Closed-Cell PolyHIPE for Sustained Fertilizer Release

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Solution Overview

Problem

Existing polyHIPE-based systems for sustained release of fertilizers suffer from immediate and continuous exposure of the substance to the environment, leading to a sharp 'burst release' phase followed by a low trickle of the remaining substance, which is not sustainable or controllable.

Innovation Solution

A polyHIPE system with a closed-cell microstructure is developed, where a highly concentrated aqueous fertilizer solution or room temperature solid fertilizer is releasably entrapped. The release profile is controlled by selecting components for the polyHIPE, and degradable components can contribute to the controlled release mechanism.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Duration of action of moving object

If conventional fertilizer pellets with semi-permeable coatings are used, then the release rate can be slowed down, but the release profile shows an initial burst followed by a low trickle rather than sustained linear release

Engineering Contradiction:
Improverelease periodVSAvoidrelease profile control
Core Design Contradiction:
Duration of action of moving objectVSReliability

Solution Approach 1:

The invention employs polyHIPEs with controlled porosity (70-90% void volume) as the fertilizer carrier matrix. The porous structure provides high surface area for fertilizer incorporation while the pore size distribution and connectivity can be tuned to control diffusion rates, enabling sustained linear release profiles over extended periods without the burst-release phenomenon characteristic of conventional coated pellets.

Inventive Principle:
Principle #31Porous materials

Solution Approach 2:

The invention uses composite polymeric materials formed from HIPE templates, combining hydrophobic and hydrophilic polymer phases to create a bicontinuous porous structure. This composite material integrates both the structural framework and the fertilizer reservoir functions, with the ability to incorporate degradable polymers that further enhance controlled release through progressive matrix degradation.

Inventive Principle:
Principle #40Composite materials

2Duration of action of stationary object

If highly concentrated aqueous fertilizer solutions are entrapped in polyHIPEs, then sustained release over extended periods is achieved, but the system complexity increases compared to conventional pellets

Engineering Contradiction:
Improvesustained release periodVSAvoidsystem structure
Core Design Contradiction:
Duration of action of stationary objectVSDevice complexity

Solution Approach 1:

The invention pre-forms the polyHIPE matrix with its specific porous structure and incorporates the fertilizer solution during the polymerization process itself. This preliminary incorporation ensures uniform distribution of fertilizer throughout the matrix before deployment, eliminating the need for subsequent coating or encapsulation steps that would increase system complexity.

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The polyHIPE matrix serves multiple functions simultaneously: it provides the structural framework, acts as the fertilizer reservoir, controls the release rate through its porous structure, and can incorporate degradable components for enhanced controlled release. This multi-functionality reduces the need for separate components that would increase system complexity.

Inventive Principle:
Principle #6Universality (Multi-functionality)

3Reliability

If degradable components are incorporated into polyHIPEs, then controlled release mechanism is enhanced, but the manufacturing process becomes more complex

Engineering Contradiction:
Improvecontrolled release mechanismVSAvoidpolymerization process
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The invention combines the degradable polymer components with the primary polyHIPE matrix-forming polymers in a single polymerization reaction. The degradable polymers (such as polylactic acid, polyglycolic acid, or polyepsilon-caprolactone) are copolymerized or blended with the structural polymers during HIPE template polymerization, creating an integrated matrix where degradation and structural integrity work together to enable controlled release.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The closed-cell polyHIPE system achieves a sustained and controlled release of fertilizers over an extended period, avoiding the initial burst release phase and maintaining a substantially linear release profile, thus providing a more effective and sustainable fertilizer delivery system.

Implementation Method 1

The release profile is controlled by selecting components for the polyHIPE, and degradable components can contribute to the controlled release mechanism

Methodology Applied
Scientific EffectDiffusion: Diffusion

Implementation Method 2

degradable components can contribute to the controlled release mechanism

Methodology Applied
Scientific EffectDegradation: Decomposition (biological)

Implementation Method 3

a highly concentrated aqueous fertilizer solution or room temperature solid fertilizer is releasably entrapped

Methodology Applied
Scientific EffectPhysical containment: Physical Containment

Data Source

PatentEP3500622B1Polyhipe-based substance-releasing systems
Publication Date: 2025.04.09 TECHNION RES & DEV FOUND LTD
  • EP3500622B1 patent drawingFigure 1A~1D
  • EP3500622B1 patent drawingFigure 2A~2B
  • EP3500622B1 patent drawingFigure 3~4

AI summary

A polyHipe-based substance-releasing system capable of releasably encapsulating a highly concentrated solution and/or a room temperature solid while minimizing or avoiding burst release from the closed-cell micro structure of an elastic polyHIPE.