Acid-Base Washing for Polyolefin VOC Removal

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Solution Overview

Problem

Current recycling methods for polyolefins, particularly polypropylene and polyethylene, face challenges in achieving high purity and quality due to contamination and poor mechanical properties, with existing methods for removing volatile organic compounds being energy-intensive and inefficient.

Innovation Solution

A process involving treatment with an aqueous solution of an inorganic oxoacid at a pH of 2.0 or lower, followed by a caustic solution at a pH of 7.0 or higher, to reduce hydrophobic and hydrophilic volatile organic compounds in recycled polyolefins, improving their mechanical and odor properties.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Object-generated harmful factors

If aeration is used to remove volatile organic compounds from recycled polyolefin, then VOC content is reduced, but energy consumption increases significantly

Engineering Contradiction:
ImproveVOC contentVSAvoidenergy consumption
Core Design Contradiction:
Object-generated harmful factorsVSUse of energy by moving object

Solution Approach 1:

The invention changes the chemical parameters of the treatment solution by adjusting pH levels (using acid at pH 2.0 or lower, then base at pH 7.0 or higher) to selectively remove different types of VOCs. This chemical parameter approach replaces the energy-intensive physical aeration process, achieving VOC removal through chemical reactions rather than thermal/oxidative aeration.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The invention replaces the mechanical/physical aeration system with a chemical treatment system using aqueous acid and base solutions. Instead of using mechanical aeration equipment to remove VOCs, the process uses chemical reactions with treatment solutions, substituting a mechanical removal process with a chemical extraction process that consumes less energy.

Inventive Principle:
Principle #28Mechanics substitution (Replace mechanical system)

2Ease of manufacture

If recycled polyolefin is used directly, then production cost is reduced, but mechanical properties and odor performance deteriorate

Engineering Contradiction:
Improveproduction costVSAvoidmechanical properties
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The invention applies preliminary chemical treatment to recycled polyolefin before it is used in final applications. By pre-treating the material with acid and base solutions to remove VOCs and contaminants, the process ensures that the recycled material meets quality requirements before being incorporated into products, thereby maintaining mechanical properties and odor performance while still using cost-effective recycled content.

Inventive Principle:
Principle #10Preliminary action

3Ease of manufacture

If recycled polyolefin is used directly, then production cost is reduced, but odor and taste performance deteriorate

Engineering Contradiction:
Improveproduction costVSAvoidodor and taste
Core Design Contradiction:
Ease of manufactureVSObject-generated harmful factors

Solution Approach 1:

The invention changes the chemical environment parameters by using acid treatment (pH 2.0 or lower) followed by base treatment (pH 7.0 or higher) to selectively remove odor-causing VOCs. This parameter-based chemical treatment approach removes hydrophobic functional group-containing VOCs and hydrophilic VOCs that cause odor and taste issues, while maintaining cost-effectiveness by using simple aqueous treatment solutions rather than expensive purification systems.

Inventive Principle:
Principle #35Parameter changes

Data Source

PatentUS20230323069A1Removal of odorants from post-consumer polyolefin waste
Publication Date: 2023.10.12 BOREALIS AG

AI summary

A process for reducing the hydrophobic functional group-containing volatile organic compound content and hydrophilic volatile organic compound content of recycled polyolefin comprising an acid washing step followed by an alkaline/neutral washing step.