Polymerization Flush Medium Switching to Reduce Inert Gas Loss

Resolve Bottlenecks,
Find Innovative Solutions
Generate Solutions

Solution Overview

Problem

In polymerization processes, existing flushing methods using inert gases like nitrogen can lead to significant losses of valuable materials due to their similar molecular weight and the need for extensive purging, which is inefficient and costly.

Innovation Solution

The process involves using different flush mediums at different times, switching from an inert gas to a non-inert gas, such as the monomer being polymerized, to minimize fouling and reduce purge requirements, allowing for increased flush rates without excessive inert gas usage.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If inert gas (nitrogen) is used as flush medium, then the polymerisation reaction is not affected, but significant losses of valuable materials occur due to purging requirements

Engineering Contradiction:
Improvepolymerisation reaction stabilityVSAvoidvaluable material loss
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The patent changes the chemical nature parameter of the flush medium from inert gas to reactive monomer gas, transforming it from a non-participating substance to one that actively engages in polymerisation reactions, thereby eliminating the need for purging and preventing material losses

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent converts the previously harmful effect of flush medium accumulation (which required purging and caused material loss) into a beneficial effect where the monomer gas participates in polymerisation reactions, utilizing what would have been waste material for productive purposes

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

2Reliability

If high flush rates are used to prevent polymer build-up, then fouling is prevented, but excessive inert gas consumption occurs

Engineering Contradiction:
Improvefouling preventionVSAvoidinert gas consumption
Core Design Contradiction:
ReliabilityVSLoss of substance

Solution Approach 1:

The monomer gas performs a dual function: it serves as the flush medium to prevent polymer build-up in lines and connections, and simultaneously serves as reactant material for the polymerisation process, making the system self-sufficient and eliminating the need for separate inert gas supply

Inventive Principle:
Principle #25Self-service

3Reliability

If inert gas is used for flushing connections, then polymer contact with seals is prevented, but the inert gas builds up to high levels requiring extensive purging

Engineering Contradiction:
Improveseal protectionVSAvoidinert gas accumulation
Core Design Contradiction:
ReliabilityVSQuantity of substance

Solution Approach 1:

The patent changes the chemical reactivity parameter of the flush medium from zero (inert gas) to high (monomer gas), enabling the flush medium to participate in polymerisation reactions and preventing accumulation that would require purging

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

This approach reduces the amount of inert gas needed for purging, minimizes losses of valuable components, and allows for higher flush rates during production, thereby optimizing the polymerization process efficiency and reducing material losses.

Implementation Method 1

a flush medium which enters the polymerisation system, wherein initially said component is flushed with a first flush medium

Methodology Applied
Scientific EffectFluid flow:

Data Source

PatentUS9868802B2Polymerisation process
Publication Date: 2018.01.16 INEOS EUROPE AG

AI summary

Polymerization process for the polymerization of monomer in a polymerization system having at least one component attached thereto which component is flushed with a flush medium which enters the polymerization system. Initially, the component is flushed with a first flush medium, and subsequently the component is flushed with a second flush medium.