Polyol Ester Lubricant for Fluorinated Olefin Refrigerants

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Solution Overview

Problem

Existing refrigeration systems face challenges with phase separation and viscosity reduction due to the miscibility of fluorinated olefin refrigerants with traditional polyol ester lubricants, leading to decreased performance and efficiency, especially when using hydrofluoro-olefin refrigerants like R-1234ze.

Innovation Solution

A polyol ester lubricant composition with a specific blend of alkylcarboxy esters of pentaerythritol, di-pentaerythritol, and tri-pentaerythritol oligomers, optimized to maintain high viscosity and miscibility with hydrofluoro-olefin refrigerants across a wide temperature range, preventing excessive refrigerant solubility and phase separation.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Reliability

If traditional polyol ester lubricants are used with fluorinated olefin refrigerants, then the lubricant provides good low temperature flow properties and thermal stability, but the refrigerant excessively dissolves in the lubricant causing viscosity reduction and phase separation

Engineering Contradiction:
Improvelubricant stabilityVSAvoidviscosity reduction
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The patent modifies the chemical composition parameters of the polyol ester lubricant by specifying precise weight percentage ranges of different ester components (monoesters 20-40%, diesters 10-30%, triesters 30-60%, oligomers 5-20%). This compositional parameter optimization reduces refrigerant solubility while maintaining low-temperature flow properties and thermal stability, preventing excessive viscosity reduction.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates a composite lubricant formulation by blending multiple polyol ester types (monoesters, diesters, triesters, and oligomers) with specific molecular weight ranges and structural characteristics. This composite approach balances miscibility control with lubrication performance, preventing phase separation while maintaining reliability across operating temperatures.

Inventive Principle:
Principle #40Composite materials

2Ease of operation

If the lubricant viscosity is reduced to improve flow properties, then low temperature operation is enhanced, but lubrication effectiveness and wear protection deteriorate

Engineering Contradiction:
Improveflow propertiesVSAvoidwear protection
Core Design Contradiction:
Ease of operationVSReliability

Solution Approach 1:

The patent applies local quality by assigning different functional roles to specific lubricant components: lighter monoesters and diesters provide low-temperature flow enhancement, while heavier triesters and oligomers maintain viscosity and wear protection at operating temperatures. This distributed functional approach optimizes both flow properties and lubrication effectiveness across the temperature range.

Inventive Principle:
Principle #3Local quality

Solution Approach 2:

The patent creates a dynamic viscosity response by formulating a blend where lighter components (monoesters, diesters) facilitate cold-start flow, while heavier components (triesters, oligomers) provide thermal thickening at operating temperatures. This dynamic behavior ensures adequate flow at low temperatures while maintaining sufficient viscosity for wear protection during normal operation.

Inventive Principle:
Principle #15Dynamics

3Object-affected harmful factors

If fluorinated olefin refrigerants are used to reduce global warming potential, then environmental performance is improved, but miscibility with traditional lubricants increases causing performance degradation

Engineering Contradiction:
Improveglobal warming potentialVSAvoidphase separation
Core Design Contradiction:
Object-affected harmful factorsVSStability of the object's composition

Solution Approach 1:

The patent changes the chemical parameters of the lubricant by specifying molecular weight ranges (e.g., oligomers with 10-50 repeating units) and compositional ratios that optimize the balance between miscibility and phase stability. This parameter optimization allows the use of environmentally friendly fluorinated olefin refrigerants while preventing excessive dissolution and phase separation.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent formulates a composite polyol ester system that combines components with varying polarities and molecular weights. This composite structure creates a lubricant that is sufficiently miscible with fluorinated olefin refrigerants to prevent stratification, yet maintains compositional stability and prevents excessive refrigerant dissolution across the operating temperature range.

Inventive Principle:
Principle #40Composite materials

Data Source

PatentEP3313965B1Working fluids comprising fluorinated olefins and polyol esters
Publication Date: 2021.07.07 LANXESS CORPORATION

AI summary

High viscosity working fluids comprising a fluorinated olefin refrigerant, such as a hydrofluoro-olefin refrigerant, and a high viscosity polyol ester comprising a select mixture of alkylcarboxy esters of pentaerythritol, di-pentaerythritol, tri-pentaerythritol and pentaerythritol oligomers are provided.