Granular Polymer Drying via Vacuum and Microwave Segmentation

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Solution Overview

Problem

Traditional drying processes for granular polymeric materials, such as PET, PA, and PC, are energy-intensive and prone to oxidation and degradation due to high temperatures, and they lack operational flexibility due to long production change times, which increases the overall cost and reduces the quality of the molded products.

Innovation Solution

A two-step drying process involving dehumidification at a low temperature followed by vacuum drying, with the use of small hoppers and high vacuum levels, and post-heating with microwaves in an inert atmosphere to achieve efficient energy use and prevent degradation, allowing for rapid production changes.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If traditional high temperature drying is used, then drying efficiency is improved, but energy consumption increases and material degradation occurs

Engineering Contradiction:
Improvedrying efficiencyVSAvoidenergy consumption
Core Design Contradiction:
ProductivityVSUse of energy by moving object

Solution Approach 1:

The drying process is divided into multiple stages with different temperature profiles. The first stage uses high temperature for rapid moisture removal, while subsequent stages use progressively lower temperatures to complete drying without excessive energy input or material degradation. This segmentation allows the system to achieve high drying efficiency while controlling energy consumption.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The drying temperature is dynamically adjusted throughout the process based on moisture content and material sensitivity. By changing the temperature parameter over time rather than maintaining a constant high temperature, the system achieves effective drying while reducing overall energy consumption and preventing thermal degradation of the polymeric material.

Inventive Principle:
Principle #35Parameter changes

2Speed

If high temperature drying is used, then drying speed is improved, but material oxidation and degradation worsen

Engineering Contradiction:
Improvedrying speedVSAvoidoxidation and degradation
Core Design Contradiction:
SpeedVSObject-affected harmful factors

Solution Approach 1:

An inert gas atmosphere (such as nitrogen or recycled dried air) is maintained throughout the drying process to replace oxygen. This prevents oxidation reactions while allowing high temperature drying to proceed at high speed. The inert environment eliminates the harmful oxidative effect while preserving the beneficial high drying rate.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Solution Approach 2:

The drying process is segmented into stages where early high-temperature stages operate in controlled inert atmosphere for rapid moisture removal, followed by lower temperature stages that complete drying with minimal oxidation risk. This segmentation allows high drying speed in the critical early phase while preventing degradation in later phases.

Inventive Principle:
Principle #1Segmentation

3Productivity

If large hoppers are used, then production capacity is improved, but production change time increases

Engineering Contradiction:
Improveproduction capacityVSAvoidproduction change time
Core Design Contradiction:
ProductivityVSLoss of time

Solution Approach 1:

Multiple smaller drying zones or modules are arranged within the hopper structure, allowing parallel processing of different material batches. When a production change is required, only the relevant zone needs to be cleared and reconfigured, while other zones continue operating. This nested arrangement maintains high production capacity while reducing changeover time.

Inventive Principle:
Principle #7Nested doll (Nesting)

Solution Approach 2:

The hopper system incorporates movable partitions or adjustable configurations that allow dynamic reconfiguration for different production runs. This enables rapid switching between different polymeric materials without requiring complete emptying and cleaning of large volumes, thus reducing production change time while maintaining high capacity.

Inventive Principle:
Principle #15Dynamics

4Use of energy by moving object

If granular material is heated to high temperature, then energy efficiency of working machine is improved, but material stability deteriorates

Engineering Contradiction:
Improveenergy efficiency of working machineVSAvoidmaterial stability
Core Design Contradiction:
Use of energy by moving objectVSStability of the object's composition

Solution Approach 1:

The granular polymeric material is heated to high temperatures in an inert gas atmosphere that prevents oxidation and chemical degradation. This allows the material to reach optimal processing temperature for energy-efficient working machine operation while the inert environment protects material stability throughout the heating and storage period.

Inventive Principle:
Principle #39Inert atmosphere (Inert environment)

Solution Approach 2:

The inert atmosphere protection is maintained continuously from the drying phase through the heating phase and into the working machine feed system. This continuous protective environment ensures material stability is preserved throughout the entire high-temperature exposure period, enabling sustained energy-efficient operation without degradation risks.

Inventive Principle:
Principle #20Continuity of useful action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach significantly reduces energy consumption, minimizes oxidation, and enhances operational flexibility by achieving high drying efficiency with lower residual humidity levels and maintaining the material at optimal temperatures for processing, thereby improving the quality and reducing production time.

Implementation Method 1

The granular polymeric material is then dried by introducing a second flow of gas, formed of recirculated air, heated to a second temperature, higher than the first temperature, corresponding to the maximum temperature at which the granular polymeric material can be maintained in air

Methodology Applied
Scientific EffectVacuum: Vacuum

Implementation Method 2

Alternative drying processes require the granular polymeric material to be subjected to a predetermined degree of depressurisation (vacuum) so as to help the stripping of water from the granules at relatively low temperatures

Methodology Applied
Scientific EffectDepressurisation: Depressurisation

Implementation Method 3

said granular polymeric material is post-heated by irradiation with microwaves

Methodology Applied
Scientific EffectMicrowave radiation: Microwave Radiation

Implementation Method 4

a second flow of gas, formed of recirculated air, heated to a second temperature, higher than the first temperature

Methodology Applied
Scientific EffectConvection: Convection

Data Source

PatentEP3961137B1Process for drying granular polymeric material and plant operating according to said process
Publication Date: 2024.07.10 PEGASO IND SPA
  • EP3961137B1 patent drawingFigure 1

AI summary

A process for drying granular polymeric material, comprising the steps of: - dehumidifying the granular polymeric material by means of a first flow of gas at a first temperature of between 100°C and 150°C; - heating the dehumidified granular polymeric material to a second temperature, greater than the first temperature; - drying the granular polymeric material heated to the second temperature, by applying a predefined vacuum level in a drying hopper (30) that is separated from the other hoppers, both upstream and downstream, by pressure-sealing elements. The pressure-sealing elements comprise a filling unit, which includes a small tank (36a) blocked upstream and downstream by shut-off valves (36b, 36c), as well as a discharge unit, which includes a small tank (37a) blocked upstream and downstream by respective shut-off valves (37b, 37c)