Enzymatic Polyester Degradation via Terephthalic Acid Buffering

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

Current enzymatic depolymerization processes for degrading polyester plastics, such as PET, face challenges with pH regulation and salt production, leading to high base and acid consumption, which increases costs and reduces the economic viability of the process.

Innovation Solution

Implementing a process where enzymatic depolymerization of polyester is performed at acidic conditions (pH 4-6) in a reaction medium with a high concentration of soluble terephthalic acid salts, eliminating the need for pH regulation and reducing base consumption, by maintaining the pH through a physicochemical equilibrium.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If enzymatic depolymerization is performed under conventional conditions with pH regulation, then enzyme activity is maintained, but base and acid consumption increases significantly leading to high costs and salt production

Engineering Contradiction:
Improveenzyme activityVSAvoidbase and acid consumption
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The reaction medium is designed to self-regulate pH through the buffer capacity provided by terephthalic acid and its salts, eliminating the need for external pH regulation. The system uses its own chemical components to maintain optimal conditions for enzyme activity without requiring additional base or acid additions.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The invention changes the pH parameter from regulated (maintained at optimal enzyme pH) to controlled through chemical equilibrium. By adjusting the ratio of terephthalic acid to its salts in the reaction medium, the pH is naturally maintained within the optimal range for enzyme activity without external intervention.

Inventive Principle:
Principle #35Parameter changes

2Productivity

If pH regulation is implemented to maintain optimal enzyme activity, then depolymerization efficiency is improved, but the complexity of the process increases due to continuous monitoring and adjustment requirements

Engineering Contradiction:
Improvedepolymerization efficiencyVSAvoidpH regulation system
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The reaction medium contains terephthalic acid and its salts in specific ratios that provide inherent buffer capacity, allowing the system to self-regulate pH without external control systems. This eliminates pH probes, dosing pumps, and control algorithms while maintaining optimal enzyme activity.

Inventive Principle:
Principle #25Self-service

Solution Approach 2:

The invention extracts the pH regulation function from the process control system and embeds it directly into the reaction medium chemistry. Instead of actively regulating pH through external systems, the buffering capacity is built into the chemical composition of the reaction medium itself.

Inventive Principle:
Principle #2Taking out (Extraction)

3Quantity of substance

If strong acid is used to recover terephthalic acid by precipitation, then terephthalic acid recovery is achieved, but huge production of valuable salts is avoided and cost increases

Engineering Contradiction:
Improveterephthalic acid recoveryVSAvoidsalt production
Core Design Contradiction:
Quantity of substanceVSLoss of substance

Solution Approach 1:

The invention converts the previously harmful effect of salt production into a beneficial buffer system. The salts that were considered waste products are now intentionally maintained in the reaction medium at controlled concentrations to provide pH buffering, transforming a disposal problem into a process advantage.

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

Solution Approach 2:

The invention changes the recovery approach from acid-induced precipitation to controlled crystallization by adjusting temperature and concentration parameters. Terephthalic acid is recovered by cooling and concentration rather than acid addition, preventing salt formation while maintaining high recovery efficiency.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach allows for efficient enzymatic depolymerization of polyester plastics with reduced base consumption and salt production, enhancing the economic and industrial feasibility of the process while maintaining enzyme activity.

Implementation Method 1

a main step of enzymatic depolymerization of said at least one polyester

Methodology Applied
Scientific EffectEnzymatic depolymerization: Enzyme

Implementation Method 2

enzymatic depolymerization of polyester is performed at acidic conditions (pH 4-6)

Methodology Applied
Scientific EffectHydrolysis: Hydrolysis

Implementation Method 3

eliminating the need for pH regulation and reducing base consumption, by maintaining the pH through a physicochemical equilibrium

Methodology Applied
Scientific EffectPhysicochemical equilibrium:

Data Source

PatentUS20240228731A1Process for degrading a plastic product comprising at least one polyester
Publication Date: 2024.07.11 CARBIOS

AI summary

The present invention relates to a process for degrading plastic products that comprises a step of enzymatic depolymerization implemented in acidic conditions at a pH between 4 and 6, in a reaction medium containing a defined amount of soluble equivalent terephthalic acid mostly in the form of salts.