Polypropylene Nonwoven Beta Nucleating Agent Spinning Stability

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Solution Overview

Problem

Polypropylene-based nonwoven and yarn production processes face limitations due to high draw forces, unstable process conditions, and narrow thermal bonding windows, particularly with Ziegler-Natta and metallocene polypropylenes, which affect spinning speeds and tensile strengths.

Innovation Solution

Incorporating beta nucleating agents into polypropylene during the spunbonding, meltblowing, or Bulk Continuous Filament processes to improve processability, stability, and thermal bonding characteristics by forming a mixture with polypropylene, extruding, quenching, and bonding the fibers or yarns, which enhances elongational viscosity and melting range.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Speed

If Ziegler-Natta or metallocene polypropylenes are used in spunbonding or meltblowing processes, then the polypropylene can be processed into nonwoven webs or yarns, but the process becomes unstable at high spinning speeds due to significant elongational viscosity decrease

Engineering Contradiction:
Improvespinning speedVSAvoidprocess stability
Core Design Contradiction:
SpeedVSReliability

Solution Approach 1:

The patent changes the chemical composition parameters of polypropylene by incorporating specific comonomers (ethylene, propylene, butene, pentene, or hexene) in controlled ratios (5-95 wt% polypropylene, 5-95 wt% comonomer). This compositional parameter change modifies the polymer's rheological properties to maintain elongational viscosity at high spinning speeds, thereby stabilizing the process while enabling higher production speeds.

Inventive Principle:
Principle #35Parameter changes

Solution Approach 2:

The patent creates composite polypropylene materials by combining polypropylene with specific comonomers (ethylene, propylene, butene, pentene, or hexene) to form copolymer compositions. This composite approach leverages the complementary properties of different polymer components to achieve both high processability at elevated speeds and maintained structural integrity during spinning operations.

Inventive Principle:
Principle #40Composite materials

2Speed

If metallocene polypropylenes are used, then higher spinning speeds can be achieved, but the narrow melting range creates a narrow thermal bonding process window that limits overall process speed

Engineering Contradiction:
Improvespinning speedVSAvoidoverall process speed
Core Design Contradiction:
SpeedVSProductivity

Solution Approach 1:

The patent modifies the thermal parameters of polypropylene by incorporating comonomers that broaden the melting range. This parameter change in the polymer composition allows for a wider thermal bonding process window, enabling the bonding step to proceed at broader temperature ranges and thus increasing overall process productivity while maintaining high spinning speeds.

Inventive Principle:
Principle #35Parameter changes

3Length of moving object

If high draw force is applied to attenuate filaments, then finer fiber diameters can be achieved, but the process becomes more difficult and requires higher energy input

Engineering Contradiction:
Improvefiber diameterVSAvoidprocess difficulty
Core Design Contradiction:
Length of moving objectVSEase of manufacture

Solution Approach 1:

The patent changes the rheological parameters of the polymer melt by incorporating specific comonomers, which modifies the viscosity-temperature relationship. This parameter change allows filament attenuation to occur at lower draw forces and reduced energy inputs while still achieving the desired fine fiber diameters, thereby reducing process difficulty and energy consumption.

Inventive Principle:
Principle #35Parameter changes

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The use of beta nucleating agents stabilizes high-speed spinning, reduces filament breaks, allows finer fiber diameters, increases tensile strength, and broadens the thermal bonding window, leading to higher production speeds and improved mechanical properties of nonwovens and yarns.

Implementation Method 1

beta nucleating agents are added to the polymer to be processed

Methodology Applied
Scientific EffectNucleation: Nucleation

Implementation Method 2

forming a mixture with polypropylene, extruding, quenching, and bonding the fibers or yarns

Methodology Applied
Scientific EffectCrystallization: Crystallisation

Implementation Method 3

extruding a mixture comprising a polypropylene and a beta-nucleating agent to form fibers

Methodology Applied
Scientific EffectExtrusion: Extrusion

Implementation Method 4

quenching the fibers

Methodology Applied
Scientific EffectQuenching: Freezing

Data Source

PatentEP2633104A1Nonwoven and yarn polypropylene with additivation
Publication Date: 2013.09.04 LUMMUS NOVOLEN TECH

AI summary

A process to produce improved polypropylene nonwovens or yarns by extruding a mixture of polypropylene(s) and beta nucleating agent(s), or in the alternative, certain clarifiers, to form the improved polypropylene filaments.