Polyolefin Separator Thermal Shrinkage Control

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Solution Overview

Problem

High-capacity lithium ion secondary batteries face challenges with safety and cycle characteristics due to thinner separators, increased risk of internal short circuits, and inadequate resistance against foreign matters and high temperatures, leading to reduced stability and capacity retention.

Innovation Solution

A polyolefin microporous membrane with specific physical properties, including a tensile strength ratio of 0.75 to 1.25, thermal shrinkage rate less than 10% at 120°C, and controlled aluminum content, is developed to enhance resistance against foreign matters and maintain cycle characteristics at high temperatures.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Quantity of substance

If the separator is formed to be thinner to increase battery capacity, then the battery capacity increases, but the risk of internal short circuit increases due to electrode active material penetration

Engineering Contradiction:
Improvebattery capacityVSAvoidrisk of internal short circuit
Core Design Contradiction:
Quantity of substanceVSReliability

Solution Approach 1:

The invention uses a composite microporous membrane comprising a polyolefin base layer combined with a heat-resistant porous layer containing inorganic particles (such as alumina, silica, or boehmite) dispersed in a binder resin. This composite structure provides both the thin profile needed for high capacity and the enhanced mechanical strength and thermal stability required to prevent penetration by electrode active materials, thereby resolving the contradiction between capacity and safety.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention applies different material properties to different regions/layers of the separator. The base layer provides porosity and ion conductivity, while the heat-resistant porous layer provides enhanced mechanical strength and thermal stability. This localized functional differentiation allows the separator to simultaneously achieve thinness for high capacity and sufficient strength to prevent short circuits.

Inventive Principle:
Principle #3Local quality

2Quantity of substance

If the separator thickness is reduced to increase battery capacity, then the battery capacity increases, but the resistance against foreign matters and high temperatures decreases

Engineering Contradiction:
Improvebattery capacityVSAvoidresistance against foreign matters and high temperatures
Core Design Contradiction:
Quantity of substanceVSObject-affected harmful factors

Solution Approach 1:

The composite microporous membrane combines a polyolefin base layer with a heat-resistant porous layer containing inorganic particles (alumina, silica, boehmite) and binder resin. This composite structure provides enhanced resistance against foreign matters and high temperatures while maintaining thin thickness, thereby resolving the contradiction between capacity and resistance to harmful factors.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The heat-resistant porous layer is designed with controlled porosity (30-80%) and specific pore size (0.01-10 μm) to maintain ion conductivity while providing mechanical strength and thermal stability. The porous structure of the inorganic particle-binder composite provides both the necessary permeability for battery operation and the structural integrity to resist foreign matters and high temperatures.

Inventive Principle:
Principle #31Porous materials

3Quantity of substance

If the separator is made thinner to increase battery capacity, then the battery capacity increases, but the cycle characteristics at high temperature deteriorate due to separator shrinkage

Engineering Contradiction:
Improvebattery capacityVSAvoidcycle characteristics at high temperature
Core Design Contradiction:
Quantity of substanceVSDuration of action of stationary object

Solution Approach 1:

The composite microporous membrane combines a polyolefin base layer with a heat-resistant porous layer containing inorganic particles and binder resin. The inorganic particles (alumina, silica, boehmite) have low thermal expansion coefficients and high thermal stability, which constrain the separator from shrinking at high temperatures. This composite structure maintains dimensional stability during cycling at elevated temperatures while keeping the separator thin for high capacity.

Inventive Principle:
Principle #40Composite materials

Solution Approach 2:

The invention addresses thermal expansion issues by incorporating inorganic particles with low thermal expansion coefficients (such as alumina, silica, and boehmite) into the heat-resistant porous layer. These inorganic components counteract the thermal shrinkage tendency of the polyolefin base layer at high temperatures, maintaining separator dimensional stability and preventing short circuits during high-temperature cycling.

Inventive Principle:
Principle #37Thermal expansion

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The membrane provides improved resistance against foreign matters and maintains high cycle characteristics, ensuring safety and capacity retention in high-capacity lithium ion secondary batteries.

Implementation Method 1

a thermal shrinkage rate in the width direction at 120° C. of less than 10%

Methodology Applied
Scientific EffectThermal shrinkage: Thermal Contraction

Implementation Method 2

the possibility that the electrode active material penetrates a separator to cause short circuit is increased because the separator is formed so as to be thinner

Methodology Applied
Scientific EffectPhysical barrier: Physical Containment

Data Source

PatentUS9620754B2Polyolefin microporous membrane and separator for lithium ion secondary battery
Publication Date: 2017.04.11 ASAHI KASEI BATTERY SEPARATOR CORP

AI summary

A polyolefin microporous membrane that can realize a lithium ion secondary battery having favorable resistance against foreign matters or the like, and high cycle characteristics at a high temperature is provided. The present invention provides a polyolefin microporous membrane having a ratio of tensile strength in a length direction to that in a width direction of 0.75 to 1.25, and a thermal shrinkage rate in the width direction at 120° C. of less than 10%.