Water-Soluble Polymeric Dyes for Aggregation-Resistant Fluorescence

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Solution Overview

Problem

Existing fluorescent dyes face challenges in achieving high solubility in water and are prone to aggregation, which affects their fluorescence and spectroscopic properties, limiting their effectiveness in biological assays.

Innovation Solution

Development of water-soluble polymeric dyes with branched non-ionic water-soluble groups and a signaling chromophore covalently linked to a light harvesting multichromophore, enhancing solubility and resistance to aggregation, thereby improving fluorescence and spectroscopic performance.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If conventional fluorescent dyes are used, then fluorescence function is provided, but water solubility is poor and aggregation occurs

Engineering Contradiction:
Improvewater solubilityVSAvoidaggregation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent creates a composite structure by conjugating a water-soluble polymer (such as polyethylene glycol or polyvinyl alcohol) with a fluorescent dye molecule. This composite material combines the fluorescence properties of the dye with the water solubility and aggregation-resistance properties of the polymer, resolving the contradiction between providing fluorescence function and achieving water solubility without aggregation.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The water-soluble polymer acts as an intermediary between the fluorescent dye and the aqueous environment. The polymer chain serves as a mediator that provides hydrophilic interactions with water while simultaneously separating multiple dye molecules to prevent aggregation, thus enabling the dye to function in water-based biological assays.

Inventive Principle:
Principle #24Intermediary (Mediator)

2Illumination intensity

If dye concentration is increased to improve signal intensity, then fluorescence signal brightness increases, but aggregation occurs which degrades fluorescence properties

Engineering Contradiction:
Improvefluorescence signal brightnessVSAvoidfluorescence stability
Core Design Contradiction:
Illumination intensityVSReliability

Solution Approach 1:

The patent segments the dye molecules apart from each other by attaching them to individual polymer chains. Each polymer chain acts as a separate carrier for the fluorescent dye, physically separating multiple dye molecules and preventing their aggregation even at high concentrations. This segmentation allows high fluorescence signal brightness without the degradation caused by aggregation.

Inventive Principle:
Principle #1Segmentation

Solution Approach 2:

The water-soluble polymer forms a flexible hydrophilic shell or solvation layer around the fluorescent dye molecule. This protective shell prevents direct contact and aggregation between multiple dye molecules, allowing the system to achieve high fluorescence intensity through increased dye loading while maintaining fluorescence stability and preventing aggregation-related degradation.

Inventive Principle:
Principle #30Flexible shells and thin films

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The water-soluble polymeric dyes exhibit enhanced solubility and resistance to aggregation, providing brighter fluorescence signals suitable for applications like flow cytometry and imaging, with improved excitation and emission wavelength options.

Implementation Method 1

branched non-ionic water soluble groups (WSG) comprising two or more water soluble polymers... capable of imparting solubility in water in excess of 50 mg/mL

Methodology Applied
Scientific EffectSolvation: Solvation

Implementation Method 2

Fluorescent dyes are compounds which, when irradiated with light of a wavelength which they absorb, emit light of a (usually) different wavelength

Methodology Applied
Scientific EffectFluorescence: Fluorescence

Implementation Method 3

a signaling chromophore covalently linked to the multichromophore in energy-receiving proximity therewith

Methodology Applied
Scientific EffectEnergy transfer:

Data Source

PatentEP4682210A1Water-soluble polymeric dyes
Publication Date: 2026.01.21 BECTON DICKINSON & CO
  • EP4682210A1 patent drawingFigure 1
  • EP4682210A1 patent drawingFigure 1
  • EP4682210A1 patent drawingFigure 2

AI summary

Water soluble polymeric dyes and polymeric tandem dyes are provided. The polymeric dyes include a water solvated light harvesting multichromophore having a conjugated segment of aryl or heteroaryl co-monomers including branched non-ionic water soluble groups (WSG) comprising two or more water soluble polymers. In some cases, the branched non-ionic water soluble groups (WSG) of the present disclosure are capable of imparting solubility in water in excess of 50 mg/mL to the multichromophore. The polymeric tandem dyes further include a signaling chromophore covalently linked to the multichromophore in energy-receiving proximity therewith. Also provided are aggregation-resistant labelled specific binding members that include the subject water soluble polymeric dyes. Methods of evaluating a sample for the presence of a target analyte and methods of labelling a target molecule in which the subject polymeric dyes find use are also provided. Systems and kits for practicing the subject methods are also provided.