Polycrystalline Diamond Body Wear Resistance via Particle Segmentation

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Polycrystalline diamond bodies used in drilling operations face challenges with wear rate and life due to limitations in abrasion resistance, thermal stability, and impact toughness, leading to cracking and spalling.

Innovation Solution

A method of manufacturing polycrystalline diamond bodies by dispersing coarse diamond particles within a matrix of modified fine diamond particles and a binder phase, where the fine particles preferentially fracture during high-pressure high-temperature processing, maintaining the integrity of coarse particles and enhancing wear characteristics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional PCD compacts are used with uniform diamond particle distribution, then manufacturing is simpler, but abrasion resistance and impact toughness are insufficient leading to higher wear rates

Engineering Contradiction:
Improvewear resistanceVSAvoidmanufacturing complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The diamond particle population is segmented into distinct size fractions (coarse particles ≥10 micrometers and fine particles <10 micrometers) with different morphologies. The coarse particles provide wear resistance while the fine particles fill interstices and absorb impact energy, resolving the contradiction between wear resistance and manufacturing complexity by creating a functional gradient structure

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The patent creates a composite microstructure combining coarse diamond particles (for abrasion resistance) with fine diamond particles and binder phase (for toughness and energy absorption). This composite approach at the microstructural level achieves both high wear resistance and improved impact toughness without requiring complex manufacturing processes

Inventive Principle:
Principle #40Composite materials

2Reliability

If coarse diamond particles are used to improve abrasion resistance, then wear resistance improves, but impact toughness decreases leading to cracking and spalling

Engineering Contradiction:
Improveabrasion resistanceVSAvoidimpact toughness
Core Design Contradiction:
ReliabilityVSStrength

Solution Approach 1:

Different regions of the PCD compact have different local qualities: coarse diamond particles are distributed to provide abrasion resistance in high-wear zones, while fine particles and binder phase are positioned in regions requiring impact energy absorption. This local differentiation resolves the contradiction between abrasion resistance and impact toughness by optimizing particle distribution rather than using uniform composition

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent changes the particle size parameter distribution by incorporating a bi-modal or multi-modal size distribution with both coarse (≥10 μm) and fine (<10 μm) particles. This parameter change allows the material to exhibit both high abrasion resistance from coarse particles and high impact toughness from fine particles that can deform and absorb energy

Inventive Principle:
Principle #35Parameter changes

3Strength

If fine diamond particles are used to improve impact toughness, then energy absorption improves, but abrasion resistance decreases leading to higher wear rates

Engineering Contradiction:
Improveimpact toughnessVSAvoidabrasion resistance
Core Design Contradiction:
StrengthVSReliability

Solution Approach 1:

The diamond particle population is segmented into distinct size fractions with coarse particles (≥10 micrometers) providing abrasion resistance and fine particles (<10 micrometers) providing impact toughness. This segmentation allows each particle size fraction to perform its specialized function, resolving the contradiction between abrasion resistance and impact toughness

Inventive Principle:
Principle #1Segmentation

4Stability of the object's composition

If diamond particles are sintered at high pressure and temperature to improve bonding, then thermal stability improves, but particle fracture increases reducing toughness

Engineering Contradiction:
Improvethermal stabilityVSAvoidtoughness
Core Design Contradiction:
Stability of the object's compositionVSStrength

Solution Approach 1:

The patent performs preliminary action by pre-selecting a bi-modal or multi-modal particle size distribution before sintering, with coarse particles intended to maintain integrity and fine particles intended to fracture and absorb energy. This preliminary preparation ensures that during high-pressure high-temperature sintering, the fine particles will preferentially fracture to absorb energy while coarse particles maintain their structural integrity, resolving the contradiction between thermal stability and toughness

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in improved wear resistance and extended life of polycrystalline diamond bodies by preserving coarse particle integrity and increasing diamond phase density, reducing stress concentrations and promoting energy absorption, thereby reducing cracking and spalling.

Implementation Method 1

The polycrystalline diamond body may be formed in a high pressure high temperature (HPHT) process, in which diamond grains are held at pressures and temperatures at which the diamond particles bond to one another.

Methodology Applied
Scientific EffectSintering: Sintering

Implementation Method 2

the fine particles preferentially fracture during high-pressure high-temperature processing, maintaining the integrity of coarse particles

Methodology Applied
Scientific EffectFracture: Fracture Mechanics

Data Source

PatentEP3640226B1Method of making polycrystalline diamond bodies incorporating fractionated distribution of diamond particles of different morphologies
Publication Date: 2024.09.11 DIAMOND INNOVATIONS INC
  • EP3640226B1 patent drawingFigure 1~2B
  • EP3640226B1 patent drawingFigure 3A~3B
  • EP3640226B1 patent drawingFigure 4A~4B

AI summary

Diamond bodies and methods of manufacture are disclosed. Diamond bodies are ormed from at least a bimodal, alternatively a tri-modal or higher modal, feedstock having at east one fraction of modified diamond particles with a fine particle size (0.5-3.0 µm) and at east one fraction of diamond particles with coarse particle size (15.0 to 30 µm). During high pressure - high temperature processing, fine particle sized, modified diamond particles in the irst fraction preferentially fracture to smaller sizes while preserving the morphology of coarse particle sized diamond particles in the second fraction. Diamond bodies incorporating he two fractions have a microstructure including second fraction diamond particles dispersed n a continuous matrix of first fraction modified diamond particles and exhibit improved wear characteristics, particularly for wear associated with drilling of geological formations.