Aqueous Polymer Dispersion Durability via Swelling Agent Admixture

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Solution Overview

Problem

Existing compositions with polymer dispersed in water and polyvalent metal cations often have low levels of polyvalent cations, limiting their durability and effectiveness in applications like floor polishes, despite methods to increase cation levels being inefficient.

Innovation Solution

A composition comprising an aqueous polymer dispersion with a monomer mix containing 5-50% carboxylic acid functional monomers, 1-10 parts by weight of a swelling agent, and polyvalent metal ions, where the ratio of polyvalent metal ions to carboxylic acid functional groups is increased from 0.25 or less to 0.4 or more through a specific admixture process.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If the level of polyvalent metal cation is increased to improve coating durability, then the durability and hardness of the composition are improved, but the composition becomes less stable and more difficult to manufacture

Engineering Contradiction:
Improvecoating durabilityVSAvoidcomposition stability
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent applies preliminary action by first forming a preliminary admixture containing the polymer dispersion and swelling agent before adding the polyvalent metal cation. This sequential approach allows the polymer-swelling agent complex to form first, creating a stable intermediate structure that can then accommodate the metal cation without causing premature instability or difficulty in manufacturing.

Inventive Principle:
Principle #10Preliminary action

2Reliability

If a higher ratio of polyvalent metal ions to carboxylic acid functional groups is used to enhance durability, then the coating properties are improved, but the composition becomes less stable

Engineering Contradiction:
Improvecoating durabilityVSAvoidcomposition stability
Core Design Contradiction:
ReliabilityVSStability of the object's composition

Solution Approach 1:

The swelling agent acts as an intermediary between the polymer and the polyvalent metal cation. It forms a complex with the polymer first, creating a stable intermediate structure that can then bind the metal cation at higher ratios without causing composition instability. This intermediary role allows the system to achieve high durability while maintaining stability.

Inventive Principle:
Principle #24Intermediary (Mediator)

3Reliability

If conventional methods are used to increase polyvalent metal cation levels, then the coating durability is improved, but the manufacturing process becomes more complex and less efficient

Engineering Contradiction:
Improvecoating durabilityVSAvoidmanufacturing process complexity
Core Design Contradiction:
ReliabilityVSDevice complexity

Solution Approach 1:

The patent merges multiple functions into a single manufacturing step. By combining the polymer dispersion, swelling agent, and polyvalent metal cation in a controlled sequential process, the method achieves high metal cation incorporation without requiring separate complex processing steps, thus improving durability while keeping the manufacturing process relatively simple and efficient.

Inventive Principle:
Principle #5Merging (Combining)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The solution enhances the durability and effectiveness of the compositions by maintaining a higher ratio of polyvalent metal ions to carboxylic acid functional groups, improving properties such as hardness and durability in coatings like floor polishes.

Implementation Method 1

a process of forming a preliminary admixture of the dispersion (a) with some or all of the swelling agent (b)

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Implementation Method 2

the ratio of equivalents of polyvalent metal ions in the composition to equivalents of carboxylic acid functional groups in the composition is 0.4 or more

Methodology Applied
Scientific EffectComplexation: Chemical Bonding

Data Source

PatentUS7932313B2Aqueous compositions with polyvalent metal ions and dispersed polymers
Publication Date: 2011.04.26 ROHM & HAAS CO

AI summary

There is provided a composition comprising(a) at least one aqueous polymer dispersion, wherein said polymer is formed from a monomer mix comprising one or more carboxylic acid functional monomers;(b) at least one swelling agent; and(c) at least one polyvalent metal ion;wherein said composition is formed by a process comprising the step of forming a preliminary admixture of said dispersion (a) with some or all of said swelling agent (b), wherein the ratio of equivalents of polyvalent metal ions in said preliminary admixture to equivalents of carboxylic acid functional groups in said preliminary admixture is 0.25 or less.