Polyolefin Pellet Posttreatment for Bulk Density and Volatile Removal

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Solution Overview

Problem

Current methods for adjusting the bulk density of pelletized polyolefin resins are insufficient, leading to suboptimal performance in pipe manufacturing and increased shipping costs, as they cannot achieve the desired density without altering the pellet's size or geometry, and fail to effectively remove volatile and organic materials for applications requiring low odor and taste profiles.

Innovation Solution

A process involving pre-heating pellets to a hold temperature below their softening point, maintaining them for 4 to 18 hours, purging volatile materials, and treating them with a thermal destruction process to increase bulk density and reduce organic materials, such as waxes and oligomers, while maintaining or adjusting their level for specific applications.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Volume of stationary object

If current methods adjust bulk density by changing pellet length or geometry, then bulk density is improved, but pellet appearance and dimensions are adversely affected

Engineering Contradiction:
Improvebulk densityVSAvoidpellet geometry
Core Design Contradiction:
Volume of stationary objectVSShape

Solution Approach 1:

The patent applies parameter changes by heating pellets to temperatures between 80-120°C for extended periods (4-18 hours), which modifies the bulk density through thermal treatment without altering pellet geometry. This temperature-time parameter combination enables density adjustment while preserving pellet appearance

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent implements preliminary action by performing heat treatment on pellets before they are used in extrusion or shipping. This pre-treatment process consolidates the pellet structure in advance, achieving the desired bulk density before the pellets encounter any geometric constraints or processing steps

Inventive Principle:
Principle #10Preliminary action

2Quantity of substance

If pellets are shipped with lower bulk density, then shipping container capacity is reduced, but shipping cost per mass increases

Engineering Contradiction:
Improvemass of pellets per containerVSAvoidshipping cost
Core Design Contradiction:
Quantity of substanceVSEase of manufacture

Solution Approach 1:

By changing the temperature parameter during storage and transport (maintaining elevated temperatures), the patent increases bulk density, which directly increases the quantity of pellets per shipping container and reduces shipping costs on a mass basis

Inventive Principle:
Principle #35Parameter changes

3Productivity

If pellets are fed with improper bulk density to grooved feed extruders, then throughput rate decreases, but manufacturing complexity increases

Engineering Contradiction:
Improvethroughput rateVSAvoidextrusion consistency
Core Design Contradiction:
ProductivityVSManufacturing precision

Solution Approach 1:

The patent applies preliminary action by pre-adjusting the bulk density of pellets through heat treatment before they enter the extrusion process. This ensures that when pellets are fed to grooved feed extruders, they have the optimal density for maximum throughput rate and consistent extrusion performance

Inventive Principle:
Principle #10Preliminary action

Solution Approach 2:

The patent changes the bulk density parameter of pellets through thermal treatment, enabling them to flow properly into grooved feed extruders and maintain stable extrusion rates, thereby improving both productivity and manufacturing precision

Inventive Principle:
Principle #35Parameter changes

4Object-generated harmful factors

If volatiles and organic materials are not removed from resin, then processing is simpler, but odor and taste properties deteriorate

Engineering Contradiction:
Improveodor and tasteVSAvoidprocessing steps
Core Design Contradiction:
Object-generated harmful factorsVSDevice complexity

Solution Approach 1:

The patent merges the bulk density adjustment and volatile removal functions into a single heat treatment process. By heating pellets to 80-120°C for extended periods, it simultaneously consolidates the pellet structure and drives off volatiles and organic materials, eliminating the need for separate processing steps

Inventive Principle:
Principle #5Merging (Combining)

Solution Approach 2:

The patent uses parameter changes (temperature and time) to achieve dual benefits: the elevated temperature and extended duration both increase bulk density and remove harmful volatiles, reducing odor and taste issues without requiring additional complex equipment

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process achieves increased bulk density and improved odor and taste properties in polyolefin resins, enhancing pipe production efficiency and reducing shipping costs by allowing higher pellet mass per container, while ensuring compliance with food and water contact standards.

Implementation Method 1

heating the pellets in said holding vessel to a hold temperature for 4 to 18 hours at or below the softening point of the polyolefins

Methodology Applied
Scientific EffectHeating: Heating

Implementation Method 2

purging the holding vessel of volatile materials

Methodology Applied
Scientific EffectPurging:

Implementation Method 3

treating the purged volatile materials by exposing them to at least one thermal destruction process

Methodology Applied
Scientific EffectThermal destruction: Thermolysis

Data Source

PatentEP2635609B1Posttreatment of pelletized polyolefin resins
Publication Date: 2019.09.04 INEOS USA LLC
  • EP2635609B1 patent drawingFigure 1
  • EP2635609B1 patent drawingFigure 2
  • EP2635609B1 patent drawingFigure 3

AI summary

A posttreatment and a system for posttreating pelletized polyolefin resins. The posttreatment comprises a heating step.