Polycrystalline Material with Alternating Grain Sizes

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Solution Overview

Problem

Polycrystalline layers exhibit high mechanical strain and stress due to increasing crystal grain size with layer thickness, which complicates subsequent processing and can lead to unfavorable deflections in components like MEMS elements.

Innovation Solution

The production of polycrystalline materials with alternating layers of different crystal grain sizes, where the layers of one type have a smaller average spatial extension than those of another type, is achieved by controlling the growth conditions such as temperature in a single or multiple chambers, allowing for low mechanical strain and stress even in thick materials.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Length of stationary object

If the layer thickness is increased to provide thicker polycrystalline materials, then the mechanical strain within the layer increases, but this is disadvantageous for subsequent processing and component manufacture

Engineering Contradiction:
Improvelayer thicknessVSAvoidmechanical strain
Core Design Contradiction:
Length of stationary objectVSStress or pressure

Solution Approach 1:

The polycrystalline layer is segmented into multiple sub-layers with different crystal grain sizes. By dividing the thick layer into thinner sub-layers (first type with smaller grains, second type with larger grains), the mechanical strain is reduced while maintaining the overall thickness. This segmentation allows the layer to be processed without excessive strain accumulation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

Different regions of the polycrystalline layer are given different crystal grain sizes to optimize local properties. The first type layers have smaller crystal grains for lower strain, while the second type layers have larger crystal grains for other beneficial properties. This local variation in quality allows the thick layer to maintain low overall mechanical strain.

Inventive Principle:
Principle #3Local quality

2Reliability

If the crystal grain size is increased to improve material properties, then the mechanical strain increases, but this complicates subsequent processing and causes unfavorable deflections in MEMS elements

Engineering Contradiction:
Improvematerial propertiesVSAvoidsubsequent processing
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The layer structure is segmented into alternating first type and second type layers with different crystal grain sizes. This segmentation prevents the uniform large grain size from causing excessive mechanical strain, thereby facilitating subsequent processing steps and preventing deflections in MEMS elements while still providing the benefits of polycrystalline structure.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The crystal grain size parameter is changed between different layers (smaller in first type, larger in second type) to optimize both material properties and mechanical strain. By controlling this parameter to vary periodically through the layer structure, the patent achieves reliable material properties without the harmful effects of uniformly large grains.

Inventive Principle:
Principle #35Parameter changes

3Adaptability or versatility

If the crystal grain size varies greatly within the layer, then the mechanical strain distribution becomes non-uniform, but this leads to unfavorable preliminary deflections in processed components

Engineering Contradiction:
Improvecrystal grain size variationVSAvoidmechanical strain distribution
Core Design Contradiction:
Adaptability or versatilityVSStability of the object's composition

Solution Approach 1:

The layer is segmented into alternating first type and second type layers, each with controlled crystal grain sizes. This segmentation creates a periodic, controlled variation in grain size rather than random or uncontrolled variation. The alternating structure ensures that strain distribution remains manageable and predictable, preventing unfavorable deflections.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The crystal grain size varies periodically through the layer structure, with first type layers (smaller grains) alternating with second type layers (larger grains). This periodic variation in grain size creates a controlled strain distribution pattern that prevents the non-uniform strain from causing unfavorable deflections in processed components.

Inventive Principle:
Principle #19Periodic action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach enables the creation of polycrystalline materials with reduced mechanical strain, suitable for semiconductor components and microelectromechanical systems, while allowing for precise control of crystal grain size and cost-effective production.

Implementation Method 1

crystallites having different preferred growth directions and increasing size are typically produced as a function of the grown layer thickness

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Implementation Method 2

the depositing and/or the growing of the layers of the first type and of the layers of the second type taking place in the chamber, at least one source gas being used for growing and/or depositing the layers of the first type and/or the layers of the second type, the arrangement for depositing and/or for growing including in particular an epitaxy unit

Methodology Applied
Scientific EffectEpitaxy: Epitaxy

Data Source

PatentUS10766778B2Polycrystalline material having low mechanical strain; method for producing a polycrystalline material
Publication Date: 2020.09.08 ROBERT BOSCH GMBH
  • US10766778B2 patent drawing
  • US10766778B2 patent drawing
  • US10766778B2 patent drawing

AI summary

A polycrystalline material having low mechanical strain is provided. The polycrystalline material includes one or multiple layers of a first type and one or multiple layers of a second type. The layers of the first type and the layers of the second type each include at least one polycrystalline material component. The layers of the first type have a smaller average crystal grain size than the layers of the second type, a layer of the first type and a layer of the second type being situated, at least in part, one above the other in an alternating sequence, and it being the case for the transition between the layers of the first type and the layers of the second type to be abrupt or continuous.