Polyester Resin Can Coating Retort Resistance

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Solution Overview

Problem

Current polyester resins used for can coatings, such as polyvinyl chloride-based and epoxy-phenol-based resins, face issues with health hazards, environmental concerns, and inadequate performance in terms of processability, curability, retort resistance, and dent resistance, while existing polyester resin solutions do not adequately address these challenges.

Innovation Solution

A polyester resin is developed with a specific composition of terephthalic acid, 2,6-naphthalenedicarboxylic acid, ethylene glycol, and 1,2-propylene glycol, combined with a blocked isocyanate curing agent, to achieve high curability and resistance to retort, content, and dent impacts, ensuring excellent processability and stability.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If polyvinyl chloride-based resins are used as base resin for can coating, then retort resistance and content resistance are improved, but health safety deteriorates due to carcinogenic vinyl chloride monomer and toxic gas generation during incineration

Engineering Contradiction:
Improveretort resistanceVSAvoidhealth safety
Core Design Contradiction:
ReliabilityVSObject-affected harmful factors

Solution Approach 1:

The invention extracts and eliminates the harmful vinyl chloride monomer component from the resin system by replacing polyvinyl chloride-based resins with polyester-based resins that do not contain or generate carcinogenic substances, while maintaining the required retort resistance through alternative chemical composition

Inventive Principle:
Principle #2Taking out (Extraction)

Solution Approach 2:

The invention changes the chemical composition parameters by specifying precise copolymerization ratios of terephthalic acid (80-97.5 mol%), isophthalic acid (0-20 mol%), and sebacic acid (0-10 mol%), along with glycol component ratios, to achieve a resin system that provides both retort resistance and health safety without toxic gas generation

Inventive Principle:
Principle #35Parameter changes

2Strength

If epoxy-phenol-based resins are used as base resin for can coating, then adhesion to metal is improved, but processability deteriorates due to high baking temperature requirements causing foaming

Engineering Contradiction:
ImproveadhesionVSAvoidprocessability
Core Design Contradiction:
StrengthVSEase of manufacture

Solution Approach 1:

The invention changes the chemical composition parameters by using polyester-based resins with specific acid value ranges (15-80 mg KOH/g) and molecular weight characteristics that enable curing at lower temperatures (100-200°C) compared to epoxy-phenol resins, thereby improving processability and preventing foaming while maintaining adhesion through optimized resin structure

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention creates a composite resin system combining polyester base resin with specific curing agents and additives to achieve both good adhesion to metal surfaces and improved processability at lower baking temperatures, avoiding the foaming issues associated with high-temperature curing of epoxy-phenol resins

Inventive Principle:
Principle #40Composite materials

3Object-affected harmful factors

If polyester-based resins are used to replace harmful resins, then health safety and environmental compatibility are improved, but curability and processability deteriorate

Engineering Contradiction:
Improveenvironmental compatibilityVSAvoidcurability
Core Design Contradiction:
Object-affected harmful factorsVSReliability

Solution Approach 1:

The invention introduces specific curing agents as intermediaries that react with the polyester-based resin to achieve proper curability. The curing agents facilitate crosslinking and film formation at appropriate temperatures, enabling the environmentally friendly polyester system to achieve the necessary curability that pure polyester resins alone cannot provide

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention optimizes the molecular weight, acid value, and copolymerization ratio parameters of the polyester-based resin to balance environmental compatibility with curability. By controlling the resin's chemical structure parameters, the system achieves both health safety and adequate curability through proper formulation

Inventive Principle:
Principle #35Parameter changes

4Object-generated harmful factors

If polyester-based resins are used for can coating, then toxic gas generation during incineration is reduced, but dent resistance deteriorates

Engineering Contradiction:
Improvetoxic gas generationVSAvoiddent resistance
Core Design Contradiction:
Object-generated harmful factorsVSStrength

Solution Approach 1:

The invention creates a composite coating system using polyester-based resin combined with specific curing agents and functional additives that enhance dent resistance. This composite formulation maintains the environmental advantage of reduced toxic gas generation during incineration while compensating for the inherently lower dent resistance of polyester resins compared to traditional options

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The resulting coating film exhibits superior processability, curability, retort resistance, content resistance, and dent resistance, making it suitable for use in food and beverage cans without generating toxic gases during incineration and avoiding environmental hormone concerns.

Implementation Method 1

curability

Methodology Applied
Scientific EffectChemical reaction: Chemical Bonding

Implementation Method 2

retort resistance

Methodology Applied
Scientific EffectThermal resistance: Thermal Expansion

Implementation Method 3

dent resistance

Methodology Applied
Scientific EffectImpact resistance: Elasticity

Data Source

PatentUS10494542B2Polyester resin, resin composition for can paint, painted metal plate for can, and can
Publication Date: 2019.12.03 TOYOBO MC CORP

AI summary

This invention provides a polyester resin that is capable of forming a coating film having extremely excellent curability, processability, retort resistance, content resistance, and dent resistance, and also provides a resin composition for a coating composition containing the polyester resin. The polyester resin obtained from a polycarboxylic acid component and a polyol component, wherein the polyester resin meets the conditions (i) to iii) described below:(i) among the polycarboxylic acid components constituting the polyester resin, the total copolymerization ratio of terephthalic acid component and 2,6-naphthalenedicarboxylic acid component is 80 mol % or more;(ii) among the polycarboxylic acid components constituting the polyester resin, the copolymerization ratio of 2,6-naphthalenedicarboxylic acid component is 2 to 80 mol %; and(iii) among the polyol components constituting the polyester resin, the total copolymerization ratio of ethylene glycol component and 1,2-propylene-glycol component is 50 mol % or more, wherein the copolymerization ratio of 1,2-propylene-glycol component is excessive relative to the copolymerization ratio of the ethylene glycol component.