Poly(ether-phosphoramide) Polymer for Rare Earth Extraction

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Solution Overview

Problem

Existing methods for extracting rare earths from aqueous media are inefficient and environmentally harmful due to their reliance on organic solvents.

Innovation Solution

A polymer from the poly(ether-phosphoramide) family with a specific structure, which has a high affinity for rare earths such as lanthanum and cerium, is used in a solid-phase extraction process. This polymer is either used in powder form or integrated into a composite material on a solid support.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Productivity

If liquid-liquid extraction technique using organic solvents is used, then extraction efficiency is improved, but environmental harm and solvent disposal problems worsen

Engineering Contradiction:
Improveextraction efficiencyVSAvoidenvironmental harm
Core Design Contradiction:
ProductivityVSObject-affected harmful factors

Solution Approach 1:

The invention changes the phase parameter of the extraction system from liquid-liquid to solid-liquid by using a polymer in aqueous phase instead of organic solvents, maintaining extraction efficiency while eliminating environmental harm associated with organic solvent disposal

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention employs a composite polymer material with specific functional groups (phosphoramide, ether) that combines high extraction efficiency for rare earth elements with environmental compatibility, replacing the need for harmful organic solvents

Inventive Principle:
Principle #40Composite materials

2Object-affected harmful factors

If solid-liquid extraction techniques are used to avoid organic solvents, then environmental harm is reduced, but extraction performance deteriorates

Engineering Contradiction:
Improveenvironmental harmVSAvoidextraction performance
Core Design Contradiction:
Object-affected harmful factorsVSProductivity

Solution Approach 1:

The invention introduces specific functional groups (phosphoramide and ether groups) at local sites on the polymer chain that have high affinity for rare earth elements, enabling solid-liquid extraction to achieve performance comparable to or exceeding liquid-liquid extraction methods

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The invention optimizes parameters including polymer molecular weight, functional group density, and aqueous phase composition to maximize extraction performance while maintaining the environmental benefits of solvent-free operation

Inventive Principle:
Principle #35Parameter changes

3Productivity

If polymer with high rare earth affinity is used, then extraction rate is improved, but polymer structure complexity increases

Engineering Contradiction:
Improveextraction rateVSAvoidpolymer structure complexity
Core Design Contradiction:
ProductivityVSDevice complexity

Solution Approach 1:

The polymer structure incorporates multiple functional groups (phosphoramide and ether) that work synergistically to provide high extraction rate for multiple rare earth elements simultaneously, achieving universal applicability without excessive structural complexity

Inventive Principle:
Principle #6Universality (Multi-functionality)

Solution Approach 2:

The invention places specific functional groups at strategic positions along the polymer chain to maximize their interaction with rare earth ions while maintaining overall structural simplicity and ease of synthesis

Inventive Principle:
Principle #3Local quality

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The polymer achieves a high extraction rate of rare earths from liquid media, with reversible adsorption and simple desorption in the aqueous phase, thereby overcoming the limitations of previous methods.

Implementation Method 1

The adsorption of rare earths on this polymer is also reversible

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

a polymer of specific structure, from the poly(ether-phosphoramide) family, which has a particularly high affinity for rare earths

Methodology Applied
Scientific EffectComplexation: Chemical Bonding

Implementation Method 3

The adsorption of rare earths on this polymer is also reversible, and their desorption is simple to carry out

Methodology Applied
Scientific EffectDesorption: Desorption

Data Source

PatentEP4559952A1Novel poly(ether-phosphoramide) polymer and method for extracting rare earth from a liquid medium using such a polymer
Publication Date: 2025.05.28 CENT NAT DE LA RECH SCI (C N R S)
  • EP4559952A1 patent drawingFigure 1
  • EP4559952A1 patent drawingFigure 2
  • EP4559952A1 patent drawingFigure 3a~4

AI summary

The invention relates to a poly(ether-phosphoramide) polymer, a repeating unit of which comprises an isosorbide unit and a phosphoramide function, and which has a high affinity for rare earths, in particular lanthanum and cerium. This polymer is particularly useful for carrying out the extraction of a rare earth from an aqueous liquid medium containing it, such as a mining effluent, by a solid-liquid extraction method.