Non-Reactive Polysiloxane Pigment Coating for Thermoplastic Stability

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Solution Overview

Problem

Inorganic pigments can adversely affect plastics due to active sites on their surfaces and high residual moisture content, leading to polymer degradation, discoloration, and instability, especially under thermal stress, and existing organic coatings can react with water to form undesirable reaction products.

Innovation Solution

Treating inorganic pigments with non-reactive polysiloxanes that cover active sites and reduce moisture content, such as polydimethylsiloxanes with specific viscosities and formulations, to enhance stability and compatibility with plastics.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If inorganic pigments are used without coating, then coloring function is achieved, but polymer degradation occurs due to active sites on pigment surface

Engineering Contradiction:
Improvecoloring functionVSAvoidpolymer stability
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

A silane coupling agent is introduced as an intermediary substance between the inorganic pigment and the polymer matrix. The silane coupling agent contains reactive groups that bond to both the pigment surface and the polymer, creating a stable interface that prevents direct interaction between active pigment sites and the polymer, thereby preventing degradation while maintaining manufacturing simplicity

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The solution creates a composite structure where the inorganic pigment is combined with a silane coupling agent layer, forming a hybrid material system. This composite approach allows the pigment to maintain its coloring function while the silane layer provides protective properties that prevent polymer degradation

Inventive Principle:
Principle #40Composite materials

2Reliability

If inorganic pigments are coated with organic coatings, then polymer stability is improved, but reaction products like hydrogen and alcohols are formed

Engineering Contradiction:
Improvepolymer stabilityVSAvoidreaction products formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention changes the chemical parameters of the coating by using silane coupling agents with specific reactive groups that undergo controlled hydrolysis and condensation reactions. This parameter change allows the coating to provide stability without forming harmful reaction products like hydrogen and alcohols that are generated by conventional organic coatings

Inventive Principle:
Principle #35Parameter changes

3Reliability

If inorganic pigments are coated with silane, then polymer stability is improved, but water bound to pigment surface reacts to form alcohols

Engineering Contradiction:
Improvepolymer stabilityVSAvoidalcohol formation
Core Design Contradiction:
ReliabilityVSObject-generated harmful factors

Solution Approach 1:

The invention converts the harmful reaction between bound water and silane (which produces alcohols) into a beneficial process by controlling the hydrolysis and condensation reactions of the silane coupling agent. The bound water that would normally cause problems is instead utilized as part of the controlled silane reaction mechanism, forming a stable coating without harmful alcohol byproducts

Inventive Principle:
Principle #22Blessing in disguise (Convert harm into benefit)

4Ease of manufacture

If inorganic pigments with high residual moisture are used, then pigment properties are maintained, but discoloration of plastic occurs

Engineering Contradiction:
Improvepigment propertiesVSAvoiddiscoloration
Core Design Contradiction:
Ease of manufactureVSObject-affected harmful factors

Solution Approach 1:

The silane coupling agent is applied to the pigment surface in advance, creating a protective layer before the pigment is incorporated into the polymer matrix. This preliminary action prevents subsequent interactions between moisture on the pigment surface and the polymer that would cause discoloration, while maintaining the pigment's inherent properties

Inventive Principle:
Principle #10Preliminary action

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The treated inorganic pigments exhibit improved storage stability, reduced polymer degradation, and enhanced mechanical properties in plastics, with low residual moisture and minimal formation of reaction products like hydrogen or alcohols, making them suitable for use in thermoplastics and materials intended for contact with food.

Implementation Method 1

the at least one non-reactive polysiloxane is adsorbed on the inorganic pigment

Methodology Applied
Scientific EffectAdsorption: Adsorption

Implementation Method 2

The treated inorganic pigments exhibit improved storage stability, reduced polymer degradation, and enhanced mechanical properties in plastics, with low residual moisture

Methodology Applied
Scientific EffectDesorption: Desorption

Data Source

PatentEP3607005B1Pigment treated with at least one non-reactive polysiloxane for use in thermoplastics
Publication Date: 2021.04.14 HUNTSMAN P&A UERDINGEN GMBH
  • EP3607005B1 patent drawingFigure 1
  • EP3607005B1 patent drawingFigure 2
  • EP3607005B1 patent drawingFigure 3

AI summary

The present invention relates to inorganic pigments treated/coated with at least one non-reactive polysiloxane, methods for producing these coated inorganic pigments, thermoplastics comprising these coated inorganic pigments and methods for the production of these thermoplastics.