Plug-flow ion-exchange resin regeneration process

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Solution Overview

Problem

Current ion-exchange resin regeneration processes are inefficient and costly, requiring large quantities of regenerant, resulting in significant waste and increased operational costs, and are limited by the size of regeneration vessels, which can restrict their use in water treatment due to space and equipment requirements.

Innovation Solution

A counter-current and plug flow regeneration system that uses multiple stages of regenerant vessels to regenerate ion-exchange resin more quickly and with less waste, allowing for continuous operation and reduced regenerant volumes, thereby improving efficiency and reducing environmental impact.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Loss of substance

If conventional batch regeneration processes are used, then resin can be regenerated, but large quantities of regenerant are required resulting in significant waste and increased operational costs

Engineering Contradiction:
Improveregenerant wasteVSAvoidregeneration efficiency
Core Design Contradiction:
Loss of substanceVSProductivity

Solution Approach 1:

The regeneration system is divided into multiple stages (first stage, second stage, third stage) with multiple vessels in each stage. This segmentation allows the regenerant to be distributed across different vessels and stages, improving contact efficiency with the resin and reducing overall regenerant consumption while maintaining effective regeneration.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The system enables continuous operation where resin can be continuously regenerated through the multi-stage process. Multiple vessels in parallel allow one vessel to be regenerated while others are in service, ensuring continuous useful action without interruption and reducing regenerant waste by eliminating batch-to-batch inefficiencies.

Inventive Principle:
Principle #20Continuity of useful action

2Area of stationary object

If conventional regeneration systems are used, then resin regeneration is possible, but the size of regeneration vessels is limited requiring large space and equipment

Engineering Contradiction:
Improvespace requirementVSAvoidregeneration capacity
Core Design Contradiction:
Area of stationary objectVSProductivity

Solution Approach 1:

By dividing the regeneration system into multiple smaller stages and vessels rather than one large vessel, the system achieves the same or greater regeneration capacity while reducing the footprint of individual equipment pieces. This modular segmentation allows flexible arrangement in limited spaces.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The multi-stage arrangement distributes the regeneration process across different spatial dimensions and sequences, allowing efficient use of available space through vertical or horizontal stacking of vessels, thereby reducing overall space requirements while maintaining high productivity.

Inventive Principle:
Principle #17Another dimension (Dimensionality change)

3Loss of time

If conventional batch regeneration is used, then resin can be regenerated, but the process is slow and time-consuming

Engineering Contradiction:
Improveregeneration timeVSAvoidregenerant consumption
Core Design Contradiction:
Loss of timeVSLoss of substance

Solution Approach 1:

The continuous multi-stage regeneration process eliminates idle time between batches and allows parallel processing in multiple vessels. Resin flows continuously through the regeneration stages, significantly reducing total regeneration time while the efficient contact in each stage minimizes regenerant consumption.

Inventive Principle:
Principle #20Continuity of useful action

Solution Approach 2:

The system performs preliminary regeneration actions in earlier stages that prepare the resin for final regeneration in subsequent stages. This preliminary action distributes the regeneration load across multiple stages, reducing the time required at each stage and overall, while optimizing regenerant usage through progressive treatment.

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The proposed system enables faster and more efficient regeneration of ion-exchange resin, reducing waste and operational costs, and allowing for increased use of resin systems in water treatment by minimizing space and equipment requirements.

Implementation Method 1

A counter-current and plug flow regeneration system that uses multiple stages of regenerant vessels to regenerate ion-exchange resin

Methodology Applied
Scientific EffectIon Exchange: Ion Exchange

Implementation Method 2

contacting the loaded resin within the vessel with first stage regenerant in a plug flow

Methodology Applied
Scientific EffectAdvection: Advection

Data Source

PatentUS7763666B2Plug-flow regeneration process
Publication Date: 2010.07.27 IXOM OPERATIONS
  • US7763666B2 patent drawing
  • US7763666B2 patent drawing
  • US7763666B2 patent drawing

AI summary

A process for the regeneration of loaded ion-exchange resin comprising (a) providing loaded resin for regeneration; (b) providing first stage and third stage regenerant suitable for regenerating loaded resin; (c) providing a plurality of regeneration vessels; (d) filling a regeneration vessel with a desired amount of the loaded resin before filling another regeneration vessel; (e) once a regeneration vessel has been filled, contacting the loaded resin within the vessel with first stage regenerant in a plug flow to provide a first stage regenerated resin; (f) contacting the first stage regenerated resin with third stage regenerant in a plug flow to provide regenerated resin and (g) removing and collecting third stage regenerant from a vessel containing regenerated resin and adding the collected regenerant to the first stage regenerant.