Polymer-Supported Hexacyanoferrate Adsorbent for Cesium Removal

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Solution Overview

Problem

Existing adsorbents for Cs+ ions, particularly radiotoxic 137Cs+, face issues with mechanical and chemical stability, leading to pressure losses and reduced effectiveness in adsorption devices due to swelling and fragmentation, and require expensive aging treatments.

Innovation Solution

A method using polymer-based spherical activated carbon as a support for precipitating inorganic hexacyanoferrate(II) or hexacyanoferrate(III) adsorbents, which provides high mechanical and chemical stability, reducing pressure losses and maintaining effectiveness across a wide pH range.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional adsorbents (zeolites, granular activated carbon) are used for Cs+ adsorption, then adsorption capacity can be achieved, but mechanical stability deteriorates leading to swelling, fragmentation, and pressure losses

Engineering Contradiction:
Improvemechanical stabilityVSAvoidfragmentation and pressure losses
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent combines polymer-based spherical activated carbon (providing mechanical strength and stability) with inorganic precipitate ( providing Cs+ adsorption capacity). This composite structure integrates the advantages of both materials: the polymer carrier prevents swelling and fragmentation while the inorganic component maintains high adsorption selectivity for cesium ions.

Inventive Principle:
Principle #40Composite materials

2Reliability

If expensive aging treatments are applied to improve adsorbent performance, then adsorption effectiveness is enhanced, but manufacturing cost increases

Engineering Contradiction:
Improveadsorption effectivenessVSAvoidmanufacturing cost
Core Design Contradiction:
ReliabilityVSEase of manufacture

Solution Approach 1:

The patent incorporates functional groups directly into the polymer-based activated carbon carrier during manufacturing, eliminating the need for subsequent expensive aging treatments. The carrier is pre-functionalized with groups that provide both mechanical stability and adsorption capacity, allowing the adsorbent to achieve optimal performance immediately upon use.

Inventive Principle:
Principle #10Preliminary action

3Adaptability or versatility

If inorganic precipitate is used for Cs+ adsorption, then selectivity is improved, but chemical stability deteriorates limiting pH spectrum

Engineering Contradiction:
ImproveCs+ selectivityVSAvoidpH stability
Core Design Contradiction:
Adaptability or versatilityVSStability of the object's composition

Solution Approach 1:

The patent creates a composite where the polymer-based activated carbon carrier provides chemical stability across a wide pH range, while the inorganic precipitate component provides selective Cs+ adsorption. The polymer matrix protects the inorganic precipitate from pH-induced degradation, enabling the adsorbent to maintain both selectivity and stability in acidic and alkaline conditions.

Inventive Principle:
Principle #40Composite materials

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The adsorbent achieves high compressive strength, abrasion resistance, and chemical stability, minimizing carrier fragmentation and pressure drops, while maintaining Cs+ adsorption capacity and pH stability, thus enhancing the performance and durability of adsorption devices.

Implementation Method 1

the adsorbent is an inorganic precipitate capable of adsorbing a metal cation or a mixture of metal cations from a liquid, preferably aqueous, medium

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

DE 40 21 046 A1 describes a Cs+ adsorbent in which a zeolite is equipped with a ferrocyanide component by ion exchange

Methodology Applied
Scientific EffectIon exchange: Ion Exchange

Implementation Method 3

the carrier consists of a polymer-based spherical activated carbon and the adsorbent is an inorganic precipitate

Methodology Applied
Scientific EffectMechanical support:

Implementation Method 4

precipitation of an inorganic adsorbent capable of adsorbing Cs+ ions onto a support

Methodology Applied
Scientific EffectPrecipitation: Precipitation

Data Source

PatentEP2744592B1Adsorbent precipitated on a carrier, method for producing said adsorbent, and use of said adsorbent
Publication Date: 2015.03.18 BLUCHER GMBH
  • EP2744592B1 patent drawingFigure 1
  • EP2744592B1 patent drawingFigure 2

AI summary

The invention relates to an adsorbent precipitated on a carrier and to a method for producing said adsorbent. The carrier comprises a polymer-based spherical activated charcoal. The adsorbent comprises an inorganic precipitate capable of adsorbing a metal cation or a mixture of metal cations from a liquid, preferably aqueous, medium. The adsorbent precipitated on a carrier is used to remove, for example, Cs+ from water containing Cs+, in particular from water contaminated with radiotoxic 137Cs+.