective deposition of platinum on the molecular sieve, enhancing dewaxing activity.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If catalytic hydroisomerization is used to improve cold flow properties, then yield and hydrogen consumption are improved compared to hydrocracking, but side reactions still occur causing yield loss and hydrogen consumption

Engineering Contradiction:
ImproveyieldVSAvoidyield loss
Core Design Contradiction:
ProductivityVSLoss of substance

Solution Approach 1:

The patent applies local quality by creating platinum clusters with specific size distributions (at least 80% with diameter ≤1 nm) dispersed on specific molecular sieve sites. This localized control of platinum cluster size and position enhances hydroisomerization selectivity while suppressing hydrocracking side reactions, thereby improving yield and reducing yield loss simultaneously

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent changes physical parameters by controlling platinum cluster size (diameter ≤1 nm) and dispersion density on the molecular sieve. These parameter changes optimize the catalytic activity for hydroisomerization while minimizing hydrocracking reactions, resolving the contradiction between productivity and substance loss

Inventive Principle:
Principle #35Parameter changes

2Reliability

If conventional catalysts are used for hydroisomerization, then dewaxing activity is achieved, but selectivity is low leading to excessive hydrogen consumption

Engineering Contradiction:
Improvedewaxing activityVSAvoidhydrogen consumption
Core Design Contradiction:
ReliabilityVSLoss of energy

Solution Approach 1:

The patent uses local quality by dispersing platinum specifically on molecular sieve sites with controlled cluster sizes (≤1 nm). This localized deposition ensures high dewaxing activity through effective platinum-molecular sieve interaction while suppressing non-selective hydrocracking reactions that consume excessive hydrogen

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent employs composite materials by combining platinum clusters with specific molecular sieves (such as ZSM-5, beta, or Y-type zeolites) and metal oxide supports. This composite structure synergistically enhances dewaxing activity while improving selectivity to reduce hydrogen consumption

Inventive Principle:
Principle #40Composite materials

3Reliability

If platinum is dispersed on molecular sieve for hydroisomerization, then catalytic activity is enhanced, but manufacturing complexity increases

Engineering Contradiction:
Improvecatalytic activityVSAvoidmanufacturing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent applies preliminary action by pre-synthesizing molecular sieves with specific pore structures and active sites before depositing platinum clusters. This preliminary preparation of the support structure facilitates controlled platinum dispersion and cluster formation, enhancing catalytic activity while managing manufacturing complexity through a structured multi-step process

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The catalytically active material demonstrates increased dewaxing activity and selectivity, reducing hydrogen consumption and yield loss, while maintaining high activity and thermal stability, thereby improving cold flow properties with enhanced efficiency.

Implementation Method 1

A catalytically active material comprising platinum dispersed on a molecular sieve with a metal oxide support, where at least 80% of the platinum is in clusters smaller than 1 nm

Methodology Applied
Scientific EffectCatalysis: Catalysis

Implementation Method 2

allowing for improved impregnation and selective deposition of platinum on the molecular sieve

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 3

a molecular sieve having a topology such as AEI, AEL, AFO, AFX, ATO, BEA, CHA, FAU, FER, MEL, MFI, MOR, MRE, MTT, MWW or TON

Methodology Applied
Scientific EffectMolecular sieve: Molecular Sieve

Implementation Method 4

The process requires the presence of hydrogen

Methodology Applied
Scientific EffectHydrogenation: Hydrogenation

Data Source

PatentUS11384296B2Hydroisomerization catalyst
Publication Date: 2022.07.12 HALDOR TOPSOE AS

AI summary

The present disclosure relates to a precursor for a catalytically active material or a catalytically active material comprising platinum, a molecular sieve and a metal oxide support, characterized in at least 80%, 90% or 95% of said platinum being dispersed on said molecular sieve and at least 80%, 90% or 95% of said platinum being dispersed in clusters having a size below 2 nm or 1 nm, as well as a method of producing such materials and process for hydroisomerization involving such materials. The disclosure has the associated benefit of such a catalytically active material being highly active and selective towards hydroisomerization.