Polyurethane Acid Dyeing With Quaternary Ammonium Mediators

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Solution Overview

Problem

Acid dyes are ineffective in dyeing polyurethane materials under mild conditions, resulting in only light tinting, and metal complex dyes, while effective, are expensive and limited in color palette.

Innovation Solution

An aqueous dye solution comprising an acid dye compound and a quaternary ammonium compound, such as tetrabutylammonium or tetrahexylammonium salts, with a water-soluble organic solvent, is used to enhance the affinity of acid dyes for polyurethane materials, achieving deeper, richer colors and improved colorfastness.

Engineering Contradictions & Design Principles

VSEngineering Contradiction Analysis

1Ease of manufacture

If acid dyes are used under mild dyeing conditions, then the dyeing process is simple and cost-effective, but the color intensity and affinity are insufficient resulting in only light tinting

Engineering Contradiction:
Improvedyeing process simplicityVSAvoidcolor intensity
Core Design Contradiction:
Ease of manufactureVSManufacturing precision

Solution Approach 1:

A surfactant is introduced as an intermediary substance between the acid dye and polyurethane material. The surfactant forms a complex with the acid dye, enhancing its affinity for the polyurethane substrate and enabling intense coloration under mild dyeing conditions without requiring harsh chemicals or extreme temperatures.

Inventive Principle:
Principle #24Intermediary (Mediator)

Solution Approach 2:

The invention creates a composite dyeing system combining surfactant, acid dye, and polyurethane material. This composite approach allows the surfactant-dye complex to effectively interact with the polyurethane substrate, achieving both process simplicity and high color intensity simultaneously.

Inventive Principle:
Principle #40Composite materials

2Manufacturing precision

If metal complex dyes are used to achieve effective dyeing of polyurethane, then color intensity and affinity are improved, but cost increases and color palette is limited to subdued tones

Engineering Contradiction:
Improvecolor intensityVSAvoiddyeing cost
Core Design Contradiction:
Manufacturing precisionVSEase of manufacture

Solution Approach 1:

The invention replaces expensive metal complex dyes with a combination of inexpensive acid dyes and surfactants. This substitution achieves comparable or superior color intensity and affinity while significantly reducing material costs and expanding the available color palette to include bright, vibrant shades.

Inventive Principle:
Principle #27Cheap short-living objects (Disposable)

Solution Approach 2:

The invention changes the chemical parameters of the dyeing system by introducing surfactants that modify the interaction between dye and substrate. This parameter change enables acid dyes to achieve metal-complex-level performance in terms of affinity and color intensity, while maintaining the cost advantages and color versatility of acid dyes.

Inventive Principle:
Principle #35Parameter changes

3Ease of manufacture

If conventional acid dyeing of polyurethane is attempted, then the process is simple, but colorfastness is poor

Engineering Contradiction:
Improvedyeing process simplicityVSAvoidcolorfastness
Core Design Contradiction:
Ease of manufactureVSReliability

Solution Approach 1:

The surfactant acts as a mediating agent that improves the bonding between acid dye and polyurethane substrate. By forming a surfactant-dye complex, the system achieves better colorfastness and reduced color migration while maintaining the simplicity of the acid dyeing process, avoiding the need for harsh processing conditions.

Inventive Principle:
Principle #24Intermediary (Mediator)

Applied Scientific Principles

This section explains which scientific principles are used to turn an abstract innovation direction into a practical engineering solution.

Function Achieved in This Case

The process provides intensely colored, colorfast polyurethane products with a wide range of colors, including bright shades, at a lower cost than metal complex dyes, while maintaining stability and effectiveness.

Implementation Method 1

addition of particular ammonium salts to the dye solution increases affinity of the acid dye molecules toward the polyurethane materials

Methodology Applied
Scientific EffectElectrostatic interaction: Ion Repulsion/Attraction

Implementation Method 2

an aqueous dye solution comprising an acid dye compound and a quaternary ammonium compound... wherein the aqueous dye solution is prepared by dissolving the acid dye compound in water

Methodology Applied
Scientific EffectDissolution: Solvation

Data Source

PatentEP2964829B1Acid dyeing of polyurethane materials
Publication Date: 2018.07.04 NIKE INNOVATE CV

AI summary

A polyurethane is dyed with an aqueous solution of an acid dye compound, a quaternary ammonium compound selected from soluble tetrabutylammonium compounds and tetrahexylammonium compounds, and, optionally, an water-soluble organic solvent.