Polymeric Material Solid State Drawing Nanopores

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Solution Overview

Problem

Conventional foaming processes for producing low density polymeric materials result in low molecular orientation, mechanical weakness, and large cell sizes, limiting their application in high-speed production processes due to strain hardening constraints and poor pore distribution.

Innovation Solution

A thermoplastic composition with a continuous phase containing a matrix polymer and an ultrahigh molecular weight siloxane polymer, dispersed as discrete domains, is subjected to solid state drawing to create a porous network with nanopores, enhancing mechanical strength and pore distribution.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If conventional foaming processes are used to produce low density polymeric materials, then the material density is reduced, but the molecular orientation is low and mechanical strength is compromised

Engineering Contradiction:
Improvematerial densityVSAvoidmechanical strength
Core Design Contradiction:
Quantity of substanceVSStrength

Solution Approach 1:

The patent changes the physical state parameter from molten to solid state during the foaming process. By initiating pore formation in the solid state rather than the molten state, the polymer chains maintain molecular orientation and strain hardening capability, thereby achieving both low density and high mechanical strength simultaneously

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent performs preliminary molecular orientation and crystallization in the solid state before pore formation. This preliminary action establishes a structured polymer matrix that can withstand the mechanical stress of pore creation while maintaining strength, rather than forming pores in a disordered molten state

Inventive Principle:
Principle #10Preliminary action

2Quantity of substance

If typical foaming processes are used, then pore structure is created through the bulk, but cell sizes become large (greater than 100 μm)

Engineering Contradiction:
Improvepore volumeVSAvoidpore size control
Core Design Contradiction:
Quantity of substanceVSManufacturing precision

Solution Approach 1:

The patent introduces a nucleating agent that creates localized pore formation sites throughout the polymer matrix. This local quality approach ensures uniform distribution of small nanopores (0.1-10 μm) rather than large cells, by concentrating pore initiation at specific nucleation points that are evenly dispersed throughout the material

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent uses a nucleating agent as an intermediary substance that mediates between the polymer matrix and the pore structure. This nucleating agent provides controlled sites for pore formation, enabling precise control over pore size and distribution while maintaining overall material integrity

Inventive Principle:
Principle #24Intermediary (Mediator)

3Quantity of substance

If large cell sizes are generated during foaming, then pore structure is established, but melt strength is reduced causing breaks in high speed production

Engineering Contradiction:
Improvepore contentVSAvoidproduction speed
Core Design Contradiction:
Quantity of substanceVSProductivity

Solution Approach 1:

The patent changes the physical state parameter to solid state during foaming, which maintains melt strength and prevents breaks in high speed production processes. The solid state structure provides mechanical integrity that allows the material to withstand the stresses of rapid processing while still forming the desired porous structure

Inventive Principle:
Principle #35Parameter changes

4Quantity of substance

If foaming occurs in molten state, then pore formation is achieved, but strain hardening is prevented

Engineering Contradiction:
Improvepore structureVSAvoidstrain hardening
Core Design Contradiction:
Quantity of substanceVSStability of the object's composition

Solution Approach 1:

The patent changes the physical state parameter from molten to solid state, which enables strain hardening to occur during pore formation. The solid state allows polymer chains to orient and harden under stress, providing both pore structure and enhanced mechanical stability simultaneously

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The approach results in a polymeric material with a stable porous network, improved mechanical strength, and controlled pore size distribution, enabling the production of materials with reduced density and enhanced thermal resistance.

Implementation Method 1

an ultrahigh molecular weight siloxane polymer having a weight average molecular weight of about 100,000 grams per mole or more that is dispersed within the continuous phase in the form of discrete domains

Methodology Applied
Scientific EffectPhase separation:

Implementation Method 2

A porous network is defined within the thermoplastic composition that includes a plurality of nanopores

Methodology Applied
Scientific EffectPorous network formation: Porosity

Implementation Method 3

solid state drawing the thermoplastic composition to form a porous network therein

Methodology Applied
Scientific EffectSolid state deformation: Deformation

Implementation Method 4

enhanced thermal resistance

Methodology Applied
Scientific EffectThermal resistance: Thermal Insulation

Data Source

PatentEP3577162B1Polymeric material
Publication Date: 2023.11.29 KIMBERLY CLARK WORLDWIDE INC
  • EP3577162B1 patent drawingFigure 1
  • EP3577162B1 patent drawingFigure 2
  • EP3577162B1 patent drawingFigure 3

AI summary

A polymeric material that includes a thermoplastic composition containing a continuous phase that includes a matrix polymer and a siloxane component is provided. The siloxane component contains an ultrahigh molecular weight siloxane polymer that is dispersed within the continuous phase in the form of discrete domains. A porous network is defined within the thermoplastic composition that includes a plurality of nanopores.